• Title/Summary/Keyword: Trace analysis

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A Study on Multivariate Tests in the Profile Analysis (프로파일 분석에서의 다변량 검정법 비교 연구)

  • 박진경;박태성
    • The Korean Journal of Applied Statistics
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    • v.12 no.1
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    • pp.97-107
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    • 1999
  • 프로파일 분석은 반복측정 자료를 분석하는데 있어서 널리 사용되는 다변량 분석모형이다. 프로파일 분석에서는 처리 그룹간의 비교와 반응 프로파일의 평행성 검정을 위해서 4가지 검정통계량이 널리 사용되고 있다. 이들 검정통계량은 Wilks의 통계량($\Lambda$), Pillai's Trace 통계량(V), Hotelling-Lawley Trace 통계량(U), Roy's Maximum Root 통계량($\Theta$ )이다. 그 동안 이들 통계량들을 비교하기 위한 여러 연구가 있었지만 주로 일반적인 다변량 분산분석 모형에 근거한 비교였다. 본 논문에서는 자료가 반복측정 자료이고 우리의 관심이 프로파일 분석에 있을 때에 이 4가지 통계량의 비교에 초점을 맞추었다.

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A study on particles flow through gas injection in pot (가스분사를 통한 Pot내에서의 입자 거동연구)

  • Kim Sungsu;Baek Jehyun;Choi Minsuk
    • 한국전산유체공학회:학술대회논문집
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    • 2002.10a
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    • pp.144-149
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    • 2002
  • This paper presents the result of numerical simulation of particles trace following melted zinc movement with nitrogen gas injection. The code of the computational fluid dynamics for numerical analysis was performed using FLUENT related to CFD. As application model, there was applied Eulerian multiphase model for simulation of melted zinc movement at first and then was used stochastic tracking technique for particles trace secondarily. Numerical simulation results are shown that particles move to the same direction as the movement of melted zinc.

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Immobilization of Polysiloxane Liquid Phase on the Gas Chromatographic Solid Supports via In-Situ Cross-Linking

  • Kim, Kyoung-Rae;Zlatkis, Albert
    • Bulletin of the Korean Chemical Society
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    • v.8 no.3
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    • pp.133-137
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    • 1987
  • Polysiloxane SE-54 liquid phase was immobilized on the support surface as coated in thin film via in-situ cross-linking. The cross-linking between liquid molecules was initiated by dicumylperoxide. Among the supports investigated, only Chromosorb W provided the cross-linkable surface. The optimal in-situ cross-linking was achieved when Chromosorb W was coated with 5% (w/w) SE-54 and cross-linked with 1% (w/w) dicumylperoxide. The cross-linked support was useful for the trace analysis as well as for the trace enrichment.

A New On-line Coprecipitation Preconcentration Technique for Trace Metal Analysis by ICP-AES

  • Park, Gyeong Hui;Park, Yong Nam
    • Bulletin of the Korean Chemical Society
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    • v.16 no.5
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    • pp.422-427
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    • 1995
  • In a stream of water sample, trace metal ions are quantitatively coprecipitated with Indium hydroxide and filtered. The filtered precipitate is continuously dissolved in 3 M nitric acid and introduced to ICP directly. The lead, cadmium, and copper are concentrated more than 10-fold and determined with ICP-AES at a sampling frequency of 10/hour. The detection limits are 2.89, 1.43,0.52 ppb for lead, cadmium, and copper respectively. Recoveries of lead, cadmium, and copper are 98.7, 94.3, and 104.5% respectively. The RSD values for three elements are about 3-5% currently.

On-line Trace Enrichment in High Performance Liquid Chromatography Using XAD-2 Precolumn for the Determination of Lonazolac in Human Plasma

  • Lee, Hye-Suk;Kim, Eun-Joo;Zee, Ok-Pyo;Lee, Yoon-Joong
    • Archives of Pharmacal Research
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    • v.12 no.2
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    • pp.108-113
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    • 1989
  • A new column-switching high performance liquid chromatographic method was developed for the determination of lonazolac in plasma. This method was based on the on-line trace enrichment of lonazolac using a precolumn packed with Amberlite XAD-2. The analysis was complete in 20 min. between injections and the limit of detection was $0.1{\mu}g/ml$ using $100{\mu}l$ of plasma. The method was linear in range of $0.1-10{\mu}g/ml$ with a correlation coefficient of 0.9991. Absolute recovery of lonazolac from the spiked plasma samples ranged from 95.6% to 97.1%. The method was shown to be reproducible over the concentration range studied.

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AN ITERATIVE METHOD FOR ORTHOGONAL PROJECTIONS OF GENERALIZED INVERSES

  • Srivastava, Shwetabh;Gupta, D.K.
    • Journal of applied mathematics & informatics
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    • v.32 no.1_2
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    • pp.61-74
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    • 2014
  • This paper describes an iterative method for orthogonal projections $AA^+$ and $A^+A$ of an arbitrary matrix A, where $A^+$ represents the Moore-Penrose inverse. Convergence analysis along with the first and second order error estimates of the method are investigated. Three numerical examples are worked out to show the efficacy of our work. The first example is on a full rank matrix, whereas the other two are on full rank and rank deficient randomly generated matrices. The results obtained by the method are compared with those obtained by another iterative method. The performance measures in terms of mean CPU time (MCT) and the error bounds for computing orthogonal projections are listed in tables. If $Z_k$, k = 0,1,2,... represents the k-th iterate obtained by our method then the sequence of the traces {trace($Z_k$)} is a monotonically increasing sequence converging to the rank of (A). Also, the sequence of traces {trace($I-Z_k$)} is a monotonically decreasing sequence converging to the nullity of $A^*$.

Analysis of Discontinuity Distribution Property to Predict Rock Slope Failure (암반 사면의 파괴 예측을 위한 불연속면 분포 특성 분석)

  • 윤운상;김정환;배기훈
    • Proceedings of the Korean Geotechical Society Conference
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    • 1999.10a
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    • pp.147-152
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    • 1999
  • Distribution of fracture system is an important factor to analyse instability of jointed rock slope. In the most case of rock slopes, joint distribution properties are related to potential, shape, size and locality of slope failure. The purpose of this paper is to present an application of fracture characterization related to rock slope failure. Fracture data used in this study are collected by scanline survey. Two aspects of fracture characterization for rock slope are handled in this study First, In order to determine the potential and shape of slope failure, trace length of joints is considered as the weighting factor about collected orientation data. Second, Relationship between trace length and spacing is analysed to estimate failure location and size. The distribution of fracture system is directly influenced on wedge failure. It is effective to analyse the orientation of fractures by using weighting factors associated with the trace length of fractures rather than to analyse only that of fractures. It gives a conclusion that the wedge failure occurred along the peak of fracture density(or intensity) cycles.

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Toxicological Investigation of Radioactive Uranium in Seawater

  • Ly, Suw-Young;Bae, Jeong-Mi;Kim, Jin
    • Toxicological Research
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    • v.28 no.1
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    • pp.67-71
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    • 2012
  • Trace uranium detection measurement was performed using DNA immobilized on a graphite pencil electrode(DGE). The developed probe was connected to the portable handheld voltammetric systems used for seawater analysis. The sensitive voltammogram was obtained within only 30 s accumulation time, and the anodic stripping working range was attained at 100~800 ${\mu}g/l$ U and 10~50 ${\mu}g/l$. The statistic relative standard deviation of 30.0 mg/l with the $15^{th}$ stripping was 0.2115. Here, toxicological and analytical application was performed in the seawater survey in a contaminated power plant controlling water. The results were found to be applicable for real-time toxicological assay for trace control.