• Archives of Pharmacal Research
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• 제5권2호
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• pp.79-86
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• 1982

Sulfisoxazole, $C-{11}H_{13}N_{3}S$, crystallized in the orthohombic system, space group Pbca, with a = 14.492(1), b = 11.563(1), c = 14.900(2) $\AA$ and Z = 8. Intensities for 1867(1360 observed) unique reflections were measured on a four-circle diffractometer wirh CuKa radiation ($\lambda$ = 1.5418$\AA$). The structure was solved by heavy atom methods and refined by full-matrix least-squares procedures to a final R of 0.094. The benzene ring plane makes an angle of $68^{\circ}C$ with the plane of the isoxazole ring, which is plannar. The conformational angle formed by the torsional angle C(4)-S-N(2)-C(7) is $54^{\circ}C$. There are two intermolecular hydrogen bonds in the structure. One of them is of the type N-H...H with the length 2.915$\AA$. Thus two dimensional networks of hydrogen bonds form infinite moelcular sheets parallel to the (001) plane. Adjacent sheets are bound together by van der Waals forces.

• 대한치과교정학회지
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• 제37권4호
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• pp.293-304
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• 2007

본 연구에서는 임상에서 쓰이는 수종의 치과교정용 세라믹 브라켓에 교정용 호선으로 토오크 적용 시 파절에 저항하는 정도를 비교하고 그 파절 양상을 관찰하였다. $022\;{\times}\;028-inch$ slot을 가진 상악 중절치 세라믹 브라켓에 $0215\;{\times}\;027-inch$ 스테인레스 강 교정용 호선에서 발생하는 설측 치근 토오크를 적용시켜 각 15개씩 7종의 브라켓을 시험하였다. 파절 시험용 장치를 제작하고 토오크 각도를 증가시키면서 만능시험기로 세라믹 브라켓이 파절되는 순간의 토오크 값을 측정하였다. 또한 세라믹 브라켓의 파절 양상을 알아보고자 토오크 값 측정 후 파절이 일어난 부위를 관찰하고 그 위치를 기록한 주사전자현미경으로 파절면을 관찰하였다. 나타난 결과를 토대로 볼 때 세라믹 브라켓의 결정구조와 제조 방법이 파절 저항성에 크게 영향을 주는 것으로 나타났다. 단결정 알루미나 (Inspire) 브라켓이 InVu를 제외한 다결정 알루미나 브라켓에 비하여 토오크에 대한 파절 저항성이 유의성 있게 크게 나타났다 (p < 0.05). Metal slot이 삽입된 브라켓은 그렇지 않은 브라켓과 토오크에 대한 저항성에서 유의한 차이를 보이지 않았다 (p >0.05). 파절 양상에 관한 관찰에서는 metal slot이 있는 다결정 알루미나 브라켓인 Clarity는 모두 절단측 slot base에서 부분적으로만 파절이 일어났고 다른 종류의 브라켓들은 다양한 부위에서 파절이 일어났다. 본 연구 결과, 실험에 사용한 모든 세라믹 브라켓에서 파절이 일어난 순간의 토오크 값과 토오크 각은 실제로 상악 중절치의 치근을 이동하는데 필요한 토오크보다 큰 것이었으므로, 실제 임상 치료 시 적절한 파절 저항을 나타낼 것으로 보였다.

• 한국자기학회지
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• 제27권4호
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• pp.135-139
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• 2017

직경 $190{\mu}m$ Cu 와이어에 $Ni_{80}Fe_{20}$ 연자성 물질을 전기도금법으로 증착하여 금속 코어/연자성 쉘 구조의 복합 와이어를 제작하고 이 와이어에서 자기임피던스 효과(MI 효과)를 연구하였다. 원통 좌표계에서 복합 와이어의 임피던스 텐서의 두 대각 성분 $Z_{{\theta}{\theta}}$와 $Z_{zz}$는 z 방향으로 가한 자기장에 대해 큰 MI 효과를 나타낸 반면, 비대각 임피던스 $Z_{{\theta}z}$의 MI 효과는 매우 약하게 나타났다. 비대각 자기임피던스 효과가 큰 복합 와이어를 만들기 위해 비틀림 스트레인 하에서 전기도금하는 방법을 시도하였다. Cu 와이어의 한쪽 끝을 약 $270^{\circ}$ 이상 회전한 상태에서 전기도금 된 복합 와이어는 뚜렷하게 증대된 비대각 MI 효과를 보였으며 $360^{\circ}$ 회전한 상태에서 도금 된 와이어에서 최대의 비대각 MI 효과를 얻을 수 있었다. 본 연구를 통해 비대각 MI 효과가 큰 복합와이어를 제작하는 방법을 개발한 것은 금속 코어/자성 쉘 복합 와이어의 자기센서 소재로써의 응용가능성을 높일 것으로 기대된다.

• Steel and Composite Structures
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• 제3권4호
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• pp.261-275
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• 2003

Truss members built-up with double angles back-to-back have monosymmetric cross-section and twisting always accompanies flexion upon the onset of buckling about the axis of symmetry. Approximate formulae for calculating the buckling capacity are presented in this paper for routine design purpose. For a member susceptible only to flexural buckling, its optimal cross-section should consist of slender plate elements so as to get larger radius of gyration. But, occurrence of twisting changes the situation owing to the weakness of thin plates in resisting torsion. Criteria for limiting the leg slenderness are discussed herein. Truss web members in compression are usually considered as hinged at both ends for out-of-plane buckling. In case one (or both) end of member is not supported laterally by bracing member, its adjoining members have to provide an elastic support of adequate stiffness in order not to underdesign the member. The stiffness provided by either compression or tension chords in different cases is analyzed, and the effect of initial crookedness of compression chord is taken into account. Formulae are presented to compute the required stiffness of chord member and to determine the effective length factor for inadequately constrained compressive diagonals.

• Earthquakes and Structures
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• 제11권3호
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• pp.421-443
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• 2016

When conducting seismic assessment of an asymmetric building, it is essential to carry out three-dimensional analysis considering all the possible directions of seismic input. For this purpose, the author proposed a simplified procedure is to predict the largest peak seismic response of an asymmetric building subjected to horizontal bidirectional ground motion acting in an arbitrary angle of incidence in previous study. This simplified procedure has been applied to torsionally stiff (TS) asymmetric buildings with regular elevation. However, the suitability of this procedure to estimate the peak response of an asymmetric building with vertical irregularity, such as an asymmetric building with setback, has not been assessed. In this article, the pushover-based simplified procedure is applied to estimate the peak response of asymmetric buildings with bidirectional setback. Nonlinear dynamic (time-history) analysis of two six-storey asymmetric buildings with bidirectional setback and designed according to strong-column weak beam concept is carried out considering various directions of seismic input, and the results compared with those estimated by the proposed method. The largest peak displacement estimated by the simplified method agrees well with the envelope of the dynamic analysis response. The suitability assessment of the simplified procedure to analysed building models is made as well based on pushover analysis results.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2002년도 추계학술대회 논문집
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• pp.355-360
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• 2002

To calibrate a non-redundantly actuated parallel mechanism, one can find actual kinematic parameters by means of geometrical constraint of the mechanism's kinematic structure and measurement values. However, the calibration algorithm for a non-redundant case does not apply fur a redundantly actuated parallel mechanism, because the angle error of the actuating joint varies with position and the geometrical constraint fails to be consistent. Such change of joint angle error comes from constraint torque variation with each kinematic pose (meaning position and orientation). To calibrate a redundant parallel mechanism, one therefore has to consider constraint torque equilibrium and the relationship of constraint torque to torsional deflection, in addition to geometric constraint. In this paper, we develop the calibration algorithm fir a redundantly actuated parallel mechanism using these three relationships, and formulate cost functions for an optimization algorithm. As a case study, we executed the calibration of a 2-DOF parallel mechanism using the developed algorithm. Coordinate values of tool plate were measured using a laser ball bar and the actual kinematic parameters were identified with a new cost function of the optimization algorithm. Experimental results showed that the accuracy of the tool plate improved by 82% after kinematic calibration in a redundant actuation case.

• Wind and Structures
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• 제30권1호
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• pp.55-67
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• 2020

Wind tunnel test is one of the most important means to study the flutter performance of bridges, but there are blockage effects in flutter test due to the size limitation of the wind tunnel. On the other hand, the size of computational domain can be defined by users in the numerical simulation. This paper presents a study on blockage effects of a simplified box girder by computation fluid dynamics (CFD) simulation, the blockage effects on the aerodynamic characteristics and flutter performance of a long-span suspension bridge are studied. The results show that the aerodynamic coefficients and the absolute value of mean pressure coefficient increase with the increase of the blockage ratio. And the aerodynamic coefficients can be corrected by the mean wind speed in the plane of leading edge of model. At each angle of attack, the critical flutter wind speed decreases as the blockage ratio increases, but the difference is that bending-torsion coupled flutter and torsional flutter occur at lower and larger angles of attack respectively. Finally, the correction formula of critical wind speed at 0° angle of attack is given, which can provide reference for wind resistance design of streamlined box girders in practical engineering.

• Earthquakes and Structures
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• 제10권6호
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• pp.1467-1486
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• 2016

This research focuses on seismic performance of a class of single pier skewed bridges with three different pier-deck connections; skew angles vary from $0^{\circ}$ to $60^{\circ}$. A well-documented four span continuous deck bridge has been modeled and verified. Seat-type connections with fixed and sliding bearings plus monolithic pier-deck connections are studied. Shear keys are considered either fully operational or ineffective. Seismic performances of the bridges and the structural components are investigated conducting bidirectional nonlinear time history analysis in OpenSees. Several global and intermediate engineering demand parameters (EDP) have been studied. On the basis of results, the values of demand parameters of skewed bridges, such as displacement and rotation of the deck plus plastic deformation and torsional demand of the piers, increase as the skew angle increases. In order to eliminate the deck collapse probability, the threshold skew angle is considered as $30^{\circ}$ in seat-type bridges. For bridges with skew angles greater than $30^{\circ}$, monolithic pier-deck connections should be applied. The functionality of shear keys is critical in preventing large displacements in the bearings. Pinned piers experience considerable ductility demand at the bottom.

• Steel and Composite Structures
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• 제10권4호
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• pp.297-315
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• 2010

This paper is concerned with free vibration characteristics and natural frequency of horizontally curved composite plate girder bridges. Three-dimensional finite element models are developed for the girders using the software package LUSAS and analyses carried out on the models. The validity of the finite element models is first established through comparison with the corresponding results published by other researchers. Studies are then carried out to investigate the effects of total number of girders, number of cross-frames and curvature on the free vibration response of horizontally curved composite plate girder bridges. The results confirm the fact that bending modes are always coupled with torsional modes for horizontally curved bridge girder systems. The results show that the first bending mode is influenced by composite action between the concrete deck and steel beam at low subtended angle but, on the girders with larger subtended angle at the centre of curvature such influence is non-existence. The increase in the number of girders results in higher natural frequency but at a decreasing rate. The in-plane modes viz. longitudinal and arching modes are significantly influenced by composite action and number of girders. If no composite action is taken into account the number of girders has no significant effect for the in-plane modes.

• Structural Engineering and Mechanics
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• 제82권4호
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• pp.517-542
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• 2022

The effect of mean angle of wind attack on the flutter critical wind speed of two generic bridge deck cross-sections, viz, one closed box type streamlined section (deck-1) and closed box trapezoidal bluff type section with extended flanges/overhangs (deck-2) type of section have been studied using Computational Fluid Dynamics (CFD) based forced vibration simulation method. Owing to the importance of the effect of the amplitude of forcing oscillation on the flutter onset, its effect on the flutter derivatives and flutter onset have been studied, especially at non-zero mean angles of wind attack. The flutter derivatives obtained have been used to evaluate flutter critical wind speeds and flutter index of the deck sections at non-zero mean angles of wind attack studied and the same have been validated with those based on experimental results reported in literature. The value of amplitude of forcing oscillation in torsional degree of freedom for CFD based simulations is suggested to be in the range of 0.5° to 2°, especially for bluff bridge deck sections. Early onset of flutter from numerical simulations, thereby conservative estimate of occurrence of instability has been observed from numerical simulations in case of bluff bridge deck section. The study aids in gaining confidence and the extent of applicability of CFD during early stages of bridge design, especially towards carrying out studies on mean incident wind effects.