• Title/Summary/Keyword: Vacuum Press

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Energy absorption of foam-filled lattice composite cylinders under lateral compressive loading

  • Chen, Jiye;Zhuang, Yong;Fang, Hai;Liu, Weiqing;Zhu, Lu;Fan, Ziyan
    • Steel and Composite Structures
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    • v.31 no.2
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    • pp.133-148
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    • 2019
  • This paper reports on the energy absorption characteristics of a lattice-web reinforced composite sandwich cylinder (LRCSC) which is composed of glass fiber reinforced polymer (GFRP) face sheets, GFRP lattice webs, polyurethane (PU) foam and ceramsite filler. Quasi-static compression experiments on the LRCSC manufactured by a vacuum assisted resin infusion process (VARIP) were performed to demonstrate the feasibility of the proposed cylinders. Compared with the cylinders without lattice webs, a maximum increase in the ultimate elastic load of the lattice-web reinforced cylinders of approximately 928% can be obtained. Moreover, due to the use of ceramsite filler, the energy absorption was increased by 662%. Several numerical simulations using ANSYS/LS-DYNA were conducted to parametrically investigate the effects of the number of longitudinal lattice webs, the number of transverse lattice webs, and the thickness of the transverse lattice web and GFRP face sheet. The effectiveness and feasibility of the numerical model were verified by a series of experimental results. The numerical results demonstrated that a larger number of thicker transverse lattice webs can significantly enhance the ultimate elastic load and initial stiffness. Moreover, the ultimate elastic load and initial stiffness were hardly affected by the number of longitudinal lattice webs.

Quality Characteristics of Press Ham Containing Conjugated Linoleic Acid-Triglyceride (Conjugated linoleic acid-triglyceride가 함유된 프레스햄 품질특성)

  • Lee, Jeong-Ill;Joo, Y.K.;Kang, G.H.;Yang, H.S.;Jeong, J.Y.;Joo, S.T.;Park, G.B.
    • Journal of Animal Science and Technology
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    • v.49 no.1
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    • pp.109-120
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    • 2007
  • CLA was chemically synthesized by alkaline isomerization method using corn oil. CLA-TG was synthesized by chemical reaction using sodium methoxide. For the control, 10% of back fat among the total component was only added without the annex of CLA-TG. For the first treatment, 5% of CLA-TG among the lard component added into the press ham was replaced. For the 2nd, 3rd and 4rd treatments, 10%, 15% and 20% of CLA-TG was respectively replaced. Manufacture press ham using CLA-TG were vacuum packaged and then stored during 1, 7, 14, 21 and 28 days at 4℃. Samples were analyzed for shear force value, sensory evaluation, TBARS, fatty acid composition and CLA content. Shear force value of control was significantly higher than that of CLA-TG treatment groups(P<0.05). All treatments were increased by the passage of storage time. No remarkable differences were found in sensory properties among control and CLA-TG treatment groups. CLA-TG treatment groups showed significantly(P<0.05) lower TBARS value than the control. TBARS value was increased significantly during storage in all treatment. In the change of fatty acid composition, the contents of C14:0~C20:4 were decreased significantly by CLA-TG additive. Whereas the increase level of CLA-TG additive resulted in the significantly higher unsaturated fatty acid and CLA content. Summing up the a forementioned results, press ham manufacturing with CLA-TG additive was not affected in sensory evaluation. Also, it may be assumed that the high quality press ham can be manufactured with the extent of storage period and CLA accumulation.

Changes of Quality Characteristics of Manufactured Press Ham using Conjugated Linoleic Acid(CLA) Accumulated Pork during Storage Periods (CLA가 축적된 돈육으로 제조된 Press Ham의 저장기간중 품질변화)

  • Lee, J.I.;Ha, Y.J.;Jung, J.D.;Kang, K.H.;Hur, S.J.;Park, G.B.;Lee, J.D.;Do, C.H.
    • Journal of Animal Science and Technology
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    • v.46 no.4
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    • pp.645-658
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    • 2004
  • To investigate the effects of conjugated linoleic acid added diet feeding on CLA accumulation and quality characteristics of manufactured press ham using CLA accwnulated pork loin meat. The CLA used to add in diet was chemically synthesized by alkaline isomerization method with com oil. Pigs were divided into 5 treatment groups(4 pigs/group) and subjected to one of five treatment diets(0, 1.25% CLA for 2weeks, 2.5% CLA for 2weeks, 1.25% CLA for 4weeks and 2.5% CLA for 4weeks, CLA diets; total fed diets) before slaughter. Pork loin were collected from the animals(110kg body weight) slaughtering at the commercial slaughter house. Manufacture press ham using CLA accumulated pork loin meat were vacuum packaged and then stored during 1, 7, 14, 21 and 28 days at 4$^{\circ}C$. Samples were analyzed for general compositions, physico-chemical properties(pH, color, shear force value), TBARS. pH value of CLA treatment(T4) was increased significantly than that of oontrol(P<0.05). pH of control and CLA treatments were increased significantly as the storage period passed(P< 0.05). Crude fat content of CLA treatment groups was significantly higher than the control pork (P<0.05). Meat color(CIE $L^*$, $a^*$$b^*$

A Study on the Performance Improvement of ta-C Thin Films Coating on Tungsten Carbide(WC) Surface for Aspherical Glass Lens by FCVA Method Compared with Ir-Re coating (Ir-RE 코팅 대비 자장여과필터방식을 이용한 비구면 유리 렌즈용 초경합금(WC)표면의 ta-C 박막 코팅 성능 개선 연구)

  • Jung, Kyung-Seo;Kim, Seung-Hee
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.20 no.12
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    • pp.27-36
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    • 2019
  • The demand for a low dispersion lens with a small refractive index and a high refractive index is increasing, and accordingly, there is an increasing need for a releasable protective film with high heat resistance and abrasion resistance. On the other hand, the optical industry has not yet established a clear standard for the manufacturing process and quality standards for mold-releasing protective films used in aspheric glass lens molding. Optical lens manufacturers treat this technology as proprietary information. In this study, an experiment was conducted regarding the optimization of ion etching, magnetron, and arc current at each source and filter part, and bias voltage in FCVA (filtered cathode vacuum arc)-based Ta-C thin film coatings. This study found that compared to iridium-rhenium alloy thin film sputtering products, the coating conditions were improved by approximately 50%, 20%, and 40% in terms of thickness, hardness, and adhesive strength of the film, respectively. The thin-film coating process proposed in this study is expected to contribute significantly to the development and utilization of glass lenses, which will help enhance the minimum mechanical properties and quality of the mold-release thin film layer required for glass mold surface forming technology.

Effects of Conjugated Linoleic Acid Accumulated Pork on Fatty Acid Composition and Quality Characteristics of Press Ham (CLA가 축적된 돈육으로 제조된 Press Ham의 지방산 조성 및 품질 특성에 미치는 영향)

  • 이정일;양한술;정진연;이진우;이제룡;주선태;도창희
    • Food Science of Animal Resources
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    • v.24 no.2
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    • pp.135-145
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    • 2004
  • The CLA used to add in diet was chemically synthesized by alkaline isomerization method with corn oil. Pigs were divided into 5 treatment groups (4 pigs/group) and subjected to one of five treatment diets (0, 1.25% CLA for 2weeks, 2.5% CLA for 2weeks, 1.25% CLA for 4weeks and 2.5% CLA for 4weeks, CLA diets; total fed diets) before slaughter. Pork loin were collected from the animals (110kg body weight) slaughtering at the commercial slaughter house. Manufacture press ham using CLA accumulated pork loin were vacuum packaged and then stored during 1, 7, 14, 21 and 28 days at 4$^{\circ}C$. Samples were analyzed for texture characteristics, sensory evaluation, fatty acid composition and CLA content. There was no significant difference in texture among control and CLA treatment groups. It was not clearly changed by storage time. No remarkable differences were found in sensory properties (color, flavor, texture and acceptability) between control and CLA treatment groups. It was not clearly changed by the passage of storage time. In the change of fatty acid composition, the contents of oleic, linoleic and arachidonic were decreased by dietary CLA-supplementation, whereas the increase level of CLA-supplementation resulted in the higher palmitic and stearic acid than control. As dietary CLA was increased in feed, the content of CLA in pork was increased.

Fabrication of Fe-Cr-Al Porous Metal with Sintering Temperature and Times (소결 온도와 유지 시간에 따른 Fe-Cr-Al 다공성 금속의 제조)

  • Koo, Bon-Uk;Lee, Su-In;Park, Dahee;Yun, Jung-Yeul;Kim, Byoung-Kee
    • Journal of Powder Materials
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    • v.22 no.2
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    • pp.100-104
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    • 2015
  • The porous metals are known as relatively excellent characteristic such as large surface area, light, lower heat capacity, high toughness and permeability. The Fe-Cr-Al alloys have high corrosion resistance, heat resistance and chemical stability for high temperature applications. And then many researches are developed the Fe-Cr-Al porous metals for exhaust gas filter, hydrogen reformer catalyst support and chemical filter. In this study, the Fe-Cr-Al porous metals are developed with Fe-22Cr-6Al(wt) powder using powder compaction method. The mean size of Fe-22Cr-6Al(wt) powders is about $42.69{\mu}m$. In order to control pore size and porosity, Fe-Cr-Al powders are sintered at $1200{\sim}1450^{\circ}C$ and different sintering maintenance as 1~4 hours. The powders are pressed on disk shapes of 3 mm thickness using uniaxial press machine and sintered in high vacuum condition. The pore properties are evaluated using capillary flow porometer. As sintering temperature increased, relative density is increased from 73% to 96% and porosity, pore size are decreased from 27 to 3.3%, from 3.1 to $1.8{\mu}m$ respectively. When the sintering time is increased, the relative density is also increased from 76.5% to 84.7% and porosity, pore size are decreased from 23.5% to 15.3%, from 2.7 to $2.08{\mu}m$ respectively.

Cold Isostatic Pressing and Sintering Behavior of (Al +12.5%Cu)3Zr Nanocrystalline Intermetallic Compound Synthesized by Mechanical Alloying (기계적합금화한 (Al +12.5%Cu)3Zr 초미립 금속간화합물의 CIP 성형 및 소결 거동)

  • Moon, H.G.;Hong, K.T.;Kim, S.J.
    • Korean Journal of Materials Research
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    • v.12 no.8
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    • pp.634-640
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    • 2002
  • To improve the ductility of mTEX>$(Al +12.5%Cu)<_3$Zr intermetallics, which are the potential high temperature structural materials, the mechanical alloying behavior, the effect of pressure and temperature on the $Ll_2$, phase formation and the behavior of the cold isostatic press and sintering were investigated. However mechanically alloyed A1$_3$Zr alloy have been known to have high mechanical strength even at high temperature, its workability was poor. A method of solution is refined grain size and phase transformation from $DO_{23}$ to $Ll_2$.$ Ll_2$ structure TEX>$(Al+12.5%Cu)<_3$Zr with nanocrystalline microstructure intermetallic powders where were prepared by mechanical alloying of elemental powders. Grain sizes of the as milled powders were less than 10nm (from transmission electron microscopy, TEM). Thermal analyses showed that $Ll_2$ structure was stable up to$ 800^{\circ}C$ for 1hour $(Al+ 12.5%Cu)<_3$Zr. $(Al+12.5%Cu)<_3$Zr has been consolidated by cold isostatic pressing (CIP 138, 207, 276, 414MPa) at room temperature and subsequent heat treatment at high temperatures where $Ll_2$ structure was stable under vacuum atmosphere. The results showed that 94.2% density of Ll$_2$ compacts was obtained for the (Al +12.5%Cu)$_3$Zr by sintering at 80$0^{\circ}C$ for 1hour (under CIPed 207MPa). This compact of the grain size was 40nm.

The use of HRSEM to characterize new and aged membranes in drinking water production

  • Wyart, Y.;Nitsche, S.;Chaudanson, D.;Glucina, K.;Moulin, P.
    • Membrane and Water Treatment
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    • v.2 no.4
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    • pp.251-266
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    • 2011
  • This work deals with the use of High Resolution Scanning Electron Microscopy (HRSEM) to verify ultrafiltration membrane selectivity at the end of the production line as well as membrane ageing. The first part of this work is focused on new membranes. It is shown that it is better to use sputtering metallization than vacuum deposition, as this latter technique entails thermal damage to the skin layer. Moreover, the impact of the metallization layer on the determination of the membrane pore size is studied and it is observed that no impact of the metallization step can be clearly defined for a metallization layer ranging from 3 to 12 nm. For example, an average pore size of 16.9 nm and a recovery rate of 6.5 % are observed for a 150 kDa cellulose acetate membrane. These results are in agreement with those given by the manufacturer: pore size ranging from 10 to 15 nm and recovery rate ranging from 5 to 10 %. The second part of this work focuses on the study of membrane ageing. A PVDF hollow fibre membrane is studied. It is shown that a 65 % decrease in the permeate flux can be linked to a decrease in the number of pores at the surface of the membrane and a decrease in the recovery rate. In conclusion, a mapping of the pores is performed for several new hollow fibre membranes used to produce drinking water, made of different materials, with different geometries and molecular weight cut-off. These results provide reference data that will help better understand the phenomena of membrane fouling and membrane ageing.

Synthesis and Properties of In-situ $MoSi_2$/W Composites ($MoSi_2$/W 복합재료의 합성과 성질에 관한 연구)

  • Jang, Dae-Kyu;Abbaschian, R.
    • Korean Journal of Materials Research
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    • v.8 no.10
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    • pp.938-944
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    • 1998
  • $MoSi_2$/W composites were fabricated by vacuum hot press at $1600^{\circ}C$ under 30MPa for 3 hrs. The effects of the amount of tungsten in the composites was explained in terms of the microstructure and mechanical properties. Although tungsten was mainly substituted to Mo atoms forming a complete solid solution of (Mo.W).Si, (x= 1, 5, y=2, 3). the grain size of composites became smaller with the increase of tungsten added. Vickers hardness was increased with the increase of tungsten content due to the solid-solution hardening. On the other hand, toughness of composites decreased sharply by increasing the amount of tungsten. Optimum tungsten amount was determined to be a 10 vol% of composite. Indentation fracture toughness was calculated to be 4.5MPa\sqrt{m}$ in this composites, compared with $2.7MPa\sqrt{m}$ in pure $MoSi_2$.

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Fabrication and Mechanical Properties of $MoSi_2$ Based Composites ($MoSi_2$ 복합재료의 제조 및 기계적 특성)

  • Park, Yi-Hyun;Lee, Sang-Pill;Lee, Sung-Eun;Jin, Joon-Ok;Kim, Sa-Woong;Lee, Jin-Kyung;Yoon, Han-Ki
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2003.05a
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    • pp.289-293
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    • 2003
  • This study dealt with the characterization of $MoSi_2$ based composites containing three types of additive materials such as SiC, $NbSi_2\;and\;ZrO_2$ particles have been investigated, based on the detailed examination of their microstructures and fracture surfaces. The effects of reinforcing materials on the high temperature strength of $MoSi_2$ based composites have been also examined. $MoSi_2$ based composites were fabricated by the hot press process under the vacuum atmosphere. The volume fraction of reinforcing materials in the composite system was fixed as 20 %. The microstructures and the mechanical properties of $MoSi_2$ based composites were investigated by means of SEM, EDS, XRD and three point bending test.

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