• Title/Summary/Keyword: Two-phase sampling

검색결과 173건 처리시간 0.031초

공기중 이소시아네이트류의 측정 및 분석방법에 관한 비교연구 (A Comparison of Sampling and Analytical Methods for Airborne Isocyanates)

  • 변혜정;윤충식;백남원
    • 한국환경보건학회지
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    • 제22권2호
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    • pp.32-42
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    • 1996
  • This study was performed to evaluate accuracy and precision of filter method and impinger method for analyzin airborne isocyanates in mixture (2, 6-TDI, HDI, 2, 4-TDI, MDI). Filter method was performed using the OSHA Method 42 and impinger method using the NIOSH Method 5521. The samples were analyzed by high performance liquid chromatography-ultraviolet detector (HPLC-UVD). After the optimum operating conditions for each method were investigated, samples with various concentration levels were quantified at the conditions. The precision was expressed by the pooled coefficient of variation(C.V.) and the accuracy by overall accuracy. The results are summarized as follows: 1. The optimum condition of filter method was determined at 35/65 ACN/buffer (0.01 M ammonium acetate) in mobile phase. And in case of impinger method, it was at 30/70 ACN/buffer(0.2 M sodium acetate). The effect of concentrations of acetate on the separation of the peaks was not significant, but, the effect of ACN/buffer ratio was significant. 2. The correlation coefficients for the two methods were above 0.9 in all isocyanate compounds. Average recovery efficiencies for 2, 6-TDI, HDI, 2, 4-TDI and MDI in filter method were 92.4%, 102.6%, 87.3% and 101.0%, respectively. Those in impinger method were 106.6%, 106.7%, 99.0% and 103.6%, respectively. As a result, the recovery efficiency of impinger method was higher than those of filter method in analyzing isocyanate compounds. 3. The pooled coefficients of variations of the methods were slightly higher than expected. The overall accuracies of the methods were within $\pm 25%$ for each isocyanate compound. Since these results satisfy NIOSH criteria, the accuracy of the experiment is appropriate. 4. As seen above, impinger method is more efficient than filter method. But, there are many disadvantages in impinger method. Therefore, solid sorbent such as a glass fiber filter must be developed in order to have the high efficiency not less than that of impinger method in the future.

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오존발생장치용 정출력 전원장치의 개발 (Development of Constant Output Power Supply System for Ozonizer)

  • 우정인;우성훈;노인배;박지호;김동완
    • 조명전기설비학회논문지
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    • 제19권7호
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    • pp.113-121
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    • 2005
  • 본 논문에서는 오존발생장치의 전원측 파형에 포함되는 고주파수의 노이즈를 제거하고, 디지털 궤환 제어에 의해 오존 출력을 제어하기 위하여 전원장치의 출력측 LC 필터와 방전관 용량으로부터 커패시터 전압과 전류를 검출하여 2중의 제어루프를 설계하였다. 디지털 제어기의 연산지연시간을 보상하기 위하여 연산지연시간을 전원장치 플랜트의 고유한 파라미터로 가정하고, 플랜트 모델에 포함시켜 모델링 하였다. 오존발생장치의 부하변동에 따르는 과도상태 응답특성을 개선하고, 파라미터 변동에 강인한 특성을 얻기 위하여 내부 전류 모델 제어기를 제안하였다. 또한 오존발생장치용 전원장치에서 영 오차의 정상 상태를 얻기 위하여 외부 전압 제어루프를 구성하여 비례 제어기와 공진 제어기를 병렬로 연결한 비례-공진 전압제어기를 제안하였다.

UPS 인버터의 성능 개선을 위한 강인한 2중 디지털 제어기의 설계 (Design of Robust Double Digital Controller to Improve Performance for UPS Inverter)

  • 박지호;노태균;김춘삼;안인모;우정인
    • 전력전자학회논문지
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    • 제8권2호
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    • pp.116-127
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    • 2003
  • 본 논문에서는 UPS 인버터의 성능 개선을 위하여 출력측 LC 필터의 커패시터 전압과 전류의 2중 제어루프를 구성하고, 2중 제어루프에 디지털 제어시스템을 채택하였다 또한, 디지털 제어기의 연산지연시간을 보상하기 위하여 이러한 연산지연시간을 인버터 플랜트의 고유한 파라미터로 가정하고, 플랜트 모델에 포함시켜 모델링 하였다. UPS 인버터 출련전압의 과도상태 응답특실을 개선하고, 파라미터 변동에 강인한 특성을 얻기 위하여 2중 제어루프에서 내부 전류 제어루프는 내부 모델 제어기를 제안하였다. UPS 인버터 출력전압의 0의 정상상태 오차를 얻기 위하여 외부 전압 제어루프는 비례 제어기와 공진 제어기를 병렬로 연결한 비례-공진 진압제어기를 제안하였다.

미지 호흡운동에 의한 MRI 아티팩트의 수정 (MRI Artifact Correction due to Unknown Respiratory Motion)

  • 김응규
    • 대한전자공학회논문지SP
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    • 제41권5호
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    • pp.53-62
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    • 2004
  • 본 연구에서는 화상평면내 미지 호흡운동에 의한 MRI 아티팩트를 수정하기 위한 개선된 후처리 기법을 제안한다. 호흡운동은 2차원의 선형확대축소 운동으로 모델화 된다 신체조직을 비압축성 유체모양의 물질로 가정할 때 촬상 대상물체에 대한 단위체적당 푸로톤 밀도는 일정하다고 가정한다. 적용한 모델에 의하면 호흡운동은 위상오차와 불균일 표본화 및 진폭변조왜를 MRI 데이터에 부여한다. 운동파라메타가 알려져 있거나 추정가능하다고 할 때 양선형 중첩법에 기초한 재구성 알고리즘이 MRI 아티팩트를 수정하기 위해 사용된다. 운동 파라메타가 미지인 경우 스펙트럼 이동법을 적용해서 호흡변동함수와 x 방향 확대계수 및 x 방향 확대중심을 추정한다. 다음으로 에너지 최소법을 이용해서 y 방향 확대계수 및 y 방향 확대중심을 추정한다. 최종적으로 시뮬레이션된 체동화상을 통해서 제안한 본 방법의 유효성을 확인한다.

위상차 현미경법을 이용한 공기중 석면농도 분석에서의 정도관리 (Quality Control of Asbestos Fiber Counting for Airborne Samples Using Phase Contrast Microscopy)

  • 강보영;신용철;백남원
    • 한국산업보건학회지
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    • 제1권2호
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    • pp.221-237
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    • 1991
  • This study was conducted to evaluate the accuracy and the precision of asbestos counting data produced by the Division of Industrial Health, School of Public Health, Seoul National Universitys (SNU). The study was performed from July 18 to October 4, 1991, and the results are summarized as follows. 1. Intracounter Relative Standard Deviations (Sr) in the category of 5-50.5 fibers as total fibers counted ranged from 0.27 to 0.37, which were greater than 0.10-0.17 which were reported by the NIOSH. The reasons are supposed to be as follows. First, inexperience of counters in asbestos fiber counting was considered to be a main reason. Second, poor quality of samples due to sampling and mounting error increased variation of counting. Third, fiber density of many samples were less than $100fibers/mm^2$. But Intracounter Relative Standard Deviations (Sr) in samples with >50.5 fibers ranged from 0.l6 to 0.20, approaching the value 01 NIOSH. 2. Intralaboratory Relative Standard Deviations (Sr) in categories of 5-20.5, >20.5-50.5 and >50.5 fibers were 0.54, 0.37 and 0.26, respectively. Intralaboratory Sr in samples with fiber density greater than $100fibers/mm^2$ was 0.26. This was similar to the values reported by other foreign experienced laboratories. 3. Comparing results of three counters, Counter C, a beginner, overestimated asbestos fiber concentrations. 4. Since our SNU laboratory has participated in two quality control programs, IOMA-F.R.I.C.A., U.K. and NIOSH PAT Program, U.S.A., this laboratory has been evaluated as " Rating 1" and "Proficient" laboratory, by IOM and NIOSH, respectively.

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UPS 인버터의 디지털 제어기 및 모니터링 시스템의 개발 (Development of Digital Controller and Monitoring System for UPS Inverter)

  • 박지호;황기현;김동완
    • 전자공학회논문지SC
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    • 제44권1호
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    • pp.1-11
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    • 2007
  • 본 논문에서는 UPS 인버터의 성능 개선을 위하여 출력측 LC 필터의 커패시터 전압과 전류의 2중 제어루프를 구성하고, 2중 제어루프에 디지털 제어시스템을 설계하였다. 또한, 디지털 제어기의 연산지연시간을 보상하기 위하여 이러한 연산지연시간을 인버터 플랜트의 고유한 파라미터로 가정하고, 플랜트 모델에 포함시켜 모델링 하였다. UPS 인버터 출력전압의 과도상태 응답특성을 개선하고, 파라미터 변동에 강인한 특성을 얻기 위하여 2중 제어루프에서 내부 전류 제어루프는 내부 모델 제어기를 제안하였다. UPS 인버터 출력전압의 0의 정상상태 오차를 얻기 위하여 외부 전압 제어루프는 비례 제어기와 공진 제어기를 병렬로 연결한 비례-공진 전압제어기를 제안하였다. 또한, 사용자에게 쉽게 UPS의 동작 상태를 표시하기 위하여 그래픽 사용자 인터페이스를 이용한 UPS의 모니터링 시스템을 구현하였다.

Three-dimensional Kinematic Analysis of the Yurchenko Layout with 360-degree Twist in Female Vaults: Deterministic Model and Judges' Scores

  • Park, Cheol-Hee;Kim, Young-Kwan
    • 한국운동역학회지
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    • 제27권1호
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    • pp.9-18
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    • 2017
  • Objective: The purpose of this study was to identify kinematic variables that govern successful performance and judges' scores and to establish correlative relationships among those of Yurchenko layout with a full twist in female vaults. Method: Four video cameras with sampling rate of 60 Hz collected 32 motion data of Yurchenko vaults from twenty-two female participants (age: $18.6{\pm}3.6years$, height: $153.0{\pm}6.5cm$, mass: $44.7{\pm}7.3kg$) during national competition. Posting processing and calculations of kinematic variables were performed in Kwon 3D XP and $Matlab^{(R)}$ programs. Correlation and regression analyses were applied to find the relationships between the obtained scores and kinematic variables. Deterministic model (Hay & Reid, 1988) was used to investigate the strength of correlative relationships among kinematic variables. Results: The obtained scores from the judges' decision were mainly affected by post-flight peak height, horse contact time, knee angle at landing, and horse takeoff angle. Strong blocking during horse contact was required to get successful performance and obtain high scores. Modified deterministic model showed that round-off entrance and takeoff angles and resultant velocity of the center of mass (CM) during the roundoff phase were the starting variables affecting performance in the following kinematics. Knee angle at landing, a highly influential variable on the obtained point, was only determined by judges' decision without significant correlative relationship with previous kinematic variables. Conclusion: The obtained scores highly depended on kinematic variables of post-flight and horse contact phases that were affected by those from the previous phases including round-off postures and resultant velocity of the body center of mass.

CRM을 통한 고객충성도에 관한 사례연구 (A Case Study on the Customer Loyalty through CRM: -Focused on the Uzbekistan's Mobile Telecommunication Companies-)

  • 무민 마카모프;김동환
    • 한국산학기술학회논문지
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    • 제7권6호
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    • pp.1356-1363
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    • 2006
  • 본 연구의 목적은 모바일 정보통신 시장에 있어서, 이에 관련한 공급자가 어떻게 성공적으로 기업을 관리함으로써 고객 충성도를 증대시킬 것인가에 대한 것이다. 이러한 목적을 달성하기 위하여 본 연구는 우즈베키스탄의 모바일 정보통신 시장을 사례분석 함으로써 외국의 경우를 고찰하고자 하였다. 본 소고에서는 우선적으로 CRM의 영향력과 제반 요인들이 CRM 시스템을 통하여 고객 이해력에 의한 충성도를 제고시킬 것인가를 분석 검토 하고자 하였다. 고객의 욕구와 고객 만족, 고객 충성도의 관련성들이 어떻게 기업의 수익성과 연계되어 발생하는가는 여러 가지 복잡한 방법들과 관련되어 있는 것으로 나타났다. 본 연구의 특징은 외국의 사례를 중심으로 고객만족과 고객충성도의 관련 속에서 분리한 경우와 결합한 경우의 특성들로 각각 분석 고찰 한 점이다.

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Research on Digital Complex-Correlator of Synthetic Aperture Radiometer: theory and simulation result

  • Jingye, Yan;Ji, Wu;Yunhua, Zhang;Jiang, Changhong;Tao, Wang;Jianhua, Ren;Jingshan, Jiang
    • 대한원격탐사학회:학술대회논문집
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    • 대한원격탐사학회 2002년도 Proceedings of International Symposium on Remote Sensing
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    • pp.587-592
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    • 2002
  • A new digital correlator fur an airborne synthetic aperture radiometer was designed in order to replace the conventional analog correlator unit which will become very complicated while the number of channels is increasing. The digital correlator uses digital IQ demodulator instead of the intermediate frequency (IF) phase shifter to make the correlation processing performed digitally at base band instead of analogly at IF. This technique has been applied to the digital receiver in softradio. The down-converted IF signals from each pair of receiver channels become low rate base-band digital signals after under-sampled, Digitally Down-Converted (DDC), decimated and filtered by FIR filters. The digital signals are further processed by two digital multipliers (complex correlation), the products are integrated by the integrators and finally the outputs from the integrators compose of the real part and the imaginary part of a sample of the visibility function. This design is tested by comparing the results from digital correlators and that from analog correlators. They are agreed with each other very well. Due to the fact that the digital correlators are realized with the help of Analog-Digital Converter (ADC) chips and the FPGA technology, the realized volume, mass, power consumption and complexity turned out to be greatly reduced compared with that of the analog correlators. Simulations show that the resolution of ADC has an influence on the synthesized antenna patterns, but this can be neglected if more than 2bit is used.

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20대 남성의 낮은 조도의 평지 보행 시 보행 패턴 변화 (Changes of Walking Pattern for Young Adults dur ing Level Walking under Low Illumination)

  • 최진승;강동원;방윤환;탁계래
    • 한국운동역학회지
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    • 제20권4호
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    • pp.381-386
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    • 2010
  • This study examined the changes in the walking pattern during level walking under low illumination conditions. Fourteen male subjects ($22.1{\pm}2.21$ years, $174{\pm}3.74\;cm$, $68.86{\pm}10.81\;kg$) with normal vision and no disabilities were enrolled in this study. All experiments were performed on a level walkway with three conditions: normal walking (preferred & low speed) and walking with low illumination. 3D motion capturing system was used for acquisition and analysis of the walking motion data with a sampling frequency of 120Hz. The walking speed, normalized jerk(NJ) at the center of mass(COM), wrist and heel, knee and elbow joint angle, ratio of the knee joint angle to elbow joint angle and the toe clearance on stance phase were used to compare the differences in walking pattern between the two illumination conditions, The results showed that the walking speed and joint angles decreased in low illumination, whereas the NJ and toe minimum clearance increased. In low illumination, most variables were similar to effects of low speed walking, but toe clearance was different from the effects of low speed. These results can be used as primary data for examining the changes in the level walking pattern of young adults under low illumination. Further study will be needed to compare these results in young adults with those in the elderly.