• Title/Summary/Keyword: Ultrasonic Scanning

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Study on the Controlled Gel Formation and Photochromic Properties of a New Cholesterol-bridge-naphthopyran Dyad

  • Sun, Lin;Wang, Guang;Liu, Longbo;Wang, Ai Xia
    • Bulletin of the Korean Chemical Society
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    • v.35 no.5
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    • pp.1343-1348
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    • 2014
  • A cholesterol-bridge-naphthopyran dyad (NP-MCB) was designed and synthesized. NP-MCB can readily self-assemble into gels under ultrasound-radiation in several organic solvents and the formed gels easily transfer to solution by heat. This reversible process can be repeated many times. Scanning Electron Microscopy results showed that the morphologies of all formed xerogels in different solvents have fibrillar microstructure. The gels formation was due to energy and pressure afforded by the ultrasonic process, resulting in formation of molecular hydrogen bonding and molecular aggregation. NP-MCB displayed the normal photochromism both in solution and gel states. The kinetic results confirm that the colored merocyanine in gels show a slower fading speed than that in solution due to the compact aggregation of NP-MCB molecules in gels. The xerogel film formed in polar gelling solvent had large surface wettability than that in nonpolar gelling solvent.

The Study on Microstructures and Mechanical Properties of Mild Steel Joined with Various Spot Welding Conditions (점용접 조건에 의한 연강의 미세조직 및 기계적특성에 관한 연구)

  • 강연철;김대영;김완기;김석원
    • Journal of Welding and Joining
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    • v.18 no.1
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    • pp.52-58
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    • 2000
  • Spot welding, namely a kind of electric resisting welding has been used widely in field of automobile and aircraft industries because of easiness to apply. Specimens used in this study was a mild steel of 1.2mm thickness and the electrode was a Cu-Cr alloy of 6mm diameter. The surface sheared of specimens after testing of tensile shear was observed by SEM(scanning electron microscope) after ultrasonic cleaning for 10min., and microstructures and grain size of all specimens were measured with using of O.M.(Optical microscope). By the means of measurement and observations of tensile shear load, fatigue strength and share surface, the weldability of spot welding was evaluated. When tensile shearing testing, fracture starting point in all specimens was took place at the bond between HAZ(Heat affected zone) and nugget. With increasing in number of layers, fatigue strength was decreased. With increasing in electric current, grain size in the HAZ became more fine.

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Behavior on the wear and friction of sealing composite for ship machinery (선박기계용 실링 복합재료의 마모 및 마찰거동)

  • LEE, Jung-Kyu;KOH, Sung Wi
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.53 no.2
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    • pp.204-209
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    • 2017
  • In order to use PUR/CuO Composites as the sealing materials for ships equipment, this research has been performed. PUR/CuO composites are produced by using ultrasonic waves. The increase of CuO leads to increase in the tensile strength and shore hardness. The cumulative wear volume shows a tendency to increase in proportional to sliding distance. As the CuO particles of these composites indicated, the friction coefficient was slightly increased. The major failure mechanisms were lapping layers, deformation of matrix, plowing, debonding of particles and microcracking by scanning electric microscopy photograph of the wear tested surface.

Study of Self Texturing on ZnO:Al TCO surface for Thin-Film Solar Cell (박막태양전지용 ZnO:Al 투명전도막 표면 Self-Texturing 연구)

  • Oh, Kyoung Suk;Yoon, Soon Gil;Lee, Jeong Chul
    • 한국신재생에너지학회:학술대회논문집
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    • 2011.05a
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    • pp.127.2-127.2
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    • 2011
  • 본 연구에서는 RF Magnetron Sputtering System을 이용하여 ZnO계 투명전도막 증착시 Vaporization된 MeOH를 유입함으로써 박막증착과 동시에 표면의 Roughness를 제어하여 이에따른 전기적 특성 및 광학적 특성의 개선에 대하여 연구하였다. 실험방법으로 기존의 RF Magnetron Sputtering System에 Vaporization이 가능한 Ultrasonic을 이용하여 MeOH를 Vaporized시켜 MFC Controll을 통해 챔버에 유입하여 ZnO계 투명전도막의 박막증착과 동시에 표면 Texturing을 하였다. ZnO계 투명전도막의 박막증착시 Vaporized MeOH의 유입에 따른 광학적 특성변화를 UV-visible-nIR spectrometry로 조사하였으며, 전기적 특성 변화를 4-Point-Probe로 조사하였으며, 표면적 특성 변화를 Atomic Force Microscope(AFM), Scanning Electron Microscopy(SEM)를 조사하였으며, 박막의 결정성장특성 변화를 X-ray Diffraction(XRD)으로 조사하였으며, Vaporized MeOH 유입에 따른 박막의 성분분석을 Secondary Ion Mass Spectrometry (SIMS)로 조사함으로써 최적의 조건 및 공정을 확립하였다.

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Obstacle Classification for Mobile Robot Traversability using 2-dimensional Laser Scanning (2차원 레이저 스캔을 이용한 로봇의 산악 주행 장애물 판단)

  • Kim, Min-Hee;Kwak, Kyung-Woon;Kim, Soo-Hyun
    • Journal of the Korea Institute of Military Science and Technology
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    • v.15 no.1
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    • pp.1-8
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    • 2012
  • Obstacle detection is much studied by using sensors such as laser, vision, radar and ultrasonic in path planning for UGV(Unmanned Ground Vehicle), but not much reported about its characterization. In this paper not only an obstacle classification method using 2-dimensional LMS(Laser Measurement System) but also a decision making method whether to avoid or traverse the obstacle is proposed. The basic idea of decision making is to classify the characteristics by 2D laser scanned data and intensity data. Roughness features are obtained by range data using a simple linear regression model. The standard deviations of roughness and intensity data are used as measures for decision making by comparing with those of reference data. The obstacle classification and decision making for the UGV can facilitate a short path to the target position and the survivability of the robot.

The Etched Surface of the Repeatedly Cast Dental Base Metal Alloy (반복 사용된 치과용 비귀금속에 의한 주조체의 식각표면에 대한 연구)

  • Lee, Sun-Hyung
    • The Journal of the Korean dental association
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    • v.23 no.7 s.194
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    • pp.577-583
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    • 1985
  • The purpose of this investigation was to evaluate scanning electron micrographs of repeatedly cast base metal alloy. For this study two Ni-Cr-Be alloys were used; Rexillium III and Verabond. They were repeatedly cast without addition o new alloy melting with an electric resistant furnace (Castron 8, Yoshida dental equipment Mfg.Co.). They were etched with 10% H₂SO₄ Sol. at 300mA/㎠ for 3 minutes with the use of metal etching unit Oxyetch (OXY dental product Inc.), and ultrasonic cleaning in 18% HC1 Sol. was done. Etched surfaces were examined under a SEM at x 200 and x 750. The surfaces are shown in legends.

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Characteristics of Ultrasonic Transducers using Planar Scanning Technique (평면 주사법을 이웅한 초음파 변환기의 특성 조사)

  • Jho Moon Jae;Kim Yong Tae;Eun Hee Joon
    • Proceedings of the Acoustical Society of Korea Conference
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    • spring
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    • pp.167-170
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    • 1999
  • 초음파 변환기의 음향 특성 평가항목으로는 주파수에 따른 출력특성, 입력 전압에 대한 출력의 선형성(방사컨덕턴스), 방사음장의 지향성 및 대칭성 등을 들 수 있다. 평면 주사기법은 교정된 하이드로폰을 이용하여, 초음파 변환기에서 방사된 음파가 형성하는 음장의 분포를 측정하는 기법이다. 본 연구에서는 이들을 측정할 수 있는 장치로 DC servo모터를 장착한 3 축 이송 장치와 가로 400 mm, 세로 800 mm, 높이 400 m를 갖는 수조를 제작하고 제어프로그램을 개발하여 상온의 증류수에 형성된 초음파 음장의 공간 분포를 실험하여, 이론적 예측값과 비교하였다.

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Planar Scanning Simulation Technique for Prediction of the Field Distribution Radiated From Ultrasonic Transducers (초음파 변환기의 음장 분포 예측을 위한 평면 주사 모의실험)

  • Kim Yong Tae;Jho Moon Jae;Eun Hee Joon
    • Proceedings of the Acoustical Society of Korea Conference
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    • spring
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    • pp.175-178
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    • 1999
  • 원형단면을 갖는 수신용 하이드로폰과 같은 면적의 정사각형 단면을 가정하여, 상온의 증류수를 매질로 초음파 변환기에서 방사되는 음장의 공간적 분포를 모의실험하였다. 이러한 "정사각형 평면 근사 평균법(이후 평면 근사 평균법)"을 이용하여, x-축 주사, z-축 주사, xy-평면 주사 및 xz-평면 주사를 모의실험하여 실제 실험에서 나타날 수 있는 여러 가지 현상을 조사하였다. z-축 주사 모의 실험 결과는 Beissner의 이론과 비교하여 비교적 잘 일치하였다

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초음파 현미경 및 AE에 의한 결함 측정

  • 최만용;박익근;한응교
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1991.04a
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    • pp.127-133
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    • 1991
  • Acoustic microscopy has attracted much intrest recently as potential mondestructive evalution technique for detecting and sizing defects of surface and sub-surface. Also acoustic emission testing method has been developed for detecting microcracks which is more than 30 umm in length quintitatively on ceramics material. In the present paper, acoustic emission during the four point bending test in hot-pressed sintered Si$\_$3/N$\_$4/ specimen which was stressed bythermal shock has been measured by high sensitive sensing system. The surface and sub-surface cracks were detected by scanning acoustic microscope of 800 MHz and conventional ultrasonic testing in C-scope image. The purpose was to investigate the location and size of cracks by SAM and AE technique, whose experimental datas demontrates good agreement for detecting microcracks.

High Frequency Ultrasound and Its Applications to Animal and Human Imaging Focusing on Vessel and Blood (고주파 초음파의 그 응용: 혈관과 혈액을 중심으로한 동물과 인체 영상)

  • Bok, Tae-Hoon;Paeng, Dong-Guk
    • The Journal of the Acoustical Society of Korea
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    • v.29 no.2E
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    • pp.73-85
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    • 2010
  • In the diagnostic ultrasound (US) transducer technology, the high frequency US(HFUS) transducer over 20 MHz is one of the current issues to be pursued for better resolution with the expense of penetration. HFUS single element transducers and the mechanical scanning systems for imaging are reviewed, and HFUS array transducers are also briefly summarized. HFUS applications such as the human applications in ophthalmology and dermatology and small animal applications for research purposes are reviewed with vascular and blood imaging in this paper.