• 대한화학회지
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• 제25권1호
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• pp.13-20
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• 1981

Iminoxyl biradical은 biradical spin probe로 액체결정에 주입시켜 그 결정의 director분포에 관한 역학적성질을 조사하는데 유용한 물질이다. 새로운 방법으로 iminoxyl biradical을 합성하는 과정에서 각 단계의 합성중간 생성물들을 녹는점측정과 NMR, IR, UV 및 Mass 등과 같은 분광학적인 방법으로 확인하였다. 최종 생성물인 iminoxyl biradical은 EPR 분광법으로 확인하고 두 spin간의 상호작용도 EPR peaks로 고찰하였다.

• Journal of Microbiology and Biotechnology
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• 제19권7호
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• pp.658-665
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• 2009

Quality control QC for spot-uniformity is a critical point in fabricating an oligonucleotide array, and quantification of targets is very important in array analysis. We developed two new types of QC probes as a means of confirming the quality of the uniformity of attached probes and the quantification of targets. We compared the signal intensities and fluorescent images of the QC and target-specific probes of arrays containing only target-specific probes and those containing both QC and target-specific probes. In a comparison of quality control methods, it was found that the arrays containing QC probes could check spot-uniformity or spot defects during all processes of array fabrication, including after spotting, after washing, and after hybridization. In a comparison of quantification results, the array fabricated by the method using QC probes showed linear and regular results because it was possible to normalize variations in spot size and morphology and amount of attached probe. This method could avoid errors originating in probe concentration and spot morphology because it could be normalized by QC probes. There were significant differences in the signal intensities of all mixtures (P<0.05). This result indicates that the method using QC probes is more useful than the ordinary method for quantification of mixed target. In the quantification of mixed targets, this method could determine a range for mixed targets of various amounts. Our results suggest that methods using QC probes for array fabrication are very useful to the quality control of spots in the fabrication processes of quantitative oligonucleotide arrays.

• Nuclear Engineering and Technology
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• 제53권9호
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• pp.2982-2989
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• 2021

One of the consequences of the 475 ℃ embrittlement of duplex stainless steels is the reduction of the resistance to localized corrosion. Therefore, the detection of this type of embrittlement before the material exhibits significant loss in toughness, and corrosion resistance is important to ensure the structural integrity of critical components under corrosion threats. In this research, conductivity measurements are performed using the alternating current potential drop (ACPD) technique with using a portable four-point probe as a nondestructive evaluation (NDE) method for detecting the embrittlement in a 2507 (UNS S32750) super duplex stainless steel (SDSS) aged at 475 ℃ from as-received condition to 300 h. The electric conductivity results were compared against two electrochemical tests namely double loop electrochemical potentiokinetic reactivation (DL-EPR) and critical pitting temperature (CPT). Mechanical tests and the microstructure characterized using scanning electron microscopy (SEM) imaging are conducted to track the progress of embrittlement. It is shown that the electric conductivity correlates with the changes in impact energy, microhardness, and CPT corrosion tests result demonstrating the feasibility of the four-point probe as a possible field-deployable method for evaluating the 475 ℃ embrittlement of 2507 SDSS.

• Journal of Korean Dental Science
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• 제9권2호
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• pp.49-54
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• 2016

Purpose: The purpose of this study was to assess the relationship between gingival biotype and underlying crestal bone morphology in the maxillary anterior region. Materials and Methods: The maxillary anterior teeth from 40 subjects (20 thin biotype, 20 thick biotype) with ages from 20 to 50 years were included in this study. All subjects had healthy gingiva in the maxillary anterior region and had no history of orthodontic treatment, periodontal treatment, or hyperplastic medication. Using the probe transparency method, the scalloped distance (SCD) between the contact point-bone crest and the midface-bone crest was measured for each maxillary anterior teeth of two groups. Result: The mean SCD was $3.00{\pm}0.21mm$ in thin biotype and $2.81{\pm}0.20mm$ in thick biotype. The SCD value in the thin biotype was statistically significantly greater than in the thick biotype (t=2.982, P<0.01). Comparing the degree of crestal bone scallop in each maxillary anterior teeth in the two groups, all six teeth in the thin biotype showed higher bone scallop than in the thick biotype. Conclusion: A simple procedure using a probe could to determine gingival biotype and to predict the underlying crestal bone morphology was introduced. This may be useful for effective treatment planning.

• 대한기계학회논문집B
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• 제25권10호
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• pp.1281-1292
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• 2001

Experiments were done for the comparison of performance and flow characteristics between a two -stage axial flow fan and a counter-rotating axial flow fan. Each stage of the two -stage axial flow fan used fur the present study has an eight bladed rotor and thirteen slater blades. The front and the rear rotor of the counter - rotating axial flow fan have eight blades each and are driven by coaxial counter ro latins shafts through a gearbox located between the rear rotor and the electric motor. Both of the two axial fan configurations have identical rotor blades and the same operating condition fur the one -to-one comparison of the two. Performance curves of the two configurations were obtained and compared by varying the blade pitch angles and axial gaps between the blade rows. The fan characteristic curves were obtained following the Korean Standard Testing Methods for Turbo Fans and Blowers (KS B 6311). The fa n flow characteristics were measured using a five-hole probe by a non-nulling method. The velocity profiles between the hub and tip of the fans were measured and analyzed at the particular operating condition s of peak efficiency, minimum and maximum pressure coefficients. The peak efficiency of the counter-rotating axial fan was improved about 2% respectively, compared with the two stage axial fan. At the minimum pressure coefficient point of the two stage axial fan, the fan inlet flow patterns show that axial velocity highly decreased in the vicinity of the blade tip region. Also, the reverse flow took place at the blade tip.

• 한국공작기계학회논문집
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• 제13권6호
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• pp.34-40
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• 2004

This paper presents studies on curvature radius measurement using the laser interferometer. It is a general practice to measure to $10^{-10}$m in length with the recent improvement and innovations in measurement technology and the processor used. The measurement methods can generally be categorized as these two: the contactual method and non-contactual method; and in this study, we will find ways to lower the cost for a CMM, or a coordinate measurement machine, and try to find an alternative. Furthermore, we will discuss some of the ways to improve the non-contactual measurement methods-optical interferometer method and the optical triangulation method. We will measure an object using a laser distance measuring device and Set the Point-contact result with the ball-bearing type and line-contact result with the bearing type, to decide on which probe type will be used.

• Journal of Magnetics
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• 제16권2호
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• pp.169-172
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• 2011

This study reports an alternative method for measuring the magnetoresistance of unpatterned magnetic tunnel junctions similar to the current-in-plane tunneling (CIPT) method. Instead of using microprobes, a series of point contacts with different spacings are coated on the top surface of the junctions and R-H loops at various spacings are then measured by the usual four-point probe method. The values of magnetoresistance and resistance-area products can be obtained by fitting the measured data to the CIPT theoretical model. The test results of two types of junctions were highly similar to those obtained from standard CIPT tools. The proposed method may help to accelerate the process for evaluating the quality of magnetic tunnel junctions when commercial CIPT tools are not accessible.

• 한국정밀공학회지
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• 제10권4호
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• pp.16-29
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• 1993

The objective of this research is in the development of a flexible 3-dimensional inspection system for the sculptured surface by integrating the Coordinate Measuring Machine (CMM), CAD database, and vision system. To achieve the proposed flexible inspection system, two research categories are discussed in the study: new inspection planning method includes a new measuring point selection method and various new probe path generation methods. The object recognition and localization process for the unknown surface can be easily carried out by introducing a new concept called "Z-Layer". The experimental results indicate that the developed flexible inspection system, with the proposed algorithm, can be inplemented in real situation.situation.

• 대한기계학회논문집B
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• 제24권2호
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• pp.288-297
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• 2000

This paper describes the results of an experimental investigation of the flow characteristics and the heat transfer rate on a surface by interaction of a pair of vortices. The test facility consists of a boundary-layer wind tunnel with a vortex introduced into the flow by half-delta wings(vortex generators) protruding from the surface. In order to control the strength of the two longitudinal vortices, the angles of attack of the vortex generators are varied from 20 degree to 45 degree, but spacings between the vortex generators are fixed to 4 cm. The 3-dimensional mean velocity downstream of the vortex generators is measured by a five-hole pressure probe, and the hue-capturing method using the thermochromatic liquid crystals has been used to provide the local distribution of the heat transfer coefficient. By using the method mentioned above, the following conclusions are obtained from the present experiment. The boundary layer is thinned in the regions where the secondary flow is directed toward the wall and thickened where it is directed away from the wall. The peak augmentation of the local heat transfer coefficient occurs in the downwash region near the point of minimum boundary-layer thickness. Streamwise distributions of averaged Stanton number on the measurement planes show very similar trends for all the cases(${\beta}=20^{circ},\;30^{\circ}\;and\;45^{\circ}$).

• 대한기계학회논문집B
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• 제27권11호
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• pp.1618-1629
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• 2003

The effects of the interaction between flow field and heat transfer caused by the longitudinal vortices are experimentally investigated using a five hole probe and a transient liquid crystal technique. The test facility consists of a wind tunnel with vortex generators protruding from a bottom surface and a mesh heater. In order to control the strength of the longitudinal vortices, the angle of attack of vortex generators used in the present experiment is 20$^{\circ}$, and the spacing between the vortex generators is 25mm. The height and cord length of the vortex generator is 20mm and 50mm, respectively. Three-component mean velocity measurements are made using a f-hole probe system, and the surface temperature distribution is measured by the hue capturing method using a transient liquid crystal technique. The transient liquid crystal technique in measuring heat transfer has become one of the most effective ways in determining the full surface distributions of heat transfer coefficients. The key point of this technique is to convert the inlet flow temperature into an exponential temperature profile using the mesh heater set up in the wind tunnel. The conclusions obtained in the present experiment are as follows: The two maximum heat transfer values exist over the whole domain, and as the longitudinal vortices move to the farther downstream region, these peak values show the decreasing trends. These trends are also observed in the experimental results of other researchers to have used the uniform heat flux method.