• Title/Summary/Keyword: Thermal Treatment

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Analyses on the Increment of Surface Hydrophobicity of Epoxy Composites by Thermal Treatment (열철리에 따른 Epoxy 복합재료의 표면 소수성증가에 관한 해석)

  • Lim, Kyung-Bum;Lee, Beak-Su;Chung, Mu-Yong;Lee, Duck-Chool
    • The Transactions of the Korean Institute of Electrical Engineers C
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    • v.50 no.4
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    • pp.153-160
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    • 2001
  • In order to analyze the degradation process of epoxy/glass fiber for outdoor condition, FRP laminate was exposed to high temperature. Then, the degradation process was evaluated by comparing contact angle, surface potential, surface resistivity, and XPS. The experimental results showed that the amount of weight loss, contact angle, surface potential and surface resistivity increased up to 200 $^{\circ}C$ as a function of temperature. These phenomena show the existence of hydrophobic surface. With the change to the hydrophobic surface and the electrical potential and resistivity on FRP surface increased. In XPS to analyze surface chemical structures, the increased hydrophobicity in thermal increase of unsaturated double bond in carbon chains. Aslo, thermal treatment caused the discoloration on the point of treated surface. These phenomena were attributed to the generations of ether group.

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The heat treatment characteristics of plasma sprayed ZrO$_2$-Y$_2$O$_3$ coatings (플라즈마 용해법에 의한 ZrO$_2$-Y$_2$O$_3$ 피복층의 가열처리효과)

  • 정병근;김한삼;김수식
    • Journal of Surface Science and Engineering
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    • v.27 no.1
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    • pp.12-18
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    • 1994
  • The plasma spray process was used to deposit coatings of $ZrO_2$-8wt%Y2O3 powders on mild steel sub-strate, and the characteristics of as-deposited and heat treated coatings have been investigated. Particulary, the variations of porosity, wear resistance, thermal barrier and thermal shock resistance in $ZrO_2$-8wt% $Y_2O_3$coatings after heat treatment under vacuum circumstance have been investigated. The porosity of the coating layer was increased with increased spray distance. In the case of the arc current of 450A and at the spray distance of 50mm, it was obtained the lowest amount of porosity. After heat treatment, the amount of porosity was found to be decreased, and the wear resistance, microhardness and thermal shock resistance were im-proved. However, the thermal barrier was decreased.

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Numerical Analysis on RF (Radio-frequency) Thermal Plasma Synthesis of Nano-sized Ni Metal (고주파 열플라즈마 토치를 이용한 Ni 금속 입자의 나노화 공정에 대한 전산해석 연구)

  • Nam, Jun Seok;Hong, Bong-Guen;Seo, Jun-Ho
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.26 no.5
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    • pp.401-409
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    • 2013
  • Numerical analysis on RF (Radio-Frequency) thermal plasma treatment of micro-sized Ni metal was carried out to understand the synthesis mechanism of nano-sized Ni powder by RF thermal plasma. For this purpose, the behaviors of Ni metal particles injected into RF plasma torch were investigated according to their diameters ($1{\sim}100{\mu}m$), RF input power (6 ~ 12 kW) and the flow rates of carrier gases (2 and 5 slpm). From the numerical results, it is predicted firstly that the velocities of carrier gases need to be minimized because the strong injection of carrier gas can cool down the central column of RF thermal plasma significantly, which is used as a main path for RF thermal plasma treatment of micro-sized Ni metal. In addition, the residence time of the injected particles in the high temperature region of RF thermal plasma is found to be also reduced in proportion to the flow rate of the carrier gas In spite of these effects of carrier gas velocities, however, calculation results show that a Ni metal particle even with the diameter of $100{\mu}m$ can be completely evaporated at relatively low power level of 10 kW during its flight of RF thermal plasma torch (< 10 ms) due to the relatively low melting point and high thermal conductivity. Based on these observations, nano-sized Ni metal powders are expected to be produced efficiently by a simple treatment of micro-sized Ni metal using RF thermal plasmas.

Treatment of Stainless Steel Cladding in Pressurized Thermal Shock Evaluation: Deterministic Analyses

  • Changheui Jang;Jeong, lll-Seok;Hong, Sung-Yull
    • Nuclear Engineering and Technology
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    • v.33 no.2
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    • pp.132-144
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    • 2001
  • Fracture mechanics is one of the major areas of the pressurized thermal shock (PTS) evaluation. To evaluate the reactor pressure vessel integrity associated with PTS, PFM methodology demands precise calculation of temperature, stress, and stress intensity factor for the variety of PTS transients. However, the existence of stainless steel cladding, with different thermal, physical, and mechanical property, at the inner surface of reactor pressure vessel complicates the fracture mechanics analysis. In this paper, treatment schemes to evaluate stress and resulting stress intensity factor for RPV with stainless steel clad are introduced. For a reference transient, the effects of clad thermal conductivity and thermal expansion coefficients on deterministic fracture mechanics analysis are examined.

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The Dielectric Characteristics of Low Density Polyethylene Film due to Thermal Treatment Effect (열처리효과에 따른 저밀도 폴리에틸렌 박막의 유전특성)

  • 김왕곤;가출현;이용우;홍진웅
    • Journal of the Korean Society of Safety
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    • v.11 no.1
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    • pp.67-74
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    • 1996
  • In order to investigate the effect and reliability coming up to properties of the matter due to the change of solid structure in dielectrics, the effect of dielectric characteristics for thermal treated LDPE film was made researches. Specimens of LDPE with thickness 100 [$\mu\textrm{m}$] were investigated into the change of solid structure by ageing. Thermal treated specimen were made, that were after applying heat at 100 [$^{\circ}C$] for 1 [hour] \circled1 air-cooled specimen slowly, \circled2 water-cooled specimen under the ,com temperature, \circled3 liquid nitrogen gas-cooled specimen rapidly. With specimen of thermal treated three types turn out and original, it was for dielectric characteristics to be experimented in the temperature range of 20~120 [$^{\circ}C$], frequency range of 30~1.5${\times}10^5/$[Hz], appling voltage from 300 to 1500[㎷]. Consequently, the degree of crystallinity was changed with 49~57 [%] according to the thermal treatment. In case of frequency, 100 [Hz], on the thermal dependance in dielectric characteristics, tan decreases due to cooling method.

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Effects of Various Thermal Treatments on Physicochemical and Nutritional Properties of Shiitake Mushrooms (열처리 방법에 따른 표고버섯의 이화학적 특성 및 영양학적 분석)

  • Lee, Jung-Gyu;Kim, Kwang-Il;Hwang, In-Guk;Yoo, Seon-Mi;Min, Sang-Gi;Choi, Mi-Jung
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.44 no.6
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    • pp.874-881
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    • 2015
  • In the food industry, thermal treatment is an important process for extending shelf-life of foods. However, heating process affects the physicochemical, nutritional, and microbial properties of foodstuff such as color, texture, pH, and proximate compositions. This study was conducted to select an optimal thermal treatment by observing physicochemical, nutritional, and microbial effects of shiitake mushrooms with different thermal treatment methods. Shiitake mushrooms were washed and sliced equally ($5cm{\times}0.5cm{\times}0.5cm$) and then heat-treated by three methods. Samples were heated in $100^{\circ}C$ boiling water, steamed for 10 min, or pan fried at $130^{\circ}C$ for 4 min. Total color difference values showed significantly increasing tendency with treatment time. For pH values, boiling water-treated mushrooms showed increasing tendency according to increased thermal treatment. For the results of hardness, boiling water or pan frying-treated mushrooms showed reduced tendency within 1 min. In the case of steam-treated mushrooms, hardness values were maintained for 1 min. Organic acid contents of steam-treated sample showed the lowest value among treatments. For microbial counts, steam-treated samples for 3 min showed the lowest value. Consequently, the results of this study suggest that steam treatment could be the optimal thermal treatment to minimize quality loss of shiitake mushrooms.

Analysis of Thermal Shock in Tool Steels for Hot Forging (열간단조 금형강의 열충격특성연구)

  • Kim, J.W.;Kim, B.J.;Jo, I.S.;Moon, Y.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.14 no.3
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    • pp.155-159
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    • 2001
  • The thermal shock resistance has been investigated and compared in three hot-work tool steels. The resistance to thermal shock is first of all a matter of good toughness and ductility. Therefore, a proper hot-work tool steel should be characterized by high fracture strength and high temperature toughness. In this study, new test method is proposed to measure the thermal shock resistance. New method is basically based on Uddeholm' thermal shock test but some modification has been properly applied. Based on these results, some critical temperature($T_{fractures}$) at which fracture occur can be measured to characterize the thermal resistance of the materials. The specific values of ${\Delta}T$, the temperature difference between holding temperature and $T_{fractures}$, has been successfully used as a measure of the thermal shock resistance in this study, the results showed that the thermal shock method used in this study was properly modified.

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THE EFFECTS OF THERMAL CYCLING ON THE BOND STRENGTH OF SELF-CURING RESIN (Thermal Cycling에 따른 자가중합 레진의 결합강도에 관한 연구)

  • Cho, Hye-Won;Ha, Jum-In
    • The Journal of Korean Academy of Prosthodontics
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    • v.35 no.4
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    • pp.697-705
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    • 1997
  • The purpose of this study was to evaluate the effects of two metal adhesive primers on the shear bond strengths of self-curing resin to Ni-Cr a]toy and the effects of 1000 thermal cycling on the durability of the bond. The two selected metal adhesive primers were Metal Primer II(G-C corp., Japan) and MR Bond(Tokuyama corp., Japan) and no treatment groups were used as control. All specimens were divided into two groups according to thermal cycling. In the group without thermal cycling, the specimens were stored in water for 24 hours. In the group with thermal cycling, the specimens were thermocycled 1000 times at temperature of $5^{\circ}C\;and\;55^{\circ}C$. Shear bond strengths were measured using the Universal testing machine(Zwick 145641, Germany) with a crosshead speed of 0.5 mm/min. The results were as follows: 1. MR Bond significantly improved the shear bond strength of resin to Ni-Cr alloy before and after thermal cycling. 2. There were no difference in the shear bond strength of resin to Ni-Cr alloy between Metal Primer II treated group and no treatment group. 3. Regardless of the type and the use of adhesive primers, there were tendency of decrease in shear bond strength with 1000 thermal cycling.

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Thermal treatment dependences of MFS devices in $BaMgF_4$ thin films on silicon structures ($BaMgF_4$ 박막을 이용한 MFS 디바이스의 열처리 의존성)

  • 김채규;정순원;이상우;김광호
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 1998.06a
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    • pp.59-62
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    • 1998
  • Thermal treatment dependences of MFS devices in $BaMgF_4$ on Si structures have been investigated. $BaMgF_4$ thin films have been directly deposited on the p-Si(100) wafers at a low temperature of $300^{\circ}$ in an ultra high vacuum(UHV) system. After in-situ post-deposition annealing was conducted for 20 s at $650^{\circ}$, bias and temperature were applied to $BaMgF_4/Si$ structures. Although X-ray diffraction analysis showed that the films were polycrystalline in nature before and after bias temperature, the C-V properties were some different between with and without bias-temperature treatment.

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Effect of Wet and Dry Thermal Setting Conditions of Stretch Fabric to Fabric Mechanical Property and Garment Formability (습·건열 열고정 조건이 스트레치 직물의 역학특성과 의류형성성능에 미치는 영향)

  • Kim, Hyun-Ah;Kim, Seung-Jin
    • Fashion & Textile Research Journal
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    • v.20 no.1
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    • pp.83-92
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    • 2018
  • This paper investigated garment formability and fabric mechanical properties of one-way and two-way stretch fabrics according to the thermal treatment methods. One-way and two-way stretch fabrics were woven using 75d and 150d PET/spandex covering yarns and then these were wet thermal treated with four kinds of finishing machines. The fabric mechanical properties of these stretch fabrics specimens were measured and compared with the regular PET fabrics. The stretch ratio of one-way stretch fabric was ranged 12 to 26 percentage, 15 to 45 percentage for 2-way stretch fabrics and 4 to 10 percentage for regular fabrics. Garment formability of stretch fabric was superior than that of regular fabrics, in addition, 2-way stretch fabric was better than one-way. The garment formability of the stretch fabrics treated with CPB and Lava wet thermal machines showed the highest values, and the stretch ratio of these 2-way stretch fabrics was also the highest, which was ranged 20 to 45 percentage. This phenomenon was assumed to be due to high extensibility and bending rigidity with low shear modulus of the 2-way stretch fabric treated with CPB and Lava wet thermal machines. It was shown that the garment formability of stretch fabrics treated without dry thermal treatment was higher than that of dry thermal treated fabrics. It revealed that high stretch fabric was available under the condition of low process tension in the wet and dry thermal treatments of the finishing process, which makes high garment formability.