• Title/Summary/Keyword: Thermal forming

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Structure -Properties Relations of Polypropylene/ Liquid Crystalline Polymer Blends

  • Sahoo, N.G.;Das, C.K.;Jeong, Hye-Won;Ha, Chang-Sik
    • Macromolecular Research
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    • v.11 no.4
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    • pp.224-230
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    • 2003
  • The blends of polypropylene (PP) with glass filled thermotropic liquid crystalline polymer (LCP-g) have been prepared by melt mixing techniques at different blend ratios. The thermal, dynamic mechanical, crystalline and morphological characteristics of these blends were investigated. Higher percent crystallinity was observed for 10% level of LCP-g in the blend in comparison to that of other blend ratios. The thermal stability increased with LCP-g concentration in the blend with PP. The variation of storage modulus, stiffness and loss modulus as a function of blend ratios suggested the phase inversion at the 50% level of LCP-g in the blend. The scanning electron microscopy (SEM) photographs showed the creation of voids and destruction of the fiber structures during the dynamic mechanical measurements. Processing behavior of the blends depended on the fiber forming characteristics of LCP-g, which again varied with the molding temperatures.

An Experimental Study on the Frost Prevention using Micro Liquid Film of an Antifreeze Solution

  • Chang Young-Soo;Yun Won-Nam
    • International Journal of Air-Conditioning and Refrigeration
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    • v.14 no.2
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    • pp.66-75
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    • 2006
  • The effect of antifreeze solution liquid film on the frost prevention is experimentally investigated. It is desirable that the antifreeze solution spreads widely on the heat exchanger surface forming thin liquid film to prevent frost nucleation while having small thermal resistance across the film. A porous layer coating technique is adopted to improve the wettability of the antifreeze solution on a parallel plate heat exchanger. The antifreeze solution spreads widely on the heat exchanger surface with $100{\mu}m$ thickness by the capillary force resulted from the porous structure. It is observed that the antifreeze solution liquid film prevents a parallel plate heat exchanger from frosting. The reductions of heat and mass transfer rate caused by the thin liquid film are only $1{\sim}2%$ compared with those for non-liquid film surface.

Optimization of Kiln Process Parameters of Low-Temperature Sintering Lightweight Aggregate by Response Surface Analysis (반응표면분석법에 따른 저온소성 경량골재의 킬른공정변수 최적화)

  • Lee, Han-Baek;Seo, Chee-Ho
    • Journal of the Korean Ceramic Society
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    • v.47 no.5
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    • pp.365-372
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    • 2010
  • This paper was to evaluate the influence of kiln process parameter(kiln angle, kiln rotating speed) of lightweight aggregate using waste glass and bottom ash with industrial by-products on thermal conductivity, density, water absorption, fracture load and porosity by response surface analysis. In the results of surface plot and contour plot, it has verified that kiln residence time of lightweight aggregate increase as kiln angle and rotating speed decreases. For this reason, pore size and quantity tend to increase by active reaction of forming agent. It seems to be that increase in pore size and quantity have caused decreasing density, fracture load and thermal conductivity, and increasing water absorption. In conclusion, optimization of kiln process parameter on thermal conductivity, density, water absorption, fracture load and porosity by response surface analysis are kiln angle 2.4646%, kiln rotating speed 40.7089 rpm.

Numerical and Experimental Investigation of the Heating Process of Glass Thermal Slumping

  • Zhao, Dachun;Liu, Peng;He, Lingping;Chen, Bo
    • Journal of the Optical Society of Korea
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    • v.20 no.2
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    • pp.314-320
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    • 2016
  • The glass thermal forming process provides a high volume, low cost approach to producing aspherical reflectors for x-ray optics. Thin glass sheets are shaped into mirror segments by replicating the mold shape at high temperature. Heating parameters in the glass thermal slumping process are crucial to improve surface quality of the formed glass. In this research, the heating process of a thermal slumping glass sheet on a concave parabolic mold was simulated with the finite-element method (FEM) to investigate the effects of heating rate and soaking temperature. Based on the optimized heating conditions, glass samples 0.5 mm thick were formed in a furnace with a steel concave parabolic mold. The figure errors of the formed glass were measured and discussed in detail. It was found that the formed glass was not fully slumped at the edges, and should be trimmed to achieve better surface deviation. The root-mean-square (RMS) deviation and peak-valley (PV) deviation between formed glass and mold along the axial direction were 2.3 μm and 4.7 μm respectively.

Thermal Shock Behavior of Porous Nozzles with Various Pore Sizes for Continuous Casting Process

  • Kim, Ju-Young;Yoon, Sang-Hyeon;Kim, Yoon-Ho;Lee, Hee-Soo
    • Journal of the Korean Ceramic Society
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    • v.48 no.6
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    • pp.617-620
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    • 2011
  • Thermal shock behavior of porous ceramic nozzles with various pore sizes for continuous casting process of steel was investigated in terms of physical properties and microstucture. Porous nozzle samples with a composition of $Al_2O_3$-$SiO_2$-$ZrO_2$ were fabricatedby adding various sizes of graphite as the pore forming agent. As the graphite size increased from 45~75 to 150~180 ${\mu}m$, both the resulting pore size and the flexural strength also increased. A thermal shock test was carried out at temperatures (${\Delta}$T) of 600, 700, 800, and 900$^{\circ}C$. Microstructure analysis revealed a small number of cracks on the sample with the largest mean pore size of 22.32 ${\mu}m$. In addition, increasing the pore size led to a smaller decrease in both pressure drop and elastic modulus. In conclusion, controlling the pore size can enhance thermal shock behavior.

A Study on the Thermal Decomposition Characteristics of Nitrophenylhydrazine (니트로페닐하이드라진의 열분해 특성에 관한 연구)

  • 김관응;이근원
    • Journal of the Korean Society of Safety
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    • v.16 no.2
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    • pp.75-79
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    • 2001
  • For handling and storage of reactive chemicals, the hazard evaluations have been extremely important. In the chemical industry, the most concerns are focused on the thermal harzards such as runaway reactions and thermal decompositions, which are mostly governed by thermodynamics and reaction kinetics or these reactive chemical in the system. This study no investigated the thermal decomposition characteristics of nitrophenylhydrazine isomers by using differential scanning calorimeter(DSC) and accelerating rate calorimeter(ARC). Experimental results showed that exothermic onset-temperatures in nitrophenylhydrazine(NPH) isomers were about 160-$210^{\circ}C$ by DSC and 100-$150^{\circ}C$ by ARC. The decomposition temperature acquired by ARC was about 50-$60^{\circ}C$ lower than that by DSC. Reaction heats were about 40-100cal/g by DSC and 330-750ca1/g by ARC. While ortho isomer of NPH show two distinct exothermic peaks, para isomer shows a single peak in DSC curves. The first exothermic peak for 2-NPH is mainly due to intramolecular dehydration forming 1-hydroxybenzotriazole(HOBT) and the second exothermic peak is mainly due to the decomposition of HOBT formed in the first step of decomposition. The exothermin peak in the DSC curve for 4-NPH is mainly due to dissociation of hydrazino and nitro groups.

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Development of a Model Instrument of Thermal Power Plant for Understanding of Air Pollutant Generation

  • Yamamoto, Mariko;Ma, Chang-Jin
    • Asian Journal of Atmospheric Environment
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    • v.10 no.3
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    • pp.156-161
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    • 2016
  • In order to deal with current environmental issues and their backgrounds, further development of current teaching methods and tools are essential. The result of questionnaire performed in this study indicates that the effect and the change of the perception of power generation in Japan after the great disaster of East Japan have caused many students (both high school and college students) to become interested in the energy situation. In the present study, we made an attempt to develop a model instrument of a thermal power plant that can be applied as a teaching tool for understanding of air pollutant forming as well as power generation. Our novel model tool consists of a body (30 cm width, 21 cm depth, and 41 cm height), a combustion chamber, two motors, a boiler, a voltmeter, and a chimney for measurement of exhaust gas. Using our novel hand-made power plant, we carried out some model experiments with learners (i.e. high school and college students). Through model experiments, students can be experienced not only about power generation but also about generation of air pollutants. In order to estimate the applicability of our novel instrument as an educational tool, we carried out the questionnaires before and after model experiments. More than 80% of educatees reported that it was very useful as a teaching tool for energy and environmental education. The results of questionnaires indicated that learners achieved a very deep understanding of the principles of power generation and the forming of air pollutants.

The Effects of Co Addition on Glass Forming Ability and Magnetic Properties for FeSiBNb Ribbon Alloys (FeSiBNb 리본 합금의 비정질 형성능과 자기적 특성에 미치는 Co의 첨가 효과)

  • Lee, Tae-Gyu;Noh, Tae-Hwan
    • Journal of the Korean Magnetics Society
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    • v.17 no.3
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    • pp.128-132
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    • 2007
  • The thermal and magnetic properties of amorphous (FeCo)SiBNb ribbon alloys with high glass forming ability have been investigated. The glass forming ability was enhanced by Co substitution in amorphous ($Fe_{1-X}Co_X)_{72}Si_4B_{20}Nb_4$ alloys with the thickness of about $40{\mu}m$. With the increase in Co content, the temperature range of supercooled liquid phase increased indicating the high glass forming ability of the Co-added alloys. Further the ac permeability increased, and the core loss decreased considerably by Co substitution, while small change in $B_8$ (magnetic flux density at 800 A/m) was observed. The frequency characteristics of permeability deteriorated as compared to conventional amorphous ribbon alloys with the thickness of about $20\;{\mu}m$ due to the increased skin effect.

Experimental and Analytical Evaluation of Forming Characteristics for AZ31B Magnesium Alloy Sheet (AZ31B 마그네슘 합금판재의 성형특성 평가를 위한 실험적·해석적 연구)

  • Lee, M.G.;Kim, H.J.
    • Transactions of Materials Processing
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    • v.20 no.2
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    • pp.146-153
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    • 2011
  • This study aimed at providing an experimental database for the mechanical properties of AZ31B magnesium alloy sheet such as stress-strain curve, yield stress, R-value and forming limit diagram(FLD) at various strain-rates and temperatures. Tensile tests were carried out on specimens having the orientations of $0^{\circ}$, $45^{\circ}$ and $90^{\circ}$ to the rolling direction with different crosshead speeds in the range between 0.008 and 8 mm/s at temperature from 25(room temperature) to $300^{\circ}C$. The influence of the specimen gage length on the tensile properties was investigated. FLD tests were performed at punch speed of 0.1 and 1.0 mm/s in the same temperature range as that of the tensile tests. Swift cup tests were conducted to verify the usefulness of the material database and the reliability of the finite element analysis(FEA). The effects of strain-rate as well as temperature were taken into account in these simulations. It was shown that the FLD-based failure was reasonably well predicted by the thermal-deformation coupled analysis for this rate-sensitive material.

Processing and mechanical property evaluation of maize fiber reinforced green composites

  • Dauda, Mohammed;Yoshiba, Masayuki;Miura, Kazuhiro;Takahashi, Satoru
    • Advanced Composite Materials
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    • v.16 no.4
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    • pp.335-347
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    • 2007
  • Green composites composed of long maize fibers and poly $\varepsilon$-caprolactone (PCL) biodegradable polyester matrix were manufactured by the thermo-mechanical processing termed as 'Sequential Molding and Forming Process' that was developed previously by the authors' research group. A variety of processing parameters such as fiber area fraction, molding temperature and forming pressure were systematically controlled and their influence on the tensile properties was investigated. It was revealed that both tensile strength and elastic modulus of the composites increase steadily depending on the increase in fiber area fraction, suggesting a general conformity to the rule of mixtures (ROM), particularly up to 55% fiber area fraction. The improvement in tensile properties was found to be closely related to the good interfacial adhesion between the fiber and polymer matrix, and was observed to be more pronounced under the optimum processing condition of $130^{\circ}C$ molding temperature and 10 MPa forming pressure. However, processing out of the optimum condition results in a deterioration in properties, mostly fiber and/or matrix degradation together with their interfacial defect as a consequence of the thermal or mechanical damages. On the basis of microstructural observation, the cause of strength degradation and its countermeasure to provide a feasible composite design are discussed in relation to the optimized process conditions.