• Title/Summary/Keyword: Vacuum condition

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Electrical characteristics of polycrystalline 3C-SiC thin film diodes (다결정 3C-SiC 박막 다이오드의 전기적 특성)

  • Chung, Gwiy-Sang;Ahn, Jeong-Hak
    • Journal of Sensor Science and Technology
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    • v.16 no.4
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    • pp.259-262
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    • 2007
  • This paper describes the electrical characteristics of polycrystalline (poly) 3C-SiC thin film diodes, in which poly 3C-SiC thin films on n-type and p-type Si wafers, respectively, were deposited by APCVD using HMDS, $H_{2}$, and Ar gas at $1150^{\circ}C$ for 3 hr. The schottky diode with Au/poly 3C-SiC/Si (n-type) structure was fabricated. Its threshold voltage ($V_{bi}$), breakdown voltage, thickness of depletion layer, and doping concentration ($N_{D}$) value were measured as 0.84 V, over 140 V, 61 nm, and $2.7{\times}10^{19}cm^{-3}$, respectively. Moreover, for the good ohmic contact, Al/poly 3C-SiC/Si (n-type) structure was annealed at 300, 400, and $500^{\circ}C$, respectively for 30 min under the vacuum condition of $5.0{\times}10^{-6}$ Torr. Finally, the p-n junction diodes fabricated on the poly 3C-Si/Si (p-type) were obtained like characteristics of single 3CSiC p-n junction diode. Therefore, poly 3C-SiC thin film diodes will be suitable for microsensors in conjunction with Si fabrication technology.

Microstructure of Electron Beam Welded Cu / STS 304 Dissimilar Materials (전자빔 용접된 Cu / STS 304강의 미세조직에 관한 연구)

  • Park, Kyoung-Tae;Kim, In-Ho;Baek, Jun-Ho;Chun, Byung-Sun
    • Journal of Welding and Joining
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    • v.28 no.2
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    • pp.47-53
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    • 2010
  • According to the research report for the recent a few years, the dissimilar welding of Cu and STS 304 alloy have been presented that a weldability is very poor. This article present a study on Lap joint by Electron beam welding dissimilar materials. The weld metals was constituted between pure copper and STS 304 steel. The experiment was performed with 125mA welding current, 520mA focusing current. The Vacuum condition of chamber is 5${\times}$10-5torr and welding speed is 300mm/min. Showing the bead shape of weld metal, the thickness of the stainless 304 using as the protect materials is 3mm and the thickness of a copper is 15mm. The analysis about the microstructure were carried out in which it was observed with SEM. The results showed that complex heterogeneous fusion zone microstructure characterized both by rapid cooling and mixing of the molten metal, however the liquation crack was formated in the fusion line.

Formation of Al2O3 Film by Activated Reactive Evaporation Method (활성화 반응 증발법에 의한 Al2O3 박막 형성)

  • Park, Yong-Gwon;Choi, Jae-Ha
    • Journal of the Korean Society for Heat Treatment
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    • v.14 no.5
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    • pp.292-296
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    • 2001
  • In this work, an ultra-high vacuum activated reactive evaporation equipment was built. With reaction of Al and oxygen plasma, $Al_2O_3$ was deposited on the surface of etched Al foil. The chamber was evacuated down to $2{\times}10^{-7}$ torr initially. The Ar and $O_2$ gas introduced into the chamber to maintain $5{\times}10^{-5}$ torr during deposition. Ar gas prevents recombining of the ionized oxygen. Evaporation was maintained by electron beam evaporator continuously. Heating filament and electrode were used in order to generate plasma. The substrate bias of -300V was introduced to accelerate deposition of evaporated Al atoms. The composition and morphology of deposited $Al_2O_3$ films were analyzed by x-ray photoelectron spectroscopy(XPS) and atomic force microscopy (AFM), respectively. The Al oxide was formed on the surface of etched Al foil. According to AFM results, the surface morphology of $Al_2O_3$ film indicates uniform feature. Dielectric characteristic was measured as a function of frequency. Measured withstanding voltage and capacitance were 52V and $24{\mu}F/cm^2$, respectively. The obtained $Al_2O_3$ film shows clean condition without contaminants, which could be adapted to capacitor production.

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A Study on Conductivity Characteristics of the Insulating Oil for X-ray Tube Housing (X선장치용(線裝置用) 절연유(絶緣油)의 도전특성(導電特性)에 관한 연구(硏究))

  • Kim, Young-Il;Lee, Duck-Chool;Chung, Yon-Tack
    • Journal of radiological science and technology
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    • v.9 no.1
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    • pp.73-81
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    • 1986
  • This paper carried out an experiment on the characteristics of time, temperature, electric field and the dependense of electrode materials and gap length by the conduction current of the insulating oil used for x-ray tube housing. The obtained results can be summarized as following: 1. In the x-ray tube housing insulating oil with vacuum condition, conduction current is declined more than the x-ray tube housing insultaing oil with the air, and is held stable states. 2. At the low electric field the higher temperature of the x-ray tube housing insulating oil is increased, the more conduction current. 3. The dependence of electrode material is appeared at the low electric field and the short gap length than the high and the long with Fe> Cu >Al. 4. At the I-E characteristics, the low electric field than 1000 [V/cm] is appeared Ohm's law region, and the high become saturation region. 5. At the same electric field, the longer gap length become, the more conduction current is increased, and the same applied voltage, the longer, the less conduction current is decreased, the less low than high temperature x-ray tube housing insulating oil.

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Evaluation of Dewatering of Cellulose Nanofibrils Suspension and Effect of Cationic Polyelectrolyte Addition on Dewatering (셀룰로오스 나노피브릴 현탁액의 탈수성 평가 및 양이온성 고분자전해질 투입의 영향)

  • Ryu, Jaeho Ryu;Sim, Kyujeong;Youn, Hye Jung
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.46 no.6
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    • pp.78-86
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    • 2014
  • Since cellulose nanofibrils (CNF) has large specific surface area and high water holding capacity, it is very difficult task to remove water from the CNF suspension. However, dewatering of CNF suspension is a prerequisite of following processes such as mat forming and drying for the application of CNF. In this study, we evaluated the drainage of cellulose fibers suspension under vacuum and pressure conditions depending on the number of grinding passes. Also, the effect of the addition of cationic polyelectrolyte on dewatering ability of CNF suspension was investigated. Regardless of dewatering condition, the total drained water amount as well as the drainage rate were decreased with an increase in the number of grinding passes. Pressure dewatering equipment enables us to prepare wet CNF mat with relatively higher grammage. The cationic polyelectrolytes improved the dewatering ability of CNF suspension by controlling the zeta potential of CNF. The fast drainage was obtained when CNF suspension had around neutral zeta potential.

A Study on Densification Behvior of Austenitic Stainless Steel Powder Compacts Processed by Warm Compaction (온간 성형법으로 제작한 오스테나이트계 스테인레스강의 소결 거동에 관한 연구)

  • 임태환
    • Journal of Powder Materials
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    • v.7 no.1
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    • pp.42-49
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    • 2000
  • Densificationbehavior of conventional austenitic stainless steel powder compacts was studied by comparing the relative density of sintered compact(Ds)with that of green compacts(Dg)prepared with various catbon contents and P/M process. Dg of 304and 316 powders by warm compaction under pressure of 686 MPa at heating temperature of powder(553K) and dies (573K) were 80% and 81%, repectively, whichwere 2 and 3% higher than those of conventional green compacts at the same pressure. Ds of 304 compacts sintered at 1373K in H2 gas has the same value of 84% max. regardless of compacting temperature, and Ds of 316 compacts at the same sintering conditions were 80% by conventional compaction and 83% by warm compaction. Oxygen contents of 304 and 316 sintered compacts were increased 1.43∼2.94% and 0.010∼0.921% higher than those of raw powders and warm green compacts, respectively. In other case, Ds of 316 compacts sintered at 1573K in vacuum had the same value of 86%max. And Ds of 316 compacts at the same sintering conditions were 83% and 86% by conventional and warm compaction, respectively. Oxygen contents of 304 sintered compacts were 0.321% and 0.360%, and in case of 316, they were 0.419% and 0.182% by the respective compating condition. With carbon additions in the range 0.1∼0.6% Ds increased to the extent of 86∼89% in 304 sintered compacts, and to 82∼84% and 85∼87% in 316 according to different two compacting peocesses compared to those of sintered compacts without carbon addition.

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Suppression of Interfacial Segregation and Control of Microstructure for Improvement of Mechanical Properties of W-Ni-Fe Heavy Alloy (계면편석 억제와 미세구조 조절에 의한 중합금의 기계적성질 향상)

  • 강석중
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 1993.11a
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    • pp.3-3
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    • 1993
  • In mechanical testing of W-Ni-Pe heavy alloys, the cracks nucleate at W/W interface and propagate through W/ Imatrix interface or through matrix phase together with the cleavage of W grains. The mechanical properties can therefore be improved by control of the interfacial strength and area. In this presentation, some experimental result and techniques on this subject will be reviewed and discussed. The hydrogen embrittlement caused by the hydrogen segregation at interfaces during sintering in an hydrogen atmosphere can be removed by an heat-treattnent in vacuum or in an inert atmosphere. The heat-treatment condition can be estimated by using a diffusion equation for a cylindrical shape. The mechanical properties, in particular the impact property, are degraded by the segregation of non-metallic impurities, such as Sand P. The degradation can be prevented by adding a fourth element, such as La or Ca, active with the non-metallic impurities. The cyclic heat-treatment at usual heat-treattnent tempemture causes the penetration of matrix between W/W grain boundaries and results in remarkable increase in impact energy. This is due to an increase in the area of ductile failure during the impact test. The instability of W/matrix interface casued by addition of Mo or Re can be controlled by using W powders of different size. The increase in the interfacial area in found to be related to the presence of non-equilibrium pure W gmins among W(Mo or Re) solid solution gmins.

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The Improved Artificial Trap Baits (통발용 인공미끼의 개발)

  • 염말구
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.34 no.2
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    • pp.185-190
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    • 1998
  • The aim of this study was to develop the artificial trap baits being able to replace the natural anchovy or sardine baits. The fishing trials for evaluating the fishing efficiencies of the artificial baits were conducted with commercial traps at coastal areas near Tongyoung, southern Korea. The preferable artificial baits which were made of minced anchovy, sardine, mackerel, or fish surplus products mixed with wheat flour into dry or wet pelleted or crumbled types, were showed some merits as the following. \circled1 Fishing efficiencies of the artificial baits were same or little higher level than that of the natural bait anchovy; \circled2 bait cost were same or little lower level; \circled3 dry artificial baits stocked in the room condition showed good fishing efficiencies; \circled4 making of artificial baits were very simple; \circled5 there were no harm to the fish and little pollution to the environment; \circled6 the releasing rate of attractants in the artificial or natural bait showed similar patterns. The artificial baits using the fish by-products which were vacuum freeze-drying extract of boiled anchovy or tunas extract, showed lower catches in the conger eel, Coner miriaster, but similar catches in the crabs, mainly Charybdis japonica, to the those of natural anchovy bait.

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The Effects of MgO Activation Process on the Discharge Characteristics of AC PDP (AC PDP 의 방전 특성에 미치는 MgO 활성화 영향에 관한 연구)

  • Kim, Young-Kee;Kim, Jun-Ho;Sohn, Je-Bong;Park, Byeong-Eon;Park, Myung-Joo;Cho, Jung-Soo;Park, Chung-Hoo
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.48 no.3
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    • pp.209-214
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    • 1999
  • This paper deals with the effects of activation process of MgO thin film on the dielectric characteristics of surface discharge type AC PDP. The discharge voltage decreased with increase in the MgO activation time and temperature until $400^{\circ}C$ under the condition of clean high vacuum. However, for the sample activated above $430^{\circ}C$ the discharge voltage increased. These results may be explained by the MgO morphology change and surface cleaning in the process of activation.

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A study on the deposition of DLC thin films by using an FCVA technique (FCVA 방법에 의한 DLC 박막의 제작에 관한 연구)

  • Lee, Hae-Seung;Uhm, Hyun-Seok;Kim, Jong-Kuk;Choi, Byoung-Ryong;Park, Jin-Seok
    • Proceedings of the KIEE Conference
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    • 1997.07d
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    • pp.1379-1382
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    • 1997
  • Diamond-like carbon(DLC) thin films are produced by using a filtered cathodic vacuum arc(FCVA) deposition system. Different magnetic components, namely steering, focusing, and filtering plasma-optic systems, are used to achieve a stable arc plasma and to prevent the macroparticles from incorporating into the deposited films. Effects of magnetic fields on plasma behavior and film deposition are examined. The carbon ion energy is found to be varied by applying a negative (accelerating) substrate bias voltage. The deposition rate of DLC films is dependent upon magnetic field as well as substrate bias voltage and at a nominal deposition condition is about $2{\AA}/s$. The structural properties of DLC films, such as internal stress, relative fraction of tetrahedral($sp^3$) bonds, and surface roughness have also been characterized as a function of substrate bias voltages and partial gas($N_2$) pressures.

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