• Title/Summary/Keyword: Thermosetting Composite

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Cure Monitoring of Composite Materials Using Dielectrometry (유전기법을 이용한 복합재료의 경화 모니터링)

  • 권재욱;김진국;김학성;이대길;최진경
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2000.11a
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    • pp.42-45
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    • 2000
  • The properties of thermosetting resins are dependent on the degree of cure and consolidation quality. Since the consolidation process of thermosetting resin matrix fiber composites is much dependent on the viscosity of resin in the composites, in this study, the dissipation factor which is a function of viscosity was measured by the newly developed Lacomtech dielectrometry apparatus and sensors. Using the measured dissipation factors, the relationship between the dissipation factor and degree of cure with respect to environmental temperature was investigated.

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Burst capacity of pipe under corrosion defects and repaired with thermosetting liner

  • Akram, Ali;Mustaffa, Zahiraniza;Albarody, Thar M. Badri
    • Steel and Composite Structures
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    • v.35 no.2
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    • pp.171-186
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    • 2020
  • This paper aims at providing insights on the use of thermosetting liner for the repair of offshore pipelines exposed to corrosion and leakage. The work which covers both experimental and numerical approaches were aspired due to the high cost of repair for pipelines, limitations of thermoplastic material and limited study of reinforced thermosetting liner. The experiment involves a destruction test called the burst test, carried out on an API 5L X42 carbon steel pipe under four case studies, namely (i) intact pipe, (ii) pipe with corrosion defect, (iii) pipe with corrosion defect and repaired with thermosetting liner and (iv) pipe with leakage and repaired with thermosetting liner. The numerical simulation was developed to first validate the experimental results and later to optimize the design of the thermosetting liner in terms of the number of layers required to restore the original strength of the pipe. The burst test shows an improvement in 23% of the burst capacity for the pipe with corrosion defects, after being repaired with a three-layer thermosetting liner. The parametric studies conducted showed that with an addition of thermosetting layers, the burst capacity improves by an average of 1.85 MPa. In conclusions, the improvement in strength can be further increased with increasing thickness of the thermosetting liner. The thermosetting liner was also determined to fail first inside the host pipe.

A New Cure Kinetic Model Using Dynamic Differential Scanning Calorimetry (일정온도 상승률 열분석법을 이용한 수지 경화 모델 개발)

  • Eom, Mun-Gwang;Hwang, Byeong-Seon;Isaac M. Daniel
    • 연구논문집
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    • s.29
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    • pp.151-162
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    • 1999
  • In general, manufacturing processes of thermosetting composites consist of mold filling and resin cure. The important parameters used in modeling and designing mold filling are the permeability of the fibrous preform and the viscosity of the resin. To consolidate a composite, resin cure or chemical reaction plays an essential role. Cure kinetics. Therefore, is necessary to quantify the extent of chemical reaction or degree of cure. It is also important to predict resin viscosity which can change due to chemical reaction during mold filling. There exists a heat transfer between the mold and the composite during mold filling and resin cure. Cure kinetics is also used to predict a temperature profile inside composite. In this study, a new scheme which can determine cure kinetics from dynamic temperature scaning was proposed. The method was applied to epoxy resin system and was verified by comparing measurements and predictions.

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Study on the Improvement of Epoxy Property for Aluminum Conductor Composite Core (복합재료 중심인장선용 에폭시 물성 개선 연구)

  • Heo, Seok-Bong;Kang, Junyoung;Youn, Young-Gil;Goh, Munju;Kim, Nam Hoon
    • Composites Research
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    • v.32 no.6
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    • pp.349-354
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    • 2019
  • The Aluminum conductor composite core consists of fast-curing thermosetting epoxy used as reinforcements and carbon fiber and glass fiber used as matrix. In this study, we have investigated fast curing epoxy cured products used for composite core(Aluminum Conductor Composite Core, ACCC). Tetrafunctional epoxy(PA 806) was used as a multifunctional epoxy, along with two kinds of curing agents, MNAn(5-Methyl-5-norbornene-2,3-dicarboxylic anhydride) and HHPA(Hexahydrophthalic Anhydride), to make an epoxy cured product and their properties were evaluated. Optimum conditions are confirmed by varying the content of curing accelerator in the selected epoxy and curing agent.

Fabrication and Characterization of Carbon Long-Fiber Thermoplastic Composites using the LFT-D System (LFT-D 시스템을 이용한 탄소 장섬유 열가소성 복합재의 제조 및 인장특성 분석)

  • Shin, Yujeong;Jeung, Han-Kyu;Park, Si-Woo;Park, Dong-Wook;Park, Yeol;Jung, Jin-Woo
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.16 no.5
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    • pp.25-30
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    • 2017
  • Carbon-fiber-reinforced plastic (CFRP) composite materials have been widely used in various industrial fields because the design variables can be adjusted according to the application of the required structure. Thermosetting and thermoplastic resins are used as the base materials of CFRP composites for the lightweight construction of automotive components. Thermoplastics have several advantages such as no curing and recyclability compared to thermosetting resin. In this study, CFRP composites were made using the Long-Fiber Thermoplastic-Direct (LFT-D) process. The LFT-D process includes an in-line production system that directly impregnates a thermoplastic resin, extrudes the composite material, and molds it. This process increases the strength and decreases the molding time. The tensile strength characteristics on the mechanical properties of CFRP were analyzed according to the parameters of LFT-D based on thermoplastics. To analyze the properties of CFRP, the specimens were prepared based on the tensile test standard ASTM 3039 of composite materials.

Research of Thermal Properties for Liquid Crystalline Epoxy Composites with Tin Oxide Filler (산화주석을 함유한 열경화성 액정 에폭시의 열적 특성에 관한 연구)

  • Hyun, Ha Nuel;Cho, Seung Hyun
    • Composites Research
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    • v.33 no.1
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    • pp.25-29
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    • 2020
  • A liquid crystalline thermosetting-epoxy-based composite was fabricated using diglycidyl ether of 4,4'-biphenol, tin(IV) oxide as a filler, and sulfanilamide as a curing agent. To investigate the thermal behavior, Thermogravimetric Analysis and Laser Flash Apparatus were performed using 3.0-7.0 wt% Tin(IV) oxide. The result showed that the activation energy and thermal conductivity were proportional to the amount of added filler.

A Preliminary Study on Fatigue Strength of High Toughness Thermoplastic Composite Material AS4/PEEK (고인성 열가소성 복합재료 AS4/PEEK의 피로강도에 관한 기초적 검토)

  • Song, Ji-Ho;Gang, Jae-Yun
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.24 no.4 s.175
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    • pp.1055-1064
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    • 2000
  • First, various specimen geometries, namely, coupon type, waisted type and dog-bone type, were examined to determine appropriate fatigue specimen of thermoplastic composite material AS4/PEEK and the n, fatigue strength of smooth and notched specimens of AS4/PEEK [-45/0/+45/90]2s was investigated. Fatigue tests were performed under load controlled condition at a stress ratio of 0. 1 at a frequency of 5Hz. Stiffness degradation of specimens with fatigue cycling was monitored using an automated unloading compliance technique. The waisted type specimen is found appropriate for smooth fatigue specimen geometry of AS4/PEEK. As for the effect of stress concentration, it is found that fatigue strength is higher for a 2mm-diameter hole notched specimen than a 5mm-diameter one. Fatigue notch factor decreases with the increase of fatigue life. These results are far different from the trend of fatigue strength of metallic materials. The stiffness variation of smooth specimen was only 4% at maximum until final fracture. On the other hand, the stiffness of hole notched specimen was reduced by 45% at maximum. Notched fatigue strength was compared between thermoplastic composite AS4/PEEK and thermosetting composite Graphite/Epoxy. In long-life fatigue (>104), the AS4/PEEK composite shows superior fatigue strength, but in short-life fatigue, the fatigue strength of the Graphite/Epoxy composite is nearly equal or somewhat higher than that of the AS4/PEEK composite.

Dielectric Cure Monitoring of Thermosetting Matrix Composites (열경화성 수지 복합재료의 유전 정화 모니터링)

  • Kim, Hyoung-Geun;Lee, Dai-Gil
    • Journal of the Korean Society for Nondestructive Testing
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    • v.23 no.5
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    • pp.409-417
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    • 2003
  • Cure monitoring can be used to improve the quality and productivity of thermosetting resin matrix composite products during their manufacturing process. In this work, the sensitivity of dielectrometry was improved by adequate separation the efforts of sensor and externals on the measured signal. A new algorithm to obtain the degree of cure during dielectric cure monitoring of glass/polyester and glass/epoxy composites was developed by employing a function of both temperature and dissipation factor, in which five cure monitoring parameters were used to calculate the degree of cure. The decreasing pattern of dissipation factor was compared with the relationships between the degree of cure and the resin viscosity. The developed algorithm might be employed for the in situ cure monitoring of thermosetting resin composites.

Manufacture of arrester module using braided composite materials (브레이드 복합재료를 이용한 피뢰기 모듈 제조에 관한 연구)

  • Han, D.H.;Cho, H.G.;Han, S.W.;Park, K.H.
    • Proceedings of the KIEE Conference
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    • 2002.07c
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    • pp.1467-1469
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    • 2002
  • This paper aims to investigate the characteristics of braided thermoplastic and thermosetting composite and pressure relief for polymer arrester. In general, braided composite has potential for improved impact and delamination resistance. Manufacturing processes of the braided composite could also be automated and could potentially lead to lower costs. Therefore, in consideration of characteristics of pressure relief for polymer arrester, the fabric pattern of braided composite was studied. And polymer arrester module was manufactured with braid.

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