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조성변화에 따른 티타늄 화합물 박막의 색상 변화

  • 이영민;장승현;양지훈;정재인
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2009년도 제38회 동계학술대회 초록집
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    • pp.266-266
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    • 2010
  • 마그네트론 스퍼터링을 이용하여 질소와 탄소를 함유한 티타늄 화합물을 합성하고, 조성 변화에 따른 색상 변화를 통해 티타늄 화합물로 구현할 수 있는 색상에 대해서 알아보았다. 스퍼터 타겟은 4"X1/4" 크기의 고순도(99.99%) 티타늄을 사용하였다. 시편은 알코올과 아세톤에서 각각 5분간 초음파 세척된 SUS304를 사용하여, 진공용기에 시편을 장착하고 압력을 $3{\times}10^{-6}\;Torr$까지 배기한 후, Ar 가스를 주입하여 진공도가 $2{\times}10^{-2}\;Torr$에 이르면 펄스 전원 공급 장치를 이용하여 800 V의 전압으로 1시간 동안 글로우 방전을 시켜 시편 청정을 실시하였다. 시편 청정이 끝나면 다시 $3{\times}10^{-6}\;Torr$까지 진공배기를 실시하고, Ar 가스를 진공용기 내로 공급하여 $1{\sim}3{\times}10^{-3}\;Torr$에서 스퍼터링을 실시하여 완충층으로 티타늄 박막을 코팅하였다. 티타늄 화합물은 티타늄을 스퍼터링 하면서 진공용기 내에 질소와 메탄가스를 적절한 비율로 공급함으로써 코팅하였다. 박막 증착 시 시편 온도는 $200^{\circ}C$, 타겟과의 거리는 12 cm를 유지하였으며, 시편을 회전시켜 코팅하였다. 티타늄 화합물의 두께와 미세구조, 조성 그리고 색상은 투과전자현미경(transmission electron microscope, TEM), 글로우 방전 분광기(glow discharge light spectroscope, GDLS), 및 색차계(spectrophotometer)를 사용하여 각각 분석하였다. TEM 분석결과 TiN의 박막 두께는 약 300 nm로 공극이 존재하지 않는 치밀한 다결정 구조를 나타내었고, TiCN은 약 600 nm로 TiN과 두 배의 두께 차이를 보였다. 이는 탄소의 공급원인 메탄가스의 주입으로 증착률이 증가한 것으로 판단된다. 또한 소량의 질소와 메탄가스의 유량 조절로 화합물의 조성을 변화시킬 수 있었으며, 이러한 조성 변화는 화합물의 색상변화로 나타났다. 따라서 본 연구에서 얻어진 결과를 외관 코팅 분야에 응용한다면 다양한 색상 구현과 외관의 경도, 내마모성, 내식성의 향상 등 많은 장점을 가질 것으로 판단된다.

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위성 SAR용 광대역 이중편파 적층형 패치 배열 안테나 설계 및 제작 (Design and Fabrication of A Wide-Band Dual-Polarization Stacked Patch Array Antenna for Satellite SAR Applications)

  • 이재민;유제우;채희덕;이유리;정화영;김종필;박종국
    • 한국ITS학회 논문지
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    • 제20권2호
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    • pp.72-78
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    • 2021
  • 본 논문에서는 위성 SAR 시스템에 적용하기 위한 광대역 이중편파 적층형 패치 안테나를 설계하고 제작 결과를 제시하였다. 위성 SAR 분야에 주로 적용되는 X-대역에서 위성 SAR 시스템의 영상 품질 향상을 위해 손실 최소화, 광대역 동작 그리고 능동위상배열안테나에 적용이 가능하도록 능동반사손실 최소화 관점에서 안테나를 설계하였다. 제작된 안테나의 대역폭은 능동반사손실 -10 dB 이하 기준에서, 수직/수평 편파 각각 19.26%/19.79% 이며, 손실은 주파수 평균으로 수직/수평 편파 각각 0.797 dB/0.799 dB 로 확인되었다. 또한, 근접전계시험으로 안테나의 빔 패턴을 확인하다. 그 결과, 배열이론을 바탕으로 계산된 이상적 패턴과 비교하여, 측정된 패턴 및 지향성이 매우 유사함을 확인하였다.

오르막 퍼팅 동작 시 볼의 위치가 퍼터와 볼의 움직임에 미치는 영향 (Ball movements in various surface angles of uphill putting based on different ball positions)

  • 류종욱;김재정
    • 한국응용과학기술학회지
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    • 제36권2호
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    • pp.448-455
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    • 2019
  • 본 연구는 오르막 퍼팅 시 좌, 우 경사에 따른 볼의 움직임이 어떻게 변화되는지에 대해 알아보는 것을 목적으로 한다. 본 연구를 위해 한국프로골프협회에서 15년 이상의 골프경기 경험이 있는 피험자들이 참여하였고, 본인들의 퍼터를 이용하여 실제 그린과 유사한 환경에서 퍼팅 동작을 수행하였다. 비디오 카메라를 이용하여 피험자들의 오르막 그린 경사에 따른 퍼팅 동작을 수집 후 동작분석을 실시하였으며, 통계적 유의수준을 a=.05로 설정하였다. 연구결과로 좌, 우 경사별 오르막 퍼팅에서 볼의 위치가 왼쪽에서 오른쪽으로 위치 할 때 볼 움직임의 속도와 각속도가 증가하는 것이 확인되었으며, 여러 경사도 중 성공률을 높여야 하는 오르막 퍼팅에서 경사에 따른 어드레스 볼 위치를 변화할 때, 임팩트 시 클럽 페이스와 볼 움직임이 어떻게 변화하는지를 검증하고, 현장적용 측면에 도움을 주는 과학적 자료를 제시하고자 본 연구를 진행하였다.

An Integrated System for Radioluminescence, Thermoluminescence and Optically Stimulated Luminescence Measurements

  • Park, Chang-Young;Park, Young-Kook;Chung, Ki-Soo;Lee, Jong-Duk;Lee, Jungil;Kim, Jang-Lyul
    • Journal of Radiation Protection and Research
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    • 제43권4호
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    • pp.160-169
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    • 2018
  • Background: This study aims to develop an integrated optical system that can simultaneously or selectively measure the signals obtained from radioluminescence (RL), thermoluminescence (TL), and optically stimulated luminescence (OSL), which are luminescence phenomena of materials stimulated by radioactivity, heat, and light, respectively. The luminescence mechanism of various materials could be investigated using the glow curves of the luminescence materials. Materials and Methods: RL/TL/OSL integrated measuring system was equipped with a X-ray tube (50 kV, $200{\mu}A$) as an ionizing radiation source to irradiate the sample. The sample substrate was used as a heating source and was also designed to optically stimulate the sample material using various light sources, such as high luminous blue light emitting diode (LED) or laser. The system measured the luminescence intensity versus the amount of irradiation/stimulation on the sample for the purpose of measuring RL, TL and OSL sequentially or by selectively combining them. Optical filters were combined to minimize the interference of the stimulation light in the OSL signal. A long-pass filter (420 nm) was used for 470 nm LED, an ultraviolet-pass filter (260-390 nm) was used for detecting the luminescence of the sample by PM tube. Results and Discussion: The reliability of the system was evaluated using the RL/OSL characteristics of $Al_2O_3:C$ and the RL/TL characteristics of LiF:Mg,Cu,Si, which were used as dosimetry materials. The RL/OSL characteristics of $Al_2O_3:C$ showed relatively linear dose-response characteristics. The glow curve of LiF:Mg,Cu,Si also showed typical RL/OSL characteristics. Conclusion: The reliability of the proposed system was verified by sequentially measuring the RL characteristics of radiation as well as the TL and OSL characteristics by concurrent thermal and optical stimulations. In this study, we developed an integrated measurement system that measures the glow curves of RL/TL/OSL using universal USB-DAQs and the control program.

Crystal Structure and Magnetic Properties of Sodium-Iron Phosphates NaFe0.9Mn0.1PO4 Cathode Material

  • Seo, Jae Yeon;Choi, Hyunkyung;Kim, Chul Sung;Lee, Young Bae
    • Journal of the Korean Physical Society
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    • 제73권12호
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    • pp.1863-1866
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    • 2018
  • The sodium-iron phosphate maricite-$NaFe_{0.9}Mn_{0.1}PO_4$ was synthesized using the ball mill method. The crystal structure and magnetic properties of the prepared materials were studied using X-ray diffraction (XRD), vibrating sample magnetometer (VSM), and $M{\ddot{o}}ssbauer$ spectroscopy. Structural refinement of maricite-$NaFe_{0.9}Mn_{0.1}PO_4$ was analyzed using the FullProf program. From the XRD patterns, the crystal structure of maricite-$NaFe_{0.9}Mn_{0.1}PO_4$ was found to be orthorhombic with the space group Pmnb. The lattice parameters of maricite-$NaFe_{0.9}Mn_{0.1}PO_4$ are as follows: $a_0=6.866{\AA}$, $b_0=8.988{\AA}$, $c_0=5.047{\AA}$, and $V=311.544{\AA}^3$. Maricite-$NaFePO_4$ has an edge-sharing structure that consists of $FeO_6$ octahedral. Under an applied field of 100 Oe, the temperature dependences of zero-field-cooled (ZFC) and field-cooled (FC) curves were measured from 4.2 to 295 K. $M{\ddot{o}}ssbauer$ spectra were also recorded at various temperatures ranging from 4.2 to 295 K. We thus confirmed that the $N{\acute{e}}el$ temperature of $NaFe_{0.9}Mn_{0.1}PO_4$ ($T_N=14K$) was lower than that of maricite-$NaFePO_4$ ($T_N=15K$).

High-Performance Compton SPECT Using Both Photoelectric and Compton Scattering Events

  • Lee, Taewoong;Kim, Younghak;Lee, Wonho
    • Journal of the Korean Physical Society
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    • 제73권9호
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    • pp.1393-1398
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    • 2018
  • In conventional single-photon emission computed tomography (SPECT), only the photoelectric events in the detectors are used for image reconstruction. However, if the $^{131}I$ isotope, which emits high-energy radiations (364, 637, and 723 keV), is used in nuclear medicine, both photoelectric and Compton scattering events can be used for image reconstruction. The purpose of our work is to perform simulations for Compton SPECT by using the Geant4 application for tomographic emission (GATE). The performance of Compton SPECT is evaluated and compared with that of conventional SPECT. The Compton SPECT unit has an area of $12cm{\times}12cm$ with four gantry heads. Each head is composed of a 2-cm tungsten collimator and a $40{\times}40$ array of CdZnTe (CZT) crystals with a $3{\times}3mm^2$ area and a 6-mm thickness. Compton SPECT can use not only the photoelectric effect but also the Compton scattering effect for image reconstruction. The correct sequential order of the interactions used for image reconstruction is determined using the angular resolution measurement (ARM) method and the energies deposited in each detector. In all the results of simulations using spherical volume sources of various diameters, the reconstructed images of Compton SPECT show higher signal-to-noise ratios (SNRs) without degradation of the image resolution when compared to those of conventional SPECT because the effective count for image reconstruction is higher. For a Derenzo-like phantom, the reconstructed images for different modalities are compared by visual inspection and by using their projected histograms in the X-direction of the reconstructed images.

Initiation, proliferation, and improvement of a micropropagation system for mass clonal production of banana through shoot-tip culture

  • Khaskheli, Allah Jurio;Ali, Muharam;Shah, Syad Zakir Hussain;Memon, Zohra Fatima;Awan, Saleem;Khaskheli, Muhammad Ibrahim;Khaskheli, Mohsin Ali;Magsi, Bilqees;Qambrani, Zareen;Khaskheli, Asad Ali
    • Journal of Plant Biotechnology
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    • 제48권2호
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    • pp.86-92
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    • 2021
  • The present study aimed to evaluate the initiation, proliferation potential, and mass clonal production ability of a micropropagation system for banana through tissue culture. A total of 60 explants were cultured on basal media supplemented with various concentrations of BAP and NAA. Banana plants regenerated on MS basal medium (control) without the addition of BAP + NAA showed a significantly (P < 0.05) lower survival rate with no signs of shoots up to the end of the experimental period. The results further revealed that the performance in MSS-XI medium was almost 89%, followed by MSS-IX and MSS-X media, both of which showed performance up to 88%. In contrast, the performance in the MSS-XVI medium was less than 60%, at the less duration of time and highly shoot induction detected at MSS-XIII medium. The maximum number of shoots (4.9) was observed in the medium supplemented with growth adjuster MSS-XI, followed by the MSS-XII medium (4.5). Surprisingly, the best performance was observed for the MSR-VII medium approximately 16 days after initiation, while the lowest performance was observed with MSR-XI (approximately 31 days). The maximum rooting percentage (98%) was observed in the MSR-V to MSR-VIII media (98%), while the minimum rooting percentage was observed in MSR-XI (approximately 45%).

Hazelcast Vs. Ignite: Opportunities for Java Programmers

  • Maxim, Bartkov;Tetiana, Katkova;S., Kruglyk Vladyslav;G., Murtaziev Ernest;V., Kotova Olha
    • International Journal of Computer Science & Network Security
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    • 제22권2호
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    • pp.406-412
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    • 2022
  • Storing large amounts of data has always been a big problem from the beginning of computing history. Big Data has made huge advancements in improving business processes by finding the customers' needs using prediction models based on web and social media search. The main purpose of big data stream processing frameworks is to allow programmers to directly query the continuous stream without dealing with the lower-level mechanisms. In other words, programmers write the code to process streams using these runtime libraries (also called Stream Processing Engines). This is achieved by taking large volumes of data and analyzing them using Big Data frameworks. Streaming platforms are an emerging technology that deals with continuous streams of data. There are several streaming platforms of Big Data freely available on the Internet. However, selecting the most appropriate one is not easy for programmers. In this paper, we present a detailed description of two of the state-of-the-art and most popular streaming frameworks: Apache Ignite and Hazelcast. In addition, the performance of these frameworks is compared using selected attributes. Different types of databases are used in common to store the data. To process the data in real-time continuously, data streaming technologies are developed. With the development of today's large-scale distributed applications handling tons of data, these databases are not viable. Consequently, Big Data is introduced to store, process, and analyze data at a fast speed and also to deal with big users and data growth day by day.

Ag 중간층 두께에 따른 ZnO 박막의 광학적, 전기적 특성 연구 (Effect of Ag interlayer on the optical and electrical properties of ZnO thin films)

  • 김현진;장진규;최재욱;이연학;허성보;공영민;김대일
    • 한국표면공학회지
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    • 제55권2호
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    • pp.91-95
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    • 2022
  • ZnO single layer (60 nm thick) and ZnO with Ag interlayer (ZnO/Ag/ZnO; ZAZ) films were deposited on the glass substrates by using radio frequency (RF) and direct current (DC) magnetron sputter to evaluate the effectiveness of Ag interlayer on the optical visible transmittance and the conductivity of the films. In the ZAZ films, the thickness of ZnO layers was kept at 30 nm, while the Ag thickness was varied as 5, 10, 15 and 20 nm. In X-ray diffraction (XRD) analysis, ZnO films show the (002) diffraction peak and ZAZ films also show the weak ZnO (002) peak and Ag (111) diffraction peak. As a thickness of Ag interlayer increased to 20 nm, the grain size of the Ag films enlarged to 11.42 nm and the optical band gap also increased from 4.15 to 4.22 eV with carrier concentration increasing from 4.9 to 10.5×1021 cm-3. In figure of merit measurements, the ZAZ films with a 10 nm thick Ag interlayer showed the higher figure of merit of 4.0×10-3 Ω-1 than the ZnO single layer and another ZAZ films. From the experimental result, it is assumed that the Ag interlayer enhanced effectively the opto-electrical performance of the ZAZ films.

합성 방법에 따른 Li1.3Al0.3Ti1.7(PO4)3 소결체의 미세 구조 및 이온전도 특성 연구 (A Study on the Microstructures and Ionic Conductivity of Li1.3Al0.3Ti1.7(PO4)3 with Different Synthesis Routes)

  • 최슬기;최재원;양민호
    • 한국분말재료학회지
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    • 제30권2호
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    • pp.107-115
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    • 2023
  • Li1.3Al0.3Ti1.7(PO4)3(LATP) is considered a promising material for all-solid-state lithium batteries owing to its high moisture stability, wide potential window (~6 V), and relatively high ion conductivity (10-3-10-4 S/cm). Solid electrolytes based on LATP are manufactured via sintering, using LATP powder as the starting material. The properties of the starting materials depend on the synthesis conditions, which affect the microstructure and ionic conductivity of the solid electrolytes. In this study, we synthesize the LATP powder using sol-gel and co-precipitation methods and characterize the physical properties of powder, such as size, shape, and crystallinity. In addition, we have prepared a disc-shaped LATP solid electrolyte using LATP powder as the starting material. In addition, X-ray diffraction, scanning electron microscopy, and electrochemical impedance spectroscopic measurements are conducted to analyze the grain size, microstructures, and ion conduction properties. These results indicate that the synthesis conditions of the powder are a crucial factor in creating microstructures and affecting the conduction properties of lithium ions in solid electrolytes.