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Synthesis and characterization of polyimides for FPC applications

  • Yeon, J.H.;Bae, Y.U.;Yoon, T.H.
    • Proceedings of the Polymer Society of Korea Conference
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    • 2006.10a
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    • pp.227-227
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    • 2006
  • It was attempted to synthesize polyimides from PPMDA and 3FPPMDA with mDAPPO/pPDA in order to afford CTE of 17ppm and adhesion property of 80g/mm, besides high Tg (>$300^{\circ}C$), good thermal stability (>$500^{\circ}C$), low water absorption and good solubility. The polyimides were prepared via a conventional two-step process; preparation of poly(amic-acid), followed by solution imidization by refluxing in NMP with o-DCB and the molar ratio of mDAPPO/pPDA was varied. The polyimides were characterized by FT-IR, NMR, DSC and TGA. In addition, intrinsic viscosity, solubility and coefficient of thermal expansion (CTE) were also measured.

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Prediction of vibration response of functionally graded sandwich plates by zig-zag theory

  • Simmi, Gupta;H.D., Chalak
    • Advances in aircraft and spacecraft science
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    • v.9 no.6
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    • pp.507-523
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    • 2022
  • This study is aimed to accurately predict the vibration response of two types of functionally graded sandwich plates, one with FGM core and another with FGM face sheets. The gradation in FGM layer is quantified by exponential method. An efficient zig-zag theory is used and the zigzag impacts are established via a linear unit Heaviside step function. The present theory fulfills interlaminar transverse stress continuity at the interface and zero condition at the top and bottom surfaces of the plate for transverse shear stresses. Nine-noded C-0 FE having 8DOF/node is utilized throughout analysis. The present model is free from the obligation of any penalty function or post-processing technique and hence is computationally efficient. Numerical results have been presented on the free vibration behavior of sandwich FGM for different end conditions, lamination schemes and layer orientations. The applicability of present model is confirmed by comparing with published results. Several new results are also specified, which will serve as the benchmark for future studies.

Direct tracking of noncircular sources for multiple arrays via improved unscented particle filter method

  • Yang Qian;Xinlei Shi;Haowei Zeng;Mushtaq Ahmad
    • ETRI Journal
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    • v.45 no.3
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    • pp.394-403
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    • 2023
  • Direct tracking problem of moving noncircular sources for multiple arrays is investigated in this study. Here, we propose an improved unscented particle filter (I-UPF) direct tracking method, which combines system proportional symmetry unscented particle filter and Markov Chain Monte Carlo (MCMC) algorithm. Noncircular sources can extend the dimension of sources matrix, and the direct tracking accuracy is improved. This method uses multiple arrays to receive sources. Firstly, set up a direct tracking model through consecutive time and Doppler information. Subsequently, based on the improved unscented particle filter algorithm, the proposed tracking model is to improve the direct tracking accuracy and reduce computational complexity. Simulation results show that the proposed improved unscented particle filter algorithm for noncircular sources has enhanced tracking accuracy than Markov Chain Monte Carlo unscented particle filter algorithm, Markov Chain Monte Carlo extended Kalman particle filter, and two-step tracking method.

Direct position tracking method for non-circular signals with distributed passive arrays via first-order approximation

  • Jinke Cao;Xiaofei Zhang;Honghao Hao
    • ETRI Journal
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    • v.46 no.3
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    • pp.421-431
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    • 2024
  • In this study, a direct position tracking method for non-circular (NC) signals using distributed passive arrays is proposed. First, we calculate the initial positions of sources using a direct position determination (DPD) approach; next, we transform the tracking into a compensation problem. The offsets of the adjacent time positions are calculated using a first-order Taylor expansion. The fusion calculation of the noise subspace is performed according to the NC characteristics. Because the proposed method uses the signal information from the previous iteration, it can realize automatic data associations. Compared with traditional DPD and two-step localization methods, our novel process has lower computational complexity and provides higher accuracy. Moreover, its performance is better than that of the traditional tracking methods. Numerous simulation results support the superiority of our proposed method.

Synthesis and Characterization of Sm2O3 Doped CeO2 Nanopowder by Reverse Micelle Processing (역마이셀을 이용한 Sm2O3 도핑 CeO2 나노분말의 합성 및 특성)

  • Kim, Jun-Seop;Bae, Dong-Sik
    • Korean Journal of Materials Research
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    • v.22 no.4
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    • pp.207-210
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    • 2012
  • The preparation of $Sm_2O_3$ doped $CeO_2$ in Igepal CO-520/cyclohexane reverse micelle solutions has been studied. In the present work, we synthesized nanosized $Sm_2O_3$ doped $CeO_2$ powders by reverse micelle process using aqueous ammonia as the precipitant; hydroxide precursor was obtained from nitrate solutions dispersed in the nanosized aqueous domains of a micro emulsion consisting of cyclohexane as the oil phase, and poly (xoyethylene) nonylphenylether (Igepal CO-520) as the non-ionic surfactant. The synthesized and calcined powders were characterized by Thermogravimetry-differential thermal analysis (TGA-DTA), X-ray diffraction analysis (XRD), and Transmission electron microscopy (TEM). The crystallite size was found to increase with increase in water to surfactant (R) molar ratio. Average particle size and distribution of the synthesized $Sm_2O_3$ doped $CeO_2$ were below 10 nm and narrow, respectively. TG-DTA analysis shows that phase of $Sm_2O_3$ doped $CeO_2$ nanoparticles changed from monoclinic to tetragonal at approximately $560^{\circ}C$. The phase of the synthesized $Sm_2O_3$ doped $CeO_2$ with heating to $600^{\circ}C$ for 30 min was tetragonal $CeO_2$. This study revealed that the particle formation process in reverse micelles is based on a two step model. The rapid first step is the complete reduction of the metal to the zero valence state. The second step is growth, via reagent exchanges between micelles through the inter-micellar exchange.

Heterologous Expression and Optimized One-Step Separation of Levansucrase via Elastin-like Polypeptides Tagging System

  • Kang, Hye-Jin;Kim, Jin-Hee;Chang, Woo-Jin;Kim, Eung-Soo;Koo, Yoon-Mo
    • Journal of Microbiology and Biotechnology
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    • v.17 no.11
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    • pp.1751-1757
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    • 2007
  • Elastin-like polypeptides (ELPs) undergo a reversible inverse phase transition upon a change in temperature. This thermally triggered phase transition allows for a simple and rapid means of purifying a fusion protein. Recovery of ELPs-tagged fusion protein was easily achieved by aggregation, triggered either by raising temperature or by adding salt. In this study, levansucrase has been used as a model enzyme in the development of a simple one-step purification method using ELPs. The levansucrase gene cloned from Pseudomonas aurantiaca S-4380 was tagged with various sizes of ELPs to functionally express and optimize the purification of levansucrase. One of two ELPs, ELP[V-20] or ELP[V-40], was fused at the C-terminus of the levansucrase gene. A levansucrase-ELP fusion protein was expressed in Escherichia coli $DH5{\alpha}$ at $37^{\circ}C$ for 18 h. The molecular masses of levansucrase-ELP[V-20] and levansucrase-ELP[V-40] were determined as 56 kDa and 65 kDa, respectively. The phase transition of levansucrase-ELP[V-20] occurred at $20^{\circ}C$ in 50 mM Tris-Cl (pH 8) buffer with 3 M NaCl added, whereas the phase transition temperature ($T_t$) of levansucrase-ELP[V-40] was $17^{\circ}C$ with 2 M NaCl. Levansucrase was successfully purified using the phase transition characteristics of ELPs, with a recovery yield of higher than 80%, as verified by SDS-PAGE. The specific activity was measured spectrophotometrically to be 173 U/mg and 171 U/mg for levansucrase-ELP[V-20] and levansucrase-ELP[V-40], respectively, implying that the ELP-tagging system provides an efficient one-step separation method for protein purification.

Kalman Filter Design For Aided INS Considering Gyroscope Mixed Random Errors (자이로의 불규칙 혼합잡음을 고려한 보조항법시스템 칼만 필터 설계)

  • Seong, Sang-Man
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.34 no.4
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    • pp.47-52
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    • 2006
  • Using the equivalent ARMA model representation of the mixed random errors, we propose Klaman filter design methods for aided INS(Inertial Navigation System) which contains the gyroscope mixed random errors. At first step, considering the characteristic of indirect feedback Kalman filter used in the aided INS, we perform the time difference of equivalent ARMA model. Next, according to the order of the time differenced ARMA model, we achieve the state space conversion of that by two methods. If the order of AR part is greater than MA part, we use controllable or observable canonical form. Otherwise, we establish the state apace equation via the method that several step ahead predicts are included in the state variable, where we can derive high and low order models depending on the variable which is compensated from gyroscope output. At final step, we include the state space equation of gyroscope mixed random errors into aided INS Kalman filter model. Through the simulation, we show that both the high and low order filter models proposed give less navigation errors compared to the conventional filter which assume the mixed random errors as white noise.

Online Video Synopsis via Multiple Object Detection

  • Lee, JaeWon;Kim, DoHyeon;Kim, Yoon
    • Journal of the Korea Society of Computer and Information
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    • v.24 no.8
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    • pp.19-28
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    • 2019
  • In this paper, an online video summarization algorithm based on multiple object detection is proposed. As crime has been on the rise due to the recent rapid urbanization, the people's appetite for safety has been growing and the installation of surveillance cameras such as a closed-circuit television(CCTV) has been increasing in many cities. However, it takes a lot of time and labor to retrieve and analyze a huge amount of video data from numerous CCTVs. As a result, there is an increasing demand for intelligent video recognition systems that can automatically detect and summarize various events occurring on CCTVs. Video summarization is a method of generating synopsis video of a long time original video so that users can watch it in a short time. The proposed video summarization method can be divided into two stages. The object extraction step detects a specific object in the video and extracts a specific object desired by the user. The video summary step creates a final synopsis video based on the objects extracted in the previous object extraction step. While the existed methods do not consider the interaction between objects from the original video when generating the synopsis video, in the proposed method, new object clustering algorithm can effectively maintain interaction between objects in original video in synopsis video. This paper also proposed an online optimization method that can efficiently summarize the large number of objects appearing in long-time videos. Finally, Experimental results show that the performance of the proposed method is superior to that of the existing video synopsis algorithm.

The Effect of Disturbed Vision on Gait Parameters of the Young Healthy Population (혼란스러운 시각의 영향에 따른 보행요소들의 평가)

  • Kim Kyoung;Park Young-Han;Bae Sung-Soo
    • The Journal of Korean Physical Therapy
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    • v.12 no.1
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    • pp.41-47
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    • 2000
  • BACKGROUND AND PURPOSE. The purpose of this study is to investigate the effect of the disturbed vision on the gait distance parameters on the healthy young population. SUBJECTS. Twenty four healthy college aged individuals are randomly assigned to both a condition with a strobe light and the other condition without a strobe light. METHODS. The instrumentation used for gait analysis is the GaitRite electronic walkway system with a personal IBM computer. The examiner naked all the subjects to walk 6 times on the gait mat without the strobe light and. 6 times on the mat with the strobe light. The first 4 trials were practice and the last two trials were recorded in both conditions. The gait parameters analyzed were as follows : velocity, cadence, step length, and heel to heel base of support. RESULTS. Paired samples t-test used for this study did not found any significant differences between the two conditions because the p-values that were analyzed on the experiment were Utter than 0.05. The gait parameters that were analyzed included cadence, velocity, left and right heel to heel base of support, and left and right step length. DISCUSSION AND CONCLUSION. Based on this population, the condition of disturbed vision via the effect of the strobe light was not significantly challenging to compromise the body's sensory systems. However, in the elderly population, these systems can undergo age related changes. Visual changes rapidly decline in people 60 to 80 years of age and changes in the vestibular system include $20-40\%$ reduction in hair cells.

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Synthesis of Silicon Carbide Whiskers (I) : Reaction Mechanism and Rate-Controlling Reaction (탄화규소 휘스커의 합성(I) : 반응기구의 율속반응)

  • 최헌진;이준근
    • Journal of the Korean Ceramic Society
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    • v.35 no.12
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    • pp.1336-1336
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    • 1998
  • A twt -step carbothermal reduction scheme has been employed for the synthesis of SiC whiskers in an Ar or a H2 atmosphere via vapor-solid two-stage and vapor-liquid-solid growth mechanism respectively. It has been shown that the whisker growth proceed through the following reaction mechanism in an Ar at-mosphere : SiO2(S)+C(s)-SiO(v)+CO(v) SiO(v)3CO(v)=SiC(s)whisker+2CO2(v) 2C(s)+2CO2(v)=4CO(v) the third reaction appears to be the rate-controlling reaction since the overall reaction rates are dominated by the carbon which is participated in this reaction. The whisker growth proceeded through the following reaction mechaism in a H2 atmosphere : SiO2(s)+C(s)=SiO(v)+CO(v) 2C(s)+4H2(v)=2CH4(v) SiO(v)+2CH4(v)=SiC(s)whisker+CO(v)+4H2(v) The first reaction appears to be the rate-controlling reaction since the overall reaction rates are enhanced byincreasing the SiO vapor generation rate.