• Title/Summary/Keyword: Volatile Data

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Partial Freezing as a Means of Keeping Quality of Sea Foods 1. Keeping Quality of Baked Mackerel Muscle during Partially Frozen Storage (빙결점동결에 의한 수산식품의 품질보존에 관한 연구 1. 빙결점동결 저장 중의 구운 고등어의 품질변화)

  • Lee, Eung Ho;Kim, Jeong Gyun;Ha, Jae Ho;Oh, Kwang Soo;Cha, Yong-Jun
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.12 no.2
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    • pp.62-65
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    • 1983
  • As a new practical method for preserving freshness of fish, partially frozen storage has been reported to be useful in terms of K-value, TBA value, sensory evaluation etc. In order to develop a storage procedure to be used in place of cooled or frozen storage for the preservation of precooked fish food, partial freezing for up to two to three weeks was examined using baked mackerel. The criteria for evaluation were made according to the changes in volatile basic nitrogen (VBN), thiobarbituric acid (TBA) value, viable bacterial number, pH, color difference and sensory evaluation in fish muscle. The changes in TBA value of baked muscle during storage at $-3^{\circ}C$ differed slightly from those obserbed during cooled ($5^{\circ}C$) and frozen storage ($-20^{\circ}C$). Partial frozen storage ($-3^{\circ}C$) was effective in prolong an induction period of lipid oxidation during early storage. VBN of baked muscle tends to increase slowly while pH value was decrease during storage and there was no observed significant differences among three different storage condition. Viable bacterial number of the baked mackerel muscle stored at $-3^{\circ}C$ showed significantly less than that stored at $5^{\circ}C$, and similar to that stored at $-20^{\circ}C$ (the levels of $10^2/g$). Judging from the results of sensory evaluation and experimental data, partial frozen storage at $-3^{\circ}C$ seems to be effective as means of short-period preserving baked mackerel.

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A portable electronic nose (E-Nose) system using PDA device (개인 휴대 단말기 (PDA)를 기반으로 한 휴대용 E-Nose의 개발)

  • Yang, Yoon-Seok;Kim, Yong-Shin;Ha, Seung-Chul;Kim, Yong-Jun;Cho, Seong-Mok;Pyo, Hyeon-Bong;Choi, Chang-Auck
    • Journal of Sensor Science and Technology
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    • v.14 no.2
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    • pp.69-77
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    • 2005
  • The electronic nose (e-nose) has been used in food industry and quality controls in plastic packaging. Recently it finds its applications in medical diagnosis, specifically on detection of diabetes, pulmonary or gastrointestinal problem, or infections by examining odors in the breath or tissues with its odor characterizing ability. Moreover, the use of portable e-nose enables the on-site measurements and analysis of vapors without extra gas-sampling units. This is expected to widen the application of the e-nose in various fields including point-of-care-test or e-health. In this study, a PDA-based portable e-nose was developed using micro-machined gas sensor array and miniaturized electronic interfaces. The rich capacities of the PDA in its computing power and various interfaces are expected to provide the rapid and application specific development of the diagnostic devices, and easy connection to other facilities through information technology (IT) infra. For performance verification of the developed portable e-nose system, Six different vapors were measured using the system. Seven different carbon-black polymer composites were used for the sensor array. The results showed the reproducibility of the measured data and the distinguishable patterns between the vapor species. Additionally, the application of two typical pattern recognition algorithms verified the possibility of the automatic vapor recognition from the portable measurements. These validated the portable e-nose based on PDA developed in this study.

Feasibility test for Solidified Fuel with Cow Manure (고체연료화 방법을 적용한 우분 처리 가능성 평가)

  • Jeong, Kwang-Hwa;Kim, Jung-Kon;Lee, Dong-Jun
    • Journal of Soil and Groundwater Environment
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    • v.22 no.6
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    • pp.112-119
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    • 2017
  • In this study, the availability of cow manure as raw material for solid fuel production was investigated. Since the water content of the cow manure was too high, it was dewatered using a laboratory hydraulic compressure ($11.3kg/cm^2$). The moisture content of the cow manure decreased from 82.01% to 73.36 wt.%. The dewatered cow manure was homogenized by the experimental apparatus and then put into the rotating cylindrical apparatus. From the consecutive processes, the cow ball-shaped pellet which size ranged from 3.0 to 25.0 mm was produced. The major factor for making palletized fuel from cow manure was the moisture content. Based on the experimental data, the moisture content of cow manure for pelletizing cow manure was identified as 65~75 wt.%. When the moisture content of the cow manure was lower than 30 wt.%, the diameter of the pellets maded from cow manure was smaller than 3 mm. On the other hand, when the water content of the cow manure was higher than 75 wt/%, the diameter of the processed pellets tended to be larger than 25 mm. The characteristics of the processed cow manure pellets was analyzed to be in accordance with the livestock solid fuel quality standard. The pyrolysis characteristic of the pellet was analyzed by raising the heating temperature of the experimental equipment from 200 to $900^{\circ}C$. The mass change between of 20 and $130^{\circ}C$ corresponds to the amount of moisture contained in the cow manure. The amount of moisture was about 15% of the total weight of cow manure samples. The cow manure pellet was thermally stable up to $280^{\circ}C$. It can be interpreted that combustion of cow manure pellet does not occur until the surface temperature reaches $280^{\circ}C$. The mass change of pellet between of 280 and $450^{\circ}C$ was considered to be due to the vaporization of volatile organic compounds (VOCs) present in the cow manure pellet. The maximum production of VOCs was showed near $330^{\circ}C$.

Laboratory Evaluation of the Accuracy, Precision, and Inter-instrumental Variance of a Portable Photoionization Detector (휴대용 광이온화 검출기의 정확도, 정밀도 및 기기간 차이에 대한 실험실 평가)

  • Choi, Dongmin;Choi, Youngeun;Yoon, Chungsik;Rhie, Kwangwon;Lee, Yunkeun;Lee, Ikmo;Park, Jeongim
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.22 no.3
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    • pp.200-208
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    • 2012
  • Objectives: This study investigated the performance of three separate units of a portable photoionization detector (PID, ppb-RAE 3000) for measuring volatile organic compounds (VOCs) in a laboratory. Methods: A laboratory evaluation of the accuracy, precision, and inter-instrumental variance of three separate units of a portable PID (ppb-RAE 3000) was performed. The evaluation was based on the preparation of a test air sample of known toluene or ethylacetate concentration in a Tedlar$^{(R)}$ bag. The test air sample was monitored and data were logged consecutively by the three PIDs. A certified gas of 50 ppm toluene was also monitored during the test to ensure the reliability of the generated test air sample. Four different concentrations ranging from 0.1 to 2 TLV were used and a series of five measurements for each concentration level was performed. The accuracy was evaluated using National Institute for Occupational Safety and Health (NIOSH) criteria. Results: The results from the oldest ppb-RAE3000 unit among the three test units generally fell outside the NIOSH recommended accuracy criteria of ${\pm}25%$, whereas the other two units produced results which were acceptable at, or greater than, 25 ppm of toluene, or 0.5 TLV. These units also met the NIOSH criteria for some ethylacetate measurements but the results were not consistent. Conclusions: Considering the inconsistent performance of these ppb-RAE 3000 units, this device may not be appropriate for use as an alternative to the standard measurement methods. However, it can serve good survey instruments to identify exposure sources or concentration profiles. For all applications, the ppb-RAE 3000 should be used with frequent calibration checks, additional validation using a reference material, and careful maintenance.

Chemical Changes of Low Salt Gulbi (salted and dried yellow corvenia) during Hot-air Drying with Different Temperatures (저염 굴비 제조 시 열풍건조 온도에 따른 화학적 특성 변화)

  • Gwak, Hyun-Jung;Eun, Jong-Bang
    • Korean Journal of Food Science and Technology
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    • v.42 no.2
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    • pp.147-154
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    • 2010
  • Gulbi, made of fresh yellow corvenia (Psendosciaena manchurica) that has been salted and dried, is one of the most popular traditional marine foods in Korea. The objective of this study was to develop a method to safely manufacture Gulbi with low levels of oxidation and contamination, by a hot air drying method. Changes in total acidity, pH, salt concentration, thiobarbituric acid-reactive substance (TBARS) and volatile basic nitrogen (VBN) were measured during drying at 30, 35 and $40^{\circ}C$ for 15 days in a hot air-dryer using a semi-dried method. Acidity increased with increasing drying time at all drying temperatures. The pH decreased gradually with increasing drying time. Salt concentration was increased as drying time increased at all drying temperatures due to moisture loss. The VBN increased as drying time increased for all drying temperatures. Data indicate that the drying at $35^{\circ}C$ appears to have a significant sensory and physicochemical advantage in Gulbi products.

Herd Behavior in the Bangladeshi Loan Market (방글라데시 상업은행의 군집행동에 관한 분석)

  • Hyeon, Jeong-Whan
    • International Area Studies Review
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    • v.22 no.1
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    • pp.123-140
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    • 2018
  • This paper analyzes herd behavior observed in the loan market from 2001 to 2014 using a panel data on commercial banks including state-owned banks, domestic private banks, foreign banks, and Islamic banks. The paper finds evidence that herd behaviors of domestic private and foreign banks have been pronounced and long-lasting around the 2008 global financial crisis when state-owned banks did not show such a behavior. This result shows that since private banks tend to be keen on maximizing profits and avoid financial risks exposed by lending during a financial crisis, their lending decisions are not independent but dependent on whether other banks increase loans or not. On the other hand, Islamic banks do not show herd behavior during the financial crisis. This finding is consistent with earlier studies that Islamic banks have different characteristics, such as profit and operation mechanisms, from other private banks. Another interesting finding is that when it comes to rural loans, all the banks' herd behavior is short-lived and the herding indexes are quite volatile. This finding is attributable to distinct features of rural loans. Usually maturities of rural loans are shorter than city loans and related to the cycle of farming. Agricultural production is heavily dependent on unpredicted factors, such as floods and droughts, not previous year's production. Lastly, the paper finds a herding across bank type that state-owned, foreign, and Islamic banks follow domestic private banks'lending decisions.

Quantitative analysis of glycerol concentration in red wine using Fourier transform infrared spectroscopy and chemometrics analysis

  • Joshi, Rahul;Joshi, Ritu;Amanah, Hanim Zuhrotul;Faqeerzada, Mohammad Akbar;Jayapal, Praveen Kumar;Kim, Geonwoo;Baek, Insuck;Park, Eun-Sung;Masithoh, Rudiati Evi;Cho, Byoung-Kwan
    • Korean Journal of Agricultural Science
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    • v.48 no.2
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    • pp.299-310
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    • 2021
  • Glycerol is a non-volatile compound with no aromatic properties that contributes significantly to the quality of wine by providing sweetness and richness of taste. In addition, it is also the third most significant byproduct of alcoholic fermentation in terms of quantity after ethanol and carbon dioxide. In this study, Fourier transform infrared (FT-IR) spectroscopy was employed as a fast non-destructive method in conjugation with multivariate regression analysis to build a model for the quantitative analysis of glycerol concentration in wine samples. The samples were prepared by using three varieties of red wine samples (i.e., Shiraz, Merlot, and Barbaresco) that were adulterated with glycerol in concentration ranges from 0.1 to 15% (v·v-1), and subjected to analysis together with pure wine samples. A net analyte signal (NAS)-based methodology, called hybrid linear analysis in the literature (HLA/GO), was applied for predicting glycerol concentrations in the collected FT-IR spectral data. Calibration and validation sets were designed to evaluate the performance of the multivariate method. The obtained results exhibited a high coefficient of determination (R2) of 0.987 and a low root mean square error (RMSE) of 0.563% for the calibration set, and a R2 of 0.984 and a RMSE of 0.626% for the validation set. Further, the model was validated in terms of sensitivity, selectivity, and limits of detection and quantification, and the results confirmed that this model can be used in most applications, as well as for quality assurance.

Effects of using different roughages in the total mixed ration inoculated with or without coculture of Lactobacillus acidophilus and Bacillus subtilis on in vitro rumen fermentation and microbial population

  • Miguel, Michelle;Mamuad, Lovelia;Ramos, Sonny;Ku, Min Jung;Jeong, Chang Dae;Kim, Seon Ho;Cho, Yong Il;Lee, Sang Suk
    • Animal Bioscience
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    • v.34 no.4
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    • pp.642-651
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    • 2021
  • Objective: This study aimed to determine the effects of different roughages in total mixed ration (TMR) inoculated with or without coculture of Lactobacillus acidophilus (L. acidophilus) and Bacillus subtilis (B. subtilis) on in vitro rumen fermentation and microbial population. Methods: Three TMRs formulations composed of different forages were used and each TMR was grouped into two treatments: non-fermented TMR and fermented TMR (F-TMR) (inoculated with coculture of L. acidophilus and B. subtilis). After fermentation, the fermentation, chemical and microbial profile of the TMRs were determined. The treatments were used for in vitro rumen fermentation to determine total gas production, pH, ammonianitrogen (NH3-N), and volatile fatty acids (VFA). Microbial populations were determined by quantitative real-time polymerase chain reaction (PCR). All data were analyzed as a 3×2 factorial arrangement design using the MIXED procedure of Statistical Analysis Systems. Results: Changes in the fermentation (pH, lactate, acetate, propionate, and NH3-N) and chemical composition (moisture, crude protein, crude fiber, and ash) were observed. For in vitro rumen fermentation, lower rumen pH, higher acetate, propionate, and total VFA content were observed in the F-TMR group after 24 h incubation (p<0.05). F-TMR group had higher acetate concentration compared with the non-fermented group. Total VFA was highest (p<0.05) in F-TMR containing combined forage of domestic and imported source (F-CF) and F-TMR containing Italian ryegrass silage and corn silage (F-IRS-CS) than that of TMR diet containing oat, timothy, and alfalfa hay. The microbial population was not affected by the different TMR diets. Conclusion: The use of Italian ryegrass silage and corn silage, as well as the inoculation of coculture of L. acidophilus and B. subtilis, in the TMR caused changes in the pH, lactate and acetate concentrations, and chemical composition of experimental diets. In addition, F-TMR composed with Italian ryegrass silage and corn silage altered ruminal pH and VFA concentrations during in vitro rumen fermentation experiment.

A preliminary study of sorptive characteristics of aromatic volatile organic compounds (VOC) on clothing materials (방향족 유기화합물의 가스상 시료를 이용한 피복류의 흡착특성 비교에 대한 예비연구)

  • Kim, K.H.;Im, M.S.;Park, S.Y.;Hong, Y.J.;Choi, Y.J.;Lee, Y.S.;Kim, S.D.;Nam, S.H.;Ok, J.S.
    • Analytical Science and Technology
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    • v.19 no.3
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    • pp.255-262
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    • 2006
  • In this study, we attempted to evaluate the sorptive loss of VOC upon their contact with different material surfaces including clothing pieces. For the purpose of this study, we developed a method to evaluate such loss by employing a filter holder pack in the thermal desorption line of the GC/FID system. The calibration curves of different aromatic VOCs including benzene, toluene, and xylene were made by loading them at different quantities through the analytical line. A series of experiments were conducted repetitively to draw calibration data sets for all three materials covering glass fiber, cotton, and nylon. The results were then compared in terms of both material types and of VOC types. The extent of sorptive loss increased in a highly systematic manner across different materials such as glass fiber, cotton, and nylon. The patterns of sorptive loss also increased gradually across VOC type such toward in the direction of increasing molecular weights: benzene, toluene, and xylene. According to this experimental study, it is concluded that sorptive behavior of pollutint compounds like VOC can be controlled by the combined effects of both chemical properties and material characteristics.

Preliminary Study on Effect of the Field Correlation Factor for Increasing of the Accuracy in a Direct Reading Instruments on Photoionization Detector for Total Volatile Organic Compounds (총휘발성유기화합물 측정 직독식장비 정확도 향상을 위한 현장보정계수 활용 연구)

  • Sungho Kim;Gwangyong Yi;Sujin Kim;Hae Dong Park
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.34 no.1
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    • pp.67-76
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    • 2024
  • Objectives: Direct reading instruments (DRIs) are widely used by industrial hygienists and other experts for preliminary survey and identifying source locations in many industrial fields. Photoionization detectors (PIDs), which are a form of hand-held portable DRIs, have been used for a variety of airborne vaporized chemicals, especially evaporated hydrocarbon solvents. The benefits of PIDs are high sensitivity between each chemical, competitive price, and portability. With the goal of increasing the accuracy of logged PID concentrations, previous studies have performed tests for the assessment of single chemical compounds, not mixtures. The purpose of this preliminary study was to measure mixtures with a PID and charcoal tube at the same time and compare the accuracy between them. Methods: A chamber test was implemented with different mixtures of hydrocarbon chemicals (acetone, isopropyl alcohol, toluene, m-xylene) and levels in the range of 14 to 864 ppm. Three PIDs and charcoal tubes were connected to the chamber and measured the chemical mixtures simultaneously. A comparison of accuracy and the PID group of concentrations with manufacture correction factor (M_CF) and field correction factor (F_CF) applied was performed. Results: The accuracy of the PID concentrations data-logged from the PID did not meet the accuracy criteria except for the mixture level B and C logged from PID No. 2, which was 18% of all tests for meeting accuracy criteria. The mean and standard deviation (SD) of concentration (ppm) of the charcoal tube followed by each mixtures' level were 10.37±0.26, 155.33±5.28, 300.80±11.65, and 774.93±22.65, respectively. When applying F_CF into the PID concentrations, the accuracy increased by nearly 82%. However, in the case of M_CF, none met the accuracy criterion. Between the PID there were differences of logged concentrations. Conclusions: In this preliminary study, the concentration of a logged PID with F_CF applied was a better way to increase accuracy compared to applying M_CF. We suggest that additional research is necessary to consider environmental factors such as temperature and humidity.