• 제목/요약/키워드: Ultra-high temperature condition

검색결과 81건 처리시간 0.037초

레이저 조사 방법으로 제조된 Co 나노닷의 초상자성 현상 관측 (Observation of superparamagnetic behaviors in Co nano dots fabricated by laser irradiation method)

  • 양정엽;윤갑수;도영호;구자현;김채옥;홍진표
    • 한국자기학회:학술대회 개요집
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    • 한국자기학회 2004년도 동계학술연구발표회 논문개요집
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    • pp.219-220
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    • 2004
  • Superparamagnetic regions and magnetic anisotropic properties in randomly orientated Co nano dots(NDs) were investigated as a function of dot diameter, spacing, and density. The Co NDs were fabricated by intentionally exposing a laser source on ultra thin film. Various dot sizes are ultimately realized by changing laser power, scan condition, and intial film thickness. Magnetic hysteresis loops, angle-dependent magnetization, and temperature dependence magnetization of the Co NDs were measured with a superconducting quantum interference device. The analysis of magnetization and hysteresis loops was effectively used to determine superparamagnetic regions of the Co NDs. Up to now, the experimentally observed results repeal that room temperature superparamagnetic limit of our Co NDs was about 30 nm in diameter, with the confirmation of high resolution transmission electron microscope.

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PLD법을 이용한 Buffer Layer 증착온도에 따른 As-doped ZnO 박막의 특성 (Characteristics of As-doped ZnO thin films with various buffer layer temperatures prepared by PLD method)

  • 이홍찬;심광보;오영제
    • 센서학회지
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    • 제15권2호
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    • pp.84-89
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    • 2006
  • Highly concentrated p-type ZnO thin films can be obtained by doping of N, P and As elements. In this study, undoped ZnO buffer layers were prepared on a (0001) sapphire substrate by a ultra high vaccum pulsed laser deposition(UHV-PLD) method. ZnO buffer layers were deposited with various deposition temperature($400{\sim}700^{\circ}C$) at 350 mtorr of oxygen working pressure. Arsenic doped(1 wt%) ZnO thin films were deposited on the ZnO buffer layers by UHV-PLD. Crystallinity of the samples were evaluated by X-ray diffractometer and scanning electron microscopy. Optical, electrical properties of the ZnO thin films were estimated by photoluminescence(PL) and Hall measurements. The optimal condition of the undoped ZnO buffer layer for the deposition of As-doped ZnO thin films was at $600^{\circ}C$ of deposition temperature.

VLS growth of ZrO2 nanowhiskers using CVD method

  • 백민기;박시정;정진환;최두진
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2016년도 제50회 동계 정기학술대회 초록집
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    • pp.149-149
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    • 2016
  • Ceramic is widely known material due to its outstanding mechanical property. Besides, Zirconia(ZrO2) has a low thermal conductivity so it is advantage in a heat insulation. Because of these superior properties, ZrO2 is attracted to many fields using ultra high temperature for example vehicle engines, aerospace industry, turbine, nuclear system and so on. However brittle fracture is a disadvantage of the ZrO2. In order to overcome this problem, we can make the ceramic materials to the forms of ceramic nanoparticles, ceramic nanowhiskers and these forms can be used to an agent of composite materials. In this work, we selected Au catalyzed Vapor-Liquid-Solid mechanism to synthesize ZrO2 nanowhiskers. The ZrO2 whiskers are grown through Hot-wall Chemical Vapor Deposition(Hot wall CVD) using ZrCl4 as a powder source and Au film as a catalyst. This Hot wall CVD method is known to comparatively cost effective. The synthesis condition is a temperature of $1100^{\circ}C$, a pressure of 760torr(1atm) and carrier gas(Ar) flow of 500sccm. To observe the morphology of ZrO2 scanning electron microscopy is used and to identify the crystal structure x-ray diffraction is used.

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0.27% C-1.5% Mn-1.0% Cr 강의 미세조직과 기계적성질에 미치는 Si의 영향 (Effect of Si on Mechanical Properties and Microstructure in 0.27% C-1.5% Mn-1.0% Cr Steel)

  • 정우창
    • 열처리공학회지
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    • 제30권3호
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    • pp.117-126
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    • 2017
  • The variation in microstructure and mechanical properties during heat treatment was examined in a series of 0.27% C-1.5% Mn-1.0% Cr steels with silicon contents in the range of 0 to 1.0 wt%. It was found that addition of 0.5%~1.0% silicon increased both tensile strength and impact toughness through solid solution strengthening and microstructural refinement. 0.27% C-1.0% Si-1.5% Mn-1.0% Cr steel showed tensile strength of 1,700 MPa in the as-quenched condition and the steel revealed a full martensitic structure even after air cooling from $900^{\circ}C$ to room temperature, showing air hardening characteristics. Tempering at $150^{\circ}C$ which corresponds to the typical paint-baking temperature after painting of body in white, slightly decreased the tensile strength and increased elongation, but substantially increased the impact toughness compared to the as-quenched steel.

가공처리조건이 초유 Immunoglobulin G의 변화에 미치는 영향 (Changes of Bovine Colostral Immunoglobulin G on Processing Conditions)

  • 이수원;양동훈;황보식;이승환
    • 한국축산식품학회지
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    • 제21권3호
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    • pp.265-271
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    • 2001
  • We investigated changes of immunoglobulin G (IgG) concentrations by heating and drying condition. Also it is performed to group for commercial product by promoting of IgG preservation and reducing of protein denaturation. The result was that content of IgG in colostrum was higher than normal milk. Especially, IgG content of colostrum within 12 hrs after parturition was over 44.67mg/ml and it is 60 times of normal milk. IgG contents was reduced rapidly according as passage of the time. IgG content of the sample heating at 30min at 65$^{\circ}C$ was still a little higher that heating for 10sec at 72$^{\circ}C$. IgG denaturation of heat treatment at 100$^{\circ}C$ for 10sec was lower than at 85$^{\circ}C$ for 30min. We investigated the changes of IgG concentrations of kinds of market milk different with heating processing. This result showed that IgG denaturation ratio by ultra high temperature pasteurization (UHT) was higher than long time low temperature pasteurization (LTLT). On the other hands, IgG content by spray drying was 14.5mg/g and freezing drying was 10.8mg/g. It showed that denaturation of protein content by freezing drying was more than spray drying.

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스퍼터링 공정 조건이 산화 구리 박막 특성에 미치는 영향 (Influence of Sputtering Conditions on Properties of Copper Oxide Thin Films)

  • 조재유;허재영
    • Current Photovoltaic Research
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    • 제5권1호
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    • pp.15-19
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    • 2017
  • The fossil fuel power consumption generates $CO_2$, which causes the problems such as global warming. Also, the increase in energy consumption has accelerated the depletion of the fossil fuels, and renewable energy is attracting attention. Among the renewable energies, the solar energy gets a lot of attention as the infinite clean energy source. But, the supply level of solar cell is insignificant due to high cost of generation of electric power in comparison with fossil fuels. Thus several researchers are recently doing the research on ultra-low-cost solar cells. Also, $Cu_2O$ is one of the applied materials as an absorption layer in ultra-low-cost solar cells. Cuprous oxide ($Cu_2O$) is highly desirable semiconductor oxide for use in solar energy conversion due to its direct band gap ($E_g={\sim}2.1eV$) and a high absorption coefficient that absorbs visible light of wavelengths up to 650 nm. In addition, $Cu_2O$ has several advantages such as non-toxicity, low cost and can be prepared with simple and cheap methods on large scale. In this work, we fabricated the $Cu_2O$ thin films by reactive sputtering method. The films were deposited with a Cu target with variable parameters such as substrate temperature, rf-power, and annealing condition. Finally, we confirmed the structural properties of thin films by XRD and SEM.

제논 혼합가스를 이용한 고효율 면광원과 국부적 밝기 제어 방식 (High Luminous Efficiency Flat Light Source with Xe mixture Gas Discharge and Areal Brightness Control Method)

  • 정재철;서인우;오병주;황기웅
    • 한국조명전기설비학회:학술대회논문집
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    • 한국조명전기설비학회 2009년도 추계학술대회 논문집
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    • pp.153-157
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    • 2009
  • A Highly efficient Mercury-free Flat Fluorescent Lamp (MFFL) with dielectric barrier Xe gas discharge was developed for an alternative of conventional line-type Cold Cathode Fluorescent Lamps (CCFLs) which shows a wide voltage margin and a stable discharge operation for diffuse glow discharge with an application of a auxiliary electrode. Electro-optic characteristics of the MFFL were examined through the changes in ambient temperature, total pressure and Xe partial pressure. the single cell is expanded into a multi-structured configuration to realize a large sized lamp by a simple repetition of the single cells, and a new driving scheme is proposed for an adaptive brightness control using dual auxiliary electrodes and bi-polar drive scheme. In addition, interesting application of this ultra high luminance flat lamp by the optimization of the gas condition and the pattern of the rear phosphor layer is suggested as a good alternative of daylight lamp source

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압축강도 및 양생조건에 따른 초고성능 콘크리트의 직접인장강도 특성 (Effect of Compressive Strength and Curing Condition on the Direct Tensile Strength Properties of Ultra High Performance Concrete)

  • 박지웅;이건철
    • 한국건축시공학회지
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    • 제17권2호
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    • pp.175-181
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    • 2017
  • 본 연구는 초고강도 섬유보강 콘크리트의 인장강도 특성을 파악하기 위한 일환의 연구로서 직접인장시험에 의한 노치가 도입된 시험체의 인장성능을 파악하기 위하여 시험변수는 목표 설계기준강도 120, 150 및 180MPa를 대상으로 하였으며, 양생조건을 일반 수중양생과 $90^{\circ}C$ 고온증기 양생조건으로 하여 그 특성을 검토하였다. 전반적으로 노치타입의 직접인장강도 시험체는 기존 직접인장 시험체에 비해 중앙균열 유도가 효과적인 것으로 나타났으며 데이터를 직접 인장강도-변형률 그래프로 나타낸 결과 먼저 재령 측면에서는 28일에서 56일로 진행할 때의 강도 상승이 가장 높은 것으로 측정 되었으며, 양생조건 측면에서는 고온증기 양생의 경우 수중양생의 비해 초기 강도가 높으나 장기 재령에 가까워질수록 두 가지 양생조건의 직접인장강도 차이가 미비해지는 것을 알 수 있었다. 최대인장강도는 수중양생의 경우 모든 목표설계강도가 재령이 증가할수록 일정하게 증가하는 것으로 나타났으며, 증기양생의 경우 재령 7일에서 초기강도 발현 효과로 인해 상당히 증가하는 경향을 나타내었다. 초기균열 강도는 수중양생의 경우 재령경과에 따라 증가하며, 증기양생의 경우 7일에서 수중양생에 비해 높은 것으로 나타난 반면에 28일 강도는 저하하는 경향을 나타내었다. 이부분에 대해서는 강섬유의 배열상태 등의 검토가 필요할 것으로 사료된다.

5kW 급 MCFC 발전시스템 촉매연소기의 유동 및 연소 특성에 대한 수치적 연구 (A Numerical Study on the Internal Flow and Combustion Characteristics of the Catalytic Combustor for the 5kW MCFC Power system)

  • 김종민;이연화;김만영;김형곤;홍동진;조주형;김한석;안국영
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2008년도 추계학술대회B
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    • pp.3049-3052
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    • 2008
  • MCFC(molten carbonate fuel cell) power generation system is prime candidate for the utilization of fossil based fuels to generate ultra clean power with a high efficiency. In the MCFC power plant system, a combustor performs a role to supply high temperature mixture gases for cathode and heat for reformer by using the stack off-gas of the anode which includes a high concentration of $H_2O$ and $CO_2$. Since a combustor needs to be operated in a very lean condition and to avoid excessive local heating, catalytic combustor is usually used. The catalytic combustion is accomplished by the catalytic chemical reaction between fuel and oxidizer at catalyst surface, different from conventional combustion. In this study, a mathematical model for the prediction of internal flow and catalytic combustion characteristics in the catalytic combustor adopted in the MCFC power plant system is suggested by using the numerical methods. The numerical simulation models are then implemented into the commercial CFD code. After verifying result by comparing with the experimental data and calibrated kinetic parameters of catalytic combustion reaction, a numerical simulation is performed to investigate the variation of flow and combustion characteristics by changing such various parameters as inlet configuration and inlet temperature. The result show that the catalytic combustion can be effectively improved for most of the case by using the perforated plate and subsequent stable catalytic combustion is expected.

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수침 및 고온이 고결모래의 전단강도에 미치는 영향 (Effect of Immersion and High Temperature on Shear Strength of Cemented Sand)

  • 문홍득;황금비;김태헌;박성식
    • 한국지반공학회논문집
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    • 제39권7호
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    • pp.17-30
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    • 2023
  • 본 논문에서는 직접전단시험을 이용하여 수침이나 고온이 고결모래의 전단강도에 미치는 영향에 대해 연구하였다. 고결제로 초속경 시멘트와 에폭시 수용액을 사용하여 표준사인 주문진표준사를 고결시켰다. 고결제는 4, 8, 또는 12%로 혼합한 다음 다짐방식으로 직경 64mm, 높이 25mm의 원주형 고결 공시체를 제작하였다. 양생일은 모두 3일로 동일하며, 양생조건은 대기중 양생, 수침 및 가열 조건이다. 여기서 가열 조건은 수침한 공시체를 전자레인지로 3분씩 3회 반복하여 공시체 내부에 90℃ 정도의 고온을 발생시켰다. 고결제의 종류에 관계없이 고결제 함유량이 증가할수록 고결모래의 점착력은 증가하였으나, 내부마찰각은 약간 증가하거나 오히려 감소하였다. 초속경 시멘트 고결모래에 비해 에폭시 고결모래가 평균적으로 점착력은 5배, 마찰각은 10° 정도 높게 나타나 더 높은 강도를 보였다. 전반적으로 고결제의 종류에 관계없이 수침 시 전단강도는 감소하고 가열 시 전단강도는 증가하였다. 특히, 에폭시 고결모래의 경우 가열 시 점착력은 평균 3배, 내부마찰각은 20° 이상 증가하였다.