• 분석과학
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• 제24권3호
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• pp.231-235
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• 2011

A spectrofluorimetric method for the determination of EDTA in real samples such as mayonnaise, powder detergent and cleansing cream with tiron (4,5-dihydroxy-1,3-benzenedisulfonic acid) as a fluorimetric reporter was developed. When tiron is chelated with Cu(II), the fluorescent intensity is decreased by a quenching effect. However, when Cu(II)-tiron chelate reacts with EDTA, fluorescent intensity is increased as tiron is released. Several experimental conditions such as pH of the sample solution, the amount of Cu(II), the amount of tiron, heating temperature and heating time were optimized. Fe(III) interfered more seriously than any other ions, interference of Fe(III) could be disregarded, because Fe(III) was scarcely contained in selected real samples. The linear range of EDTA was from $8.0{\times}106{-8}\;M$ to $2.0{\times}10^{-6}\;M$. With this proposed method, the detection limit of Fe(III) was $5.2{\times}10^{-8}\;M$. Recovery yields of 92.7~99.3% were obtained. Based on experimental results, it is proposed that this technique can be applied to the practical determination of EDTA.

• 전기화학회지
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• 제3권4호
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• pp.232-234
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• 2000

전기화학적인 방법으로 요산을 정량함에 있어서 전극의 활성을 증가시키기 위하여 초음파를 조사하여 요산의 정량을 시도하였다. 요산의 정량의 최적조건을 조사하기 위하여 초음파의 세기, 시간, 전해질 용액의 pH, 온도 등의 영향을 조사하였고 전극의 안정성에 대해서도 조사하였다. 최적 조건은 $25.0^{\circ}C$, pH 7.0,초음파의 파워 $20W/cm^2$의 조건이었으며 $8.0{\times}10^{-6}\~5.0\times10^{-4}M$의 직선범위를 가졌고, 검출한계는 $6.5\times10^{-6}M$이었다.

• KSII Transactions on Internet and Information Systems (TIIS)
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• 제10권10호
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• pp.4933-4956
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• 2016

Use-After-Free (UAF) is a common lethal form of software vulnerability. By using tools such as Web Browser Fuzzing, a large amount of samples containing UAF vulnerabilities can be generated. To evaluate the threat level of vulnerability or to patch the vulnerabilities, automatic deduplication and exploitability determination should be carried out for these samples. There are some problems existing in current methods, including inadequate pertinence, lack of depth and precision of analysis, high time cost, and low accuracy. In this paper, in terms of key dangling pointer and crash context, we analyze four properties of similar samples of UAF vulnerability, explore the method of extracting and calculate clustering eigenvalues from these samples, perform clustering by fast search and find of density peaks on a large number of vulnerability samples. Samples were divided into different UAF vulnerability categories according to the clustering results, and the exploitability of these UAF vulnerabilities was determined by observing the shape of class cluster. Experimental results showed that the approach was applicable to the deduplication and exploitability determination of a large amount of UAF vulnerability samples, with high accuracy and low performance cost.

• Bulletin of the Korean Chemical Society
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• 제17권11호
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• pp.995-999
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• 1996

A method for the determination of cobalt(Ⅱ) by differential pulse voltammetry using a carbon paste electrode constructed by incorporating 1-(2-pyridylazo)-2-naphthol(PAN) into a conventional carbon paste mixture composed of graphite powder and Nujol oil has been developed. Several influencing factors for the determination of cobalt(Ⅱ) were studied in detail and the optimum analytical conditions were found to be as follows: pH, 4.6; composition of electrode, 20%; temperature of deposition, 43 ℃; time of preconcentration, 15 min. Regeneration of the electrode surface for the continuous uses of the electrode was achieved by exposing the carbon paste electrode to an acidic solution. Response of the electrode was reproducible for the uses of five times and the relative standard deviations were 6.7 and 4.6% for 2.0×10-5 M and 4.0×10-6 M cobalt(Ⅱ), respectively. The calibration curve for cobalt(Ⅱ) obtained by differential pulse voltammetry was divided into two linear ranges of 1.7× 10-6-1.3×10-4 M and 2.0×10-7-8.0×10-7 M. The detection limit was estimated to be 1.3×10-7 M. The effects of coexisting ions were also investigated to test the applicability of the proposed method to the determination of cobalt(Ⅱ) in real samples.

• 한국토양비료학회지
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• 제43권6호
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• pp.1008-1011
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• 2010

A method currently used to determine soil organic matter (SOM), Tyurin method, is time consuming and expensive while accurate. Recently, a spectrophotometric determination was reported to be rapid, accurate, stable, easy to execute, and amendable to field use for soil samples obtained from Texas, USA. The objective of this study was to test if the spectrophotometric method is applicable to soils in Korea. Soil organic matter was extracted by 1 M HCl followed by a 0.25 M NaOH-0.1 M sodium pyrophosphate solution at a ratio of 1:250 soil:extractant. Soil organic matter determined by Tyurin method was linearly related to the value based on absorbance at 300 nm of the soil extracts with a coefficient of determination ($r^2$) of 0.81. Therefore, the result imply that this spectrophotometric method can be used to determine the soil organic matter of agricultural soils in Korea.

• 대한교통학회지
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• 제26권4호
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• pp.217-227
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• 2008

이용자가 수용 가능한 환승시간 및 환승거리의 결정은 환승시스템을 계획하는 단계에서 가장 우선적으로 고려되어야 한다. 환승 자체가 불가능한 경우, 환승시스템 구성요소의 개선은 환승을 선택하는데 있어서 전혀 영향을 주지 못한다. 한계환승도보거리는 이용자의 처음교통수단에서 다음 교통수단까지의 합리적인 도보거리와 대기시간으로 결정되어져야한다. 대중교통 네트워크나 환승시스템 계획단계에서 환승서비스 권역을 좀 더 현실적으로 결정하기 위해서는 이용자 속성이 고려되어야 한다. 따라서 본 연구에서는 환승에 초점을 맞추어 이루어 졌으며, 대중교통 이용자 인적속성에 따라 수용하는 환승거리와 시간이 다를 것이라는 가정을 한 후 대중교통 이용자 인적속성에 따라 환승시간별 환승률 산정 모형을 개발을 하는것을 목적으로 하였다. 이 중 한계환승시간과 상관관계가 높고, 환승시간에 따른 명확한 차이가 있는 성별, 월평균 수입별, 대중교통 환승횟수로 한정하여 환승시간별 환승률, 환승거리별 환승률의 결정모형을 개발하였다.

• 한국농업기계학회:학술대회논문집
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• 한국농업기계학회 2000년도 동계 학술대회 논문집
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• pp.457-463
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• 2000

• 한국농업기계학회:학술대회논문집
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• 한국농업기계학회 1998년도 동계 학술대회 논문집
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• pp.368-373
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• 1998

• 한국우주과학회:학술대회논문집(한국우주과학회보)
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• 한국우주과학회 2004년도 한국우주과학회보 제13권2호
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• pp.59-59
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• 2004

• Bulletin of the Korean Chemical Society
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• 제23권12호
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• pp.1816-1818
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• 2002