• 한국세라믹학회지
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• 제42권12호
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• pp.821-826
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• 2005

Gadolinia-doped ceria nanopowder was prepared by glycine-nitrate combustion method with different glycine/nitrate mixing ratio. The characteristics of the synthesized powder were investigated by X-ray diffraction method, transmission electron microscopy, thermal gravity, differential thermal analysis and thermo-mechanical analysis. The smallest powder was obtained with glycine/nitrate ratio 1.00 and the lowest organic and water vapor contained powder was made with glycine/nitrate ratio 1.75. According to dilatometry, fast densification was occurred around $1000^{\circ}C$ and shows full density over $1300^{\circ}C$. Finally near-fully dense ceria electrolyte was fabricated with conventional sintering technique. Glycine-nitrate process yields fine nanopowders which enable low temperature sintering and fabrication of fully dense and nanostructured oxide electrolyte.

• 한국추진공학회지
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• 제20권6호
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• pp.61-69
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• 2016

본 연구는 이중 선회 가스터빈 연소기에서 연소실 길이와 열용량을 변수로 연소불안정 현상과 관련된 결과이다. 특히 열용량이 상대적으로 작은 구간에서 연소실 길이가 길어지면 공진 주파수의 값이 일정하게 유지되는 맥놀이 현상이 발생하는 것이 확인되었다. 이러한 맥놀이 현상은 메인 화염과 파일럿 화염이 각각 다른 주기로 거동하기 때문에 발생되었으며, 연소실 길이가 증가하여도 주파수의 값이 변하지 않는 현상은 메인 화염과 파일럿 화염의 서로 다른 상호작용 결과라고 판단된다.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2008년도 추계학술대회B
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• pp.2738-2743
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• 2008

We conducted a study by computational simulation about the effects of frost thickness on the pressure drop and heat transfer characteristics as whole heat exchanger configuration changes. In order to perform the analysis for validation, we assumed that frost properties have constant values and the frost layers that are formed on the fin and tube surfaces are uniform. In order to find the constant thermal conductivity of frost layer, a variety of frost thermal conductivities are performed in our work and compared with the results by Lee et al. [4] and Yang et al. [5] proposed many experimental data about the 2-rows and 2-columns finned tube heat exchanger. The numerical results agreed well with the experimental data when frost conductivity is 0.07W/mK. After the validation had performed, we applied this procedure to the finned tube heat exchanger of domestic refrigeration and investigated the thermo-hydraulic characteristic of the heat exchanger affected by frost thickness according to the inlet velocities and temperatures of air considering the configuration change such as fin pitch.

• Computers and Concrete
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• 제23권5호
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• pp.321-327
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• 2019

Experimental isotherm compressive tests show that concrete behaviour is dependent on temperature. The aim of such tests is to reproduce how concrete will behave under environmental changes within a moderate range of temperature. In this paper, a novel constitutive elastic damage behaviour law is proposed based on a free energy with an apparent damage depending on temperature. The proposed constitutive behaviour leads to classical theory of thermo-elasticity at small strains. Fixed elastic mechanical characteristics and fixed evolution law of damage independent of temperature and the material volume element size are considered. This approach is applied to compressive tests. The model predicts compressive strength and secant modulus of elasticity decrease as temperature increases. A power scaling law is assumed for specific entropy as function of the specimen size which leads to a volume size effect on the stress-strain compressive behaviour. The proposed model reproduces theoretical and experimental results from literature for tempertaures ranging between $20^{\circ}C$ and $70^{\circ}C$. The effect of the difference in the coefficient of thermal expansion between the mortar and coarse aggregates is also considered which gives a better agreement with FIB recommendations. It is shown that this effect is of a second order in the considered moderate range of temperature.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2009년도 하계학술대회 논문집
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• pp.412-412
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• 2009

Carbon-based nano materials have a significant effect on various fields such as physics, chemistry and material science. Therefore carbon nano materials have been investigated by many scientists and engineers. Especially, since graphene, 2-dimemsonal carbon nanostructure, was experimentally discovered graphene has been tremendously attracted by both theoretical and experimental groups due to their extraordinary electrical, chemical and mechanical properties. Electrical conductivity of graphene is about ten times to that of silicon-based material and independent of temperature. At the same time silicon-based semiconductors encountered to limitation in size reduction, graphene is a strong candidate substituting for silicon-based semiconductor. But there are many limitations on fabricating large-scale graphene sheets (GS) without any defect and controlling chirality of edges. Many scientists applied micromechanical cleavage method from graphite and a SiC decomposition method to the fabrication of GS. However these methods are on the basic stage and have many drawbacks. Thereupon, our group fabricated GS through Thermo-electrical Pulse Induced Evaporation (TPIE) motivated by arc-discharge and field ion microscopy. This method is based on interaction of electrical pulse evaporation and thermal evaporation and is useful to produce not only graphene but also various carbon-based nanostructures with feeble pulse and at low temperature. On fabricating GS procedure, we could recognize distinguishable conditions (electrical pulse, temperature, etc.) to form a variety of carbon nanostructures. In this presentation, we will show the structural properties of OS by synthesized TPIE. Transmission Electron Microscopy (TEM) and Optical Microscopy (OM) observations were performed to view structural characteristics such as crystallinity. Moreover, we confirmed number of layers of GS by Atomic Force Microscopy (AFM) and Raman spectroscopy. Also, we used a probe station, in order to measure the electrical properties such as sheet resistance, resistivity, mobility of OS. We believe our method (TPIE) is a powerful bottom-up approach to synthesize and modify carbon-based nanostructures.

• 마이크로전자및패키징학회지
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• 제17권4호
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• pp.61-66
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• 2010

3차원 TSV 접합 시접합 두께 및 전, 후 추가 공정 처리가 Cu-Cu 열 압착 접합에 미치는 영향을 알아보기 위해 0.25, 0.5, 1.5, 3.0 um 두께로 Cu 박막을 제작한 후 접합 전 $300^{\circ}C$에서 15분간 $Ar+H_2$, 분위기에서 열처리 후 $300^{\circ}C$에서 30분 접합 후 후속 열처리 효과를 실시하여 계면접착에너지를 4점굽힘 시험법을 통해 평가하였다. FIB 이미지 확인 결과 Cu 두께에 상관없이 열 압착 접합이 잘 이루어져 있었다. 계면접착에너지 역시 두께에 상관없이 $4.34{\pm}0.17J/m^2$ 값을 얻었으며, 파괴된 계면을 분석 한 결과 $Ta/SiO_2$의 약한 계면에서 파괴가 일어났음을 확인하였다.

• International Journal of Aeronautical and Space Sciences
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• 제17권4호
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• pp.518-525
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• 2016

This paper presents the characteristics of non-fundamental multi-mode combustion instability and the effects of high-harmonic components on the Rayleigh criterion. Phenomenological observations of multi-harmonic-mode dynamic pressure waves regarding the intensity of harmonic components and the source of wave distortion have been explained by introducing examples of second- and third-order harmonics at various amplitudes. The amplitude and order of the harmonic components distorted the wave shapes, including the peak and the amplitude, of the dynamic pressure and heat release, and consequently the temporal Rayleigh index and its integrals. A cause-and-effect analysis was used to identify the root causes of the phase delay and the amplification of the Rayleigh index. From this analysis, the skewness of the dynamic pressure turned out to be a major source in determining whether multi-mode instability is driving or damping, as well as in optimizing the combustor design, such as the mixing length and the combustor length, to avoid unstable regions. The results can be used to minimize errors in predicting combustion instability in cases of high multi-mode combustion instability. In the future, the amount of research and the number of applications will increase because new fuels, such as fast-burning syngases, are prone to generating multi-mode instabilities.

• 대한기계학회논문집A
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• 제36권11호
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• pp.1297-1303
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• 2012

본 논문에서는 PET(Polyethylene Terephthalate)와 같은 박막 형태의 고분자 소재에서 수분 확산을 특성화 하기 위한 표준 과정을 열 중량법을 사용하여 제시하고 소재의 흡습 물성을 정량적으로 얻었다. 온도 및 습도에 대한 흡습 물성들의 영향을 조사하기 위해 아레니우스(Arrhenius) 식에 따른 PET 필름의 용해성과 확산성을 특성화 하였다. Fickian 확산에 기반한 박막 소재의 수분 투과성을 구하여 열중량법에서 얻은 흡습 물성의 타당성을 토론하였다. 고분자 소재가 금속과 같은 무기물과 다층 경계면을 가지는 경우 농도에 의존적인 비선형 수분 확산성의 특성을 실험적으로 조사하였고 Non-Fickian 모델에 따른 비선형 확산 특성을 수치적으로 정량화 하였다. 얻어진 흡습 물성들에 기반한 Fickian/Non-Fickian 모델에 대해 수치적으로 비교 및 토론 하였다.

• 대한기계학회논문집B
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• 제24권8호
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• pp.1038-1045
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• 2000

An experimental study was carried out to delineate the flow characteristics in a closed countescurrent two-phase thermo syphon with concentric tubes. This is to be installed in the HANARO research reactor as a part of a Cold Neutron Source(CNS). In the present investigation, experiments ata room temperature with Freon-II3 as a moderator were performed. Results show that, based on the magnitude of pressure fluctuation, the flow regimes could be divided into 4 distinct ones in the ($V_f,\;Q_i$) plane, where $V_f$ represents the volume of the charged liquid and $Q_i$ the heat load: a stable flow regime, an oscillatory flow regime, a restablized flow regime and a dryout flow regime. For $V_f$>2.5l, the flow is stable at low $Q_i$. However, as $Q_i$ increases, the flow becomes oscillatory and finally restablizes As $V_f$ increases, the oscillation amplitude decreases, reaching to the restablized flow region at low $Q_i$, and the liquid level in the moderator cell remains high. In the oscillatory flow regimes, for a fixed VI; the oscillating period of time varies with $Q_i$, having a minimum value at a certain value of $Q_i$. The heat load, where the oscillating period of time is minimum, decreases as $V_f$ increases.

• 동력기계공학회지
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• 제18권4호
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• pp.43-51
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• 2014

In this paper, transient temperature and vibration characteristics of a brushless DC (BLD(c) motor are studied for external load (165W~495W) and rotational speed (2000 rpm~4000 rpm). For experiment, a simple measurement system is developed to allow a change in load and speed for measuring transient temperature and vibration simultaneously. Temperature and vibration were also measured under the conditions of natural convection and forced convection. Vibrations in the directions of x-axis (#Ch1), y -axis (#Ch2) and z -axis (#Ch3) were obtained by three accelerometers and temperature was obtained by a thermo-couple with respect to time until the motor is steady. Experimental results show that the amplitude of vibration is higher in the order of z-axis (#Ch3), x -axis (#Ch1) and y-axis (#Ch2) and the amplitude of vibration at the forced convection conditions is 10.6% to 17.8% lower than that of vibration at the natural convection. However, the ratio of the vibration value is similar on average regardless of external convection condition.