• Proceedings of the Korean Institute of Surface Engineering Conference
• /
• 2007.11a
• /
• pp.61-62
• /
• 2007

HVOF thermal spray coating of micron size Co-alloy powder has been studied for the durability improvement of high velocity spindle (HVS). Optimal coating process of this system for the best surface properties is hydrogen flow rate 75 FMR, oxygen flow rate 38-42 FMR, feed rate 30 g/min at spray distance 5 inch. Friction coefficient (FC) and wear trace (WT) decrease increasing coating surface temperature from 25$^{\circ}$C to 538$^{\circ}$C due to the higher lubricant effects of the oxides at the higher temperature. At the study of adhesion of T800 coating on a light metal alloy Ti-6Al-4V (Ti64) tensile bond strength (TBS) and tensile fracture location (TFL) of Ti64/T800 are 8,740 psi and near middle of T800 coating respectively. This shows that adhesion of Ti64/T800 is higher than the cohesion strength (8,740 psi) of T800 coating. Therefore T800 coating is strongly advisable for the surface coating on HVS such as high speed air-bearing spindle.

• Journal of Powder Materials
• /
• v.29 no.3
• /
• pp.226-232
• /
• 2022

In this study, a new manufacturing process for a multilayer-clad electrical contact material is suggested. A thin and dense BCuP-5 (Cu-15Ag-5P filler metal) coating layer is fabricated on a Ag plate using a high-velocity oxygen-fuel (HVOF) process. Subsequently, the microstructure and bonding properties of the HVOF BCuP-5 coating layer are evaluated. The thickness of the HVOF BCuP-5 coating layer is determined as 34.8 ㎛, and the surface fluctuation is measured as approximately 3.2 ㎛. The microstructure of the coating layer is composed of Cu, Ag, and Cu-Ag-Cu3P ternary eutectic phases, similar to the initial BCuP-5 powder feedstock. The average hardness of the coating layer is 154.6 HV, which is confirmed to be higher than that of the conventional BCuP-5 alloy. The pull-off strength of the Ag/BCup-5 layer is determined as 21.6 MPa. Thus, the possibility of manufacturing a multilayer-clad electrical contact material using the HVOF process is also discussed.

• Journal of the Korean Crystal Growth and Crystal Technology
• /
• v.16 no.6
• /
• pp.273-277
• /
• 2006

High velocity of oxy-fuel (HVOF) thermal spray coating is progressively replacing the other classical hard coatings such as chrome plating and ceramic coating by the classical methods, since the very toxic $Cr^{6+}$ ion is well known as carcinogen causing lung cancer, and the ceramic coatings are brittle. Co-alloy T800 powder is coated on the Inconel 718 substrates by the HVOF coating procesess developed by this laboratory. For the study of the possibility of replacing of chrome plating, the wear properties of HVOF Co-alloy T800 coatings are investigated using the reciprocating sliding tester with a counter sliding SUS 304 ball both at room and at an elevated temperature of $1000^{\circ}F\;(538^{\circ}C)$. The possibility as durability improvement coating is studied for the application to the high speed spindles vulnerable to frictional heat and wear. Wear mechanisms at the reciprocating sliding wear test are studied far the application to the systems similar to the sliding test such as high speed spindles. Wear debris and frictional coefficients of T800 coatings both at room and at an elevated temperature of $538^{\circ}C$ are drastically reduced compared to those of non-coated surface of Inconel 718 substrates. Wear traces and friction coefficients of both coated and non-coated surfaces are drastically reduced at a high temperature of $538^{\circ}C$ compared with those at room temperature. These show that the coating is highly recommendable far the durability Improvement coating on the surfaces vulnerable to frictional heat and wear.

• Korean Journal of Materials Research
• /
• v.30 no.7
• /
• pp.350-358
• /
• 2020

A variety of composite powders having different aluminum and carbon contents are prepared using various organic solvents having different amounts of carbon atoms in unit volume as ball milling agents for titanium and aluminum ball milling. The effects of substrate temperature and post-heat treatment on the texture and hardness of the coating are investigated by spraying with this reduced pressure plasma spray. The aluminum part of the composite powder evaporates during spraying, so that the film aluminum content is 30.9 mass%~37.4 mass% and the carbon content is 0.64 mass%~1.69 mass%. The main constituent phase of the coating formed on the water-cooled substrate is a non-planar α₂ phase, obtained by supersaturated carbon regardless of the alloy composition. When these films are heat-treated at 1123 K, the main constituent phase becomes γ phase, and fine Ti₂AlC precipitates to increase the film hardness. However, when heat treatment is performed at a higher temperature, the hardness is lowered. The main constitutional phase of the coating formed on the preheated substrate is an equilibrium gamma phase, and fine Ti₂AlC precipitates. The hardness of this coating is much higher than the hardness of the coating in the sprayed state formed on the water-cooled substrate. When hot pressing is applied to the coating, the porosity decreases but hardness also decreases because Ti₂AlC grows. The amount of Ti₂AlC in the hot-pressed film is 4.9 vol% to 15.3 vol%, depending on the carbon content of the film.

• Journal of Powder Materials
• /
• v.22 no.6
• /
• pp.413-419
• /
• 2015

Lanthanum zirconate, $La_2Zr_2O_7$, is one of the most promising candidates for next-generation thermal barrier coating (TBC) applications in high efficient gas turbines due to its low thermal conductivity and chemical stability at high temperature. In this study, bulk specimens and thermal barrier coatings are fabricated via a variety of sintering processes as well as suspension plasma spray in lanthanum zirconates with reduced rare-earth contents. The phase formation, microstructure, and thermo-physical properties of these oxide ceramics and coatings are examined. In particular, lanthanum zirconates with reduced rare-earth contents in a $La_2Zr_2O_7-4YSZ$ composite system exhibit a single phase of fluorite or pyrochlore after fabricated by suspension plasma spray or spark plasma sintering. The potential of lanthanum zirconate ceramics for TBC applications is also discussed.

• KIEAE Journal
• /
• v.7 no.1
• /
• pp.33-40
• /
• 2007

0.4 Million tons of shell powder have been disused as waste in KOREA and caused severe environmental pollution though shell powder can be utilized in real life for many ways. It is impending problem to recycle shell powder as it requires high expense for burying and temporary outside heap and causes severe environmental pollution being a main factor of ocean waste. To suggest the basic data for development of eco-friendly and high-function Wall Coatings Thin Textured Finishes, a wall coating sample was applied to indoor walls of a mock-up and temperature and humidity were measured to assess the thermal performance of it, and a survey of preference for the color sense and feel of the materials with a movie of specimens. The results of the study are following; 1) High insulation performance is shown from the assessment result of the room polystyrene board adhered on the walls then high humidity controlling performance is shown from that of the room polystyrene board coated by shell powder. This point out that shell powder has superiority for humidity controlling. 2) The result of thermal and humidity assessment shows that shell powder makes up for thermal conduction of the polystyrene board and same result can be expected from the assessment with materials which has similar thermal characteristics with polystyrene.3) Ranking of preferred specimens is; 1st Case 13, 2nd Case 17, 3rd Case 16, and 4th Case 12. Preferred shell powder was the ark shell. Preferred powder for plaster was the powder mixed with that sifted by 0.8mm, 100mesh and 40mesh, and for spray was the fine powder mixed with that sifted by 100mesh and 40mesh.

• Proceedings of the Korean Institute of Surface Engineering Conference
• /
• 2008.11a
• /
• pp.11-12
• /
• 2008

Micron-sized Co-alloy T800 powder was coated on Inconel718 (IN718) using high velocity oxygen fuel (HVOF) thermal spraying by the optimal coating process (OCP) determined from the best surface hardness of 16 coatings prepared by Taguchi program. The surface hardness improved 140-160 % from 399 Hv of IN718 to 560-630 Hv by the coating. Porosity of the coating was 1.0-2.7 %, strongly depending on spray parameters. Both friction coefficients (FC) and wear traces (WT) of the coating were smaller than those of IN718 substrate at both $25^{\circ}C$ and $538^{\circ}C$. FC and WT of IN718 and coating decreased with increasing the surface temperature. Tensile bond strength (TBS) and fracture location (FL) of Ti64/T800 were 8,770 psi and near middle of T800 coating respectively. TBS and FL of Ti64/NiCr/T800 were 8,740 psi and near middle of T800 coating respectively. This showed that cohesion of T800 coating was 8,740-8,770 psi, and adhesion of T800 on Ti64 and NiCr was stronger than the cohesion of T800.

• Tribology and Lubricants
• /
• v.18 no.4
• /
• pp.305-311
• /
• 2002

Three different kinds of brake discs including two coated brake discs and one steel disc were tested under the same experimental conditions on a reduced scale braking test bench. A braking test bench was specially designed to analyse thermo-mechanical and frictional behaviors of two types of brake with different sizes in stop and hold braking modes. Plasma spray coating technique was also used to coat the discs with ceramic powder. During the test four commercial brake pads were coupled with discs. Ceramic coated discs showed good stability in friction coefficient at high speed and high energy braking conditions. But they caused large wear loss of pad mass compared with the steel disc. It was shown that thermal barrier effect in ceramic coated discs adjusted the thermal partition between pad and disc. For a steel disc. it showed fluctuating friction coefficient at high speed but small wear loss of pad mass compared with ceramic coated discs.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
• /
• 2002.10b
• /
• pp.429-430
• /
• 2002

In this study, three kinds of brake: discs including two coated brake discs and one steel disc were tested under the same experimental conditions on a reduced scale braking test bench. Plasma spray coating technique was used to coat ceramic powder on the discs. In the test, four commercial sintered brake pads were coupled with discs. Ceramic coated discs have shown good stability in friction coefficient at high speed and high energy braking conditions. However, ceramic coated discs caused more wear loss of pad mass than the steel disc. It was shown that thermal barrier effect in ceramic coated discs adjusted the thermal partition between pad and disc. Steel disc showed fluctuating friction coefficient at high speed but less wear loss of pad mass than ceramic coated discs.

• Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
• /
• 1998.04a
• /
• pp.97-107
• /
• 1998

Three different kinds of brake discs including two coated brake discs and one steel disc were tested under the same experimental conditions on a reduced scale braking test bench. Braking test bench was specially designed to analyse thermo-mechanical and frictional behaviors of two sizes of brake discs in stop and hold braking modes. And Plasma spray coating technique was used to coat ceramic powder on the discs. In the test four commercial brake pads were coupled with discs. Ceramic coated discs had shown good stability in friction coefficient at high speed and high energy braking conditions. But they caused large pad mass wear loss compared with the steel disc. It was shown that thermal barrier effect in ceramic coated discs adjusted the thermal partition between pad and disc. For a steel disc, it had shown fluctuating friction coefficient at high speed but a fittie pad mass wear loss compared with ceramic coated discs.