• Korean Journal of Materials Research
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• v.3 no.2
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• pp.166-174
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• 1993

Abstract The crack resistance of PSG(Phosphosilicate Glass) and PE-SiN(Plasma Enhanced CVD S${i_2}{N_4}$)films deposited on aluminium thin films on Si substrate was analyzed in this study. PSG was deposited by AP-CVD and PE- SiN by PE-CVD. All the films underwent repeated heat cycles at 45$0^{\circ}C$for 30 min. Crack formation and development were examined between each heat cycle. The crack behavior was found to be closely related to the stresses in the films. The stress induced by the difference in thermal expansion behavior between the passivation layers and underlying aluminum film may cause the crack. Crack resistance decreases as the thickness of PSG films increases due to the high tensile stress of the films. Phosphorus in the PSG films releases tensile stress and consequently the stress of the films tends to show compressive stress. As a result, crack resistance increased as the concentratin of P in the PSG films increased. Crack resistance in the PE-SiN films also increased with compressive stress. An experimental model to predict crack generation in the PSG and PE-SiN films during heat cycle was suggested.

• Journal of the Microelectronics and Packaging Society
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• v.6 no.2
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• pp.23-30
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• 1999

The relationships between morphological structures and residual stress behaviors of polyimide thin films depending on isomeric diamines were investigated. For this study, Poly(phenylene biphenyltetracarboximide) (BPDA-PDA) and poly(oxydiphenylene biphenyltetracarboximide) (BPDA-ODA) films were prepared from their isomeric diamines: 1,3-phenylene diamine (1,3-PDA) 1,4-phenylene diamine (1.4-PDA), 3,4'-oxydiphenylene diamine (3,4'-ODA), and 4,4'-oxydiphenylene diamine (4,4'-ODA), respectively. For those films, residual stresses were detected in-situ during thermal imidization of the isomeric polyimide as a function of processing temperature over the range of 25~$400^{\circ}C$ using. Thin Film Stress Analyzer (TFSA). In comparison, residual stress of BPDA-1.4PDA having better in-plain orientation and chain order was the lowest value of 7MPa whereas those of BPDA-1,3-PDA, BPDA-3,4'-ODA, and BPDA-4,4'-ODA were in the range of 40-50MPa. Conclusively, the effect of morphological nature (chain rigidity, chain order, orientation) and chain mobility relating to the g1ass transition behavior on the residual stress of isomeric polyimide thin films wart analyzed.

• Journal of Welding and Joining
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• v.1 no.2
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• pp.45-52
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• 1983

Many pressure vessels for the hot H$\sub$2//H$\sub$2/S service are made of 2+1/4Cr-1Mo steel with austenitic stainless steel overlay to combat agressive corrosion due to hydrogen sulfide. Hydrogen dissolves in to materials during operation, and sometimes gives rise to unfore-seeable damages. Appropriate precautions must, therefore, be taken to avoid the hydrogen induced damages in the design, fabrication and operation stage of such reactor vessels. Recently, hydrogeninduced cracking (or Disbonding) was found at the interface between base metal and stainless weld overlay of a desulfurizing reactor. Since the stainless steel overlay weld metal is subjected to thermal and internal-pressure loads in reactor operation, it is desirable for the overlay weld metal to have high strength and ductility from the stand point of structural safety. In section III of ASME Boiler and Pressure Vessel Code, Post-Weld Heat Treatment(PWHT) of more than one hour per inch at over 1100.deg. F(593.deg. C) is required for the weld joints of low alloy pressure vessel steels. This heat treatment to relieve stresses in the welded joint during construction of the pressure vessel is considered to cause sensitization of the overlay weld metal. The present study was carried out to make clear the diffusion of carbon migration by PWHT in dissimilar metal welded joint. The main conclusion reached from this study are as follows: 1) The theoretical analysis for diffusion of carbon in stainless steel overlay weld metal does not agree with Fick's 2nd law but the general law of molecular diffusion phenomenon by thermodynamic chemical potential. 2) In the stainless steel overlay welded joint, the PWHT at 720.deg. C for 10 hours causes a diffusion of carbon atoms from ferritic steel into austenitic steel according to the theoretical analysis for carbon migration and its experiment. 3) In case of PWHT at 720.deg. C for 10 hours, the micro-hardness of stainless steel weld metal in bonded zone increase very highly in the carburized layer with remarkable hardening than that of weld metal.

• Transactions of Materials Processing
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• v.23 no.5
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• pp.289-296
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• 2014

Uniaxial tensile tests were conducted to accurately evaluate the in-plane mechanical properties of fiber metal laminates (FMLs). The FMLs in the current study are comprised of a layer of self-reinforced polypropylene (SRPP) sandwiched between two layers of aluminum alloy 5052-H34. The nonlinear tensile behavior of the FMLs under in-plane loading conditions was investigated using both numerical simulations and a theoretical analysis. The numerical simulation was based on finite element modeling using the ABAQUS/Explicit code and the theoretical constitutive model was based on the volume fraction approach using the rule of mixture and a modification of the classical lamination theory, which incorporates the elastic-plastic behavior of the aluminum alloy and the SRPP. The simulations and the model are used to predict the inplane mechanical properties such as stress-strain response and deformation behavior of the FMLs. In addition, a post-stretching process is used to reduce the thermal residual stresses before uniaxial tensile testing of the FMLs. Through comparison of both the numerical simulations and the theoretical analysis with the experimental results, it is concluded that the numerical simulation model and the theoretical approach can describe with sufficient accuracy the actual tensile stress-strain behavior of the FMLs.

• Bulletin of the Society of Naval Architects of Korea
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• v.11 no.1
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• pp.35-44
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• 1974

열박음(shrink fitting)으로 인(因)한 동심형(同心形) 구멍을 가진 복합(複合)실린더의 과도적(過渡的) 온도분포(溫度分布), 열응력(熱應力) 및 열변형도(熱變形度)를 이론해석(理論解析)하였다. 온도분포해석(溫度分布解析)에서 외부(外部) 실린더는 균일온도(均一溫度)로 가열(加熱)되어, 실온(室溫)의 내부(內部) 실린더와 접촉면(接觸面)에서 일어나는 열전도(熱傳導)에 의(依)하여 냉각(冷却)되고, 외부(外部) 표면(表面)은 대기중(大氣中)에 노출(露出)된 상태(狀態)로 취급(取扱)하였다. 열응력(熱應力)은 평면변형도조건(平面變形度條件)을 만족(滿足)하는 것으로 생각하였으며, 물성(物性)은 온도(溫度)에 무관(無關)한 상수(常數)로 취급(取扱)하였다. 온도분포(溫度分布)는 열전도문제(熱傳導問題)만을 고려(考慮)함으로서도 유효(有效)한 해(解)를 얻을 수 있으며 열응력(熱應力)은 접촉면(接觸面)에서부터 형성(形成)되며, 반경방향응력(半徑方向應力)은 시간(時間)이 경과(經過)함에 따라 압축응력(壓縮應力)이 증가(增加)하여 접촉면(接觸面)에서 최대치(最大値)를 갖고, 원주방향응력(圓周方向應力)은 접촉면(接觸面)에서 초기(初期)부터 거의 최종상태(最終狀態)와 같은 크기를 갖음을 알 수 있다. 균일온도분포(均一溫度分布)가 이루어지면 열응력(熱應力)의 형성(形成)은 완료(完了)되게 되며, 이때의 열응력(熱應力)의 크기와 분포경향(分布傾向)은 평면응력조건(平面應力條件)을 사용(使用)하였다는 사실(事實)을 고려(考慮)하면 $Lam\acute{e}$의 이론해(理論解)와 일치(一致)함을 알 수 있었다.

• Journal of the Microelectronics and Packaging Society
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• v.25 no.4
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• pp.47-52
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• 2018

In this study, the effects of the heat treatment and multi-scale hierarchical structures on the durability of the nano-patterned functional PMMA(Poly(methyl-methacrylate)) film was evaluated. The heat treatments that consisted of high-pressure/high-temperature flat pressing and rapid cooling process were employed to improve mechanical property of the PMMA films. Multi-scale hierarchical structures were fabricated by thermal nanoimprint to protect nano-scale structures from the scratch. Examination on surface structures and functionalities such as wetting angle and transmittance revealed that the preopposed heat treatment and multi-scale hierarchical structures are effective to minimize surface damages.

• Composites Research
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• v.19 no.4
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• pp.31-38
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• 2006

In this study, effects of curing temperature and autofrettage pressure on a Type 3 cryogenic propellant tank, which is composed of composite hoop/helical layers and a metal liner, were investigated by thermo elastic analysis and composite/aluminum ring specimen tests. Temperature field of a Type 3 tank was obtained from solving the heat transfer problem and, in turn, was used as nodal temperature boundary conditions during the elastic analyses for curing temperature and autofrettage pressure effects. As a result, it was shown that the higher curing temperature was, the more residual compressive stress and tensile stress were induced in composites and metal liner, respectively. On the contrary, autofrettage pressure brought the reduction of these residual thermal stresses caused by cryogenic environments to the tank structure. This tradeoff for curing temperature and autofrettage pressure must be considered in the design and manufacturing stages for a Type 3 cryogenic tank.

• KSCE Journal of Civil and Environmental Engineering Research
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• v.26 no.4C
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• pp.283-290
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• 2006

Concrete has advantages in fire situations as it is non-combustible and has low thermal conductivity. However, concrete that is not designed against fire can experience significant explosive spalling from the build-up of pore pressures and internal tensile stresses when heated. In this study, the performance of wet-mixed high strength sprayed polymer mortar for fire resistance of tunnel system was evaluated by experimentally and numerically. The fire test was performed in fire resistance(electric) furnace according to RABT(Richtlinien fur die Ausstatung und den Betrieb von $Stra{\beta}entunneln$) time heating temperature curve, so as to evaluate the temperature distribution with cover thickness of wet-mixed high strength sprayed polymer mortar for fire resistance of tunnel system. Based on experimental results and numerical analysis, the proper cover thickness of wet-mixed high strength sprayed polymer mortar determined the more than 4cm.

• The Journal of the Convergence on Culture Technology
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• v.9 no.5
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• pp.529-534
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• 2023

Although line printing technology is capable of high-speed and large area printing, residual stresses generated during the manufacturing process can deform the feedhole, causing nozzle plate crack or ink leaks. Therefore, in this paper, we propose a new thermal inkjet print head that is robust, reliable and more suitable for line-printing. The amount of deformation of the conventional line printing head measured through the experiment was converted into an equivalent load, and the validity of the load estimation method was verified through FEA analysis. In addition, in order to minimize deformation without increasing the head size, the head structure was designed to increase internal rigidity by reinforcing the unit nozzle with a pillar or support wall or by adding a support beam or dry/wet etched bridge. The FEA analysis results show that the feedhole deformation was reduced by up to 90%, and it is confirmed that the suggested print head with dry etched feedhole bridge operates normally without nozzle plate cracks and ink leakage through fabrication.

• Journal of the Korean Ceramic Society
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• v.52 no.6
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• pp.410-416
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• 2015

Recently, a new $Y_2O_3$ coating deposited using the EB-PVD method has been developed for erosion resistant applications in fluorocarbon plasma environments. In this study, surface crack formation in the $Y_2O_3$ coating has been analyzed in terms of residual stress and elastic modulus. The coating, deposited on silicon substrate at temperatures higher than $600^{\circ}C$, showed itself to be sound, without surface cracks. When the residual stress of the coating was measured using the Stoney formula, it was found to be considerably lower than the value calculated using the elastic modulus and thermal expansion coefficient of bulk $Y_2O_3$. In addition, amorphous $SiO_2$ and crystalline $Al_2O_3$ coatings were similarly prepared and their residual stresses were compared to the calculated values. From nano-indentation measurement, the elastic modulus of the $Y_2O_3$ coating in the direction parallel to the coating surface was found to be lower than that in the normal direction. The lower modulus in the parallel direction was confirmed independently using the load-deflection curves of a micro-cantilever made of $Y_2O_3$ coating and from the average residual stress-temperature curve of the coated sample. The elastic modulus in these experiments was around 33 ~ 35 GPa, which is much lower than that of a sintered bulk sample. Thus, this low elastic modulus, which may come from the columnar feather-like structure of the coating, contributed to decreasing the average residual tensile stress. Finally, in terms of toughness and thermal cycling stability, the implications of the lowered elastic modulus are discussed.