• Title/Summary/Keyword: Thermal Treatment

Search Result 2,727, Processing Time 0.028 seconds

Microstructural Development of Ferritic 11Cr-3.45W Heat-resistance Steel for Ultra-supercritical Power Plant During Creep and Thermal Aging (크리프와 등온열화에 따른 초초임계압 발전설비용 페라이트계 11Cr-3.45W 내열합금강의 미세조직 변화)

  • Kim, Chung-Seok
    • Journal of the Korean Society for Heat Treatment
    • /
    • v.31 no.3
    • /
    • pp.91-96
    • /
    • 2018
  • Microstructural development of ferritic 11Cr-3.45W heat-resistance steel for ultra-supercritical power plant during creep and thermal aging was investigated using electron microscopy. The test samples were isothermally aged at $700^{\circ}C$ for up to 4000 hours and subjected to creep loading at $700^{\circ}C$ for predetermined periods of lifetime to prepare the damaged materials. In this structural material, a various secondary phases are the primary influence on mechanical properties of ferritic heat-resistance steel. The typical precipitates of $M_{23}C_6$, MX and $M_2X$ secondary phases had been analyzed through qualitative and quantitative manner. Coarsening of precipitates and increase of lath width were observed during creep and thermal aging. This phenomenon was remarkable for creep process compared with isothermal aging process.

A Study on Shrinkage Properties of Polytrimethylene Terephthalate (PTT) Drawn Textured Yarn (Polytrimethylene terephthalate(PTT) 가연사의 수축거동에 관한 연구)

  • Choi, Jae-Woo;Jang, Bong-Sik
    • Fashion & Textile Research Journal
    • /
    • v.6 no.4
    • /
    • pp.492-496
    • /
    • 2004
  • Shrinkage properties of drawn textured Poly(trimethylene terephthalate, PTT) yarn, which has been developed recently, were investigated to provide fundamental information for the textile industry. Shrinkage ratio characteristics on PTT yarn with six different count were investigated with tension, dry and wet thermal temperature. In non-tension, the shrinkage ratio were increased to increasing temperature at dry and wet thermal treatment, and in tension, the shrinkage ratio were increased to increasing tension at dry and wet thermal treatment.

Dispersant Effect on Thermal Performance of SG (증기발생기 열성능에 미치는 분산제 첨가효과)

  • Lee, Jae-Keun;Moon, Jeon-Soo;Yoon, Seok-Won;Maeng, Wan-Young
    • Journal of Hydrogen and New Energy
    • /
    • v.22 no.4
    • /
    • pp.546-551
    • /
    • 2011
  • The corrosion on steam generator tubes of the secondary side of pressurized water reactor inhibits heat transfer. One of the most efficient techniques improving the heat transfer performance of a nuclear electric generation is a corrosion control. The environmental parameters mostly affecting corrosion are materials and chemical additives. It seems that no further corrosion occurs in steels with Polyacrylic acid polymer dispersant treatment. Polyacrylic acid forms a protective coating with uniform thickness on metal surface. Polyacrylic treatment appears to be the most convenient way to enhance the thermal performance by the thermal conductivity improvement in steam generators.

Synthesis of Silica Aerogel at Ambient Pressure and Characterization (II) (실리카 에어로겔의 상압합성 및 특성연구(II))

  • 권영근;최세영;강신규
    • Journal of the Korean Ceramic Society
    • /
    • v.36 no.11
    • /
    • pp.1189-1197
    • /
    • 1999
  • Low-density silica gel monolith was synthesized at ambient pressure by surface modification with TMCS and sub-sequent heat treatment. The mechanical thermal and optical properties of gel were studied. Compressive strength and modulus of compression of 350$^{\circ}C$-heated gel with the density of 0.24g/cm3 were 250kPa and 0.2MPa respectively. The thermal conductivity of silica gels synthesized at ambient pressure exhibited 0.02 W/m$.$K for the density of 0.24g/cm3 which is similar to that of the gel via supercritical drying and their main thermal transfer mechanism is considered to be solid and radiation conduction at room temperature. Ambient-dried silica gels were transparent blue showing about 60% of transmittance in the wavelength of 1500-2100nm and typical absorption bands of existing bonds under heat treatment at 350$^{\circ}C$. Medium scale monolity(${\Phi}$=50mm) at ambient pressure could be successfully prepared through total 5-month process period.

  • PDF

Characterization of Pitch Derived from Petroleum Residue and Coal-tar (석유계 잔사유 및 coal-tar의 핏치 개질 특성)

  • KIM, JIHONG;KIM, HYEONGGI
    • Journal of Hydrogen and New Energy
    • /
    • v.27 no.5
    • /
    • pp.612-619
    • /
    • 2016
  • Pitch synthesis reaction was studied based on the effect for chemical composition of feedstock. Feedstock was selected as pyrolyzed fuel oil (PFO) and coal-tar (CT), which are by-products in petroleum and steel industry. Pitch was prepared at $420^{\circ}C$ for 180 minutes on atmospheric pressure by thermal treatment. Thermal stability and softening point (SP) of the prepared pitches were investigated and their molecular weight distribution was analyzed by MALDI-TOF. PFO has various aliphatic compounds and coal-tar has high aromaticity with 3 wt% of primary quinoline insolubles. The thermal property of PFO was enhanced with polymerization reaction during the thermal treatment with increased molecular weight range. But CT was inferior to PFO because of side reaction by hetero elements. CTP was appeared molecular weight by 0~200 m/z.

Effect of Rapid Thermal Annealing on the Transparent Conduction and Heater Property of ZnO/Cu/ZnO Thin Films (RTA 후속 열처리에 따른 ZnO/Cu/ZnO 박막의 투명전극 및 발열체 특성 연구)

  • Yeon-Hak Lee;Daeil Kim
    • Journal of the Korean Society for Heat Treatment
    • /
    • v.36 no.3
    • /
    • pp.115-120
    • /
    • 2023
  • ZnO/Cu/ZnO (ZCZ) thin film deposited on the glass substrate with DC and RF magnetron sputtering was rapid thermal annealed (RTA) and then effect of thermal temperature on the opto-electical and transparent heater properties of the films were considered. The visible transmittance and electrical resistivity are depends on the annealing temperature. The electrical resistivity decreased from 1.68 × 10-3 Ωcm to 1.18 × 10-3 Ωcm and the films annealed at 400℃ show a higher transmittance of 78.5%. In a heat radiation test, when a bias voltage of 20 V is applied to the ZCZ film annealed at 400℃, its steady state temperature is about 70.7℃. In a repetition test, the steady state temperature is reached within 15s for all of the bias voltages.

Effect on the Thermal Treatment for Improving Efficiency in Silicon Heterojunction Solar Cells (이종접합 실리콘 태양전지의 효율 개선을 위한 열처리의 효과)

  • Hyeong Gi Park;Junsin Yi
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.37 no.4
    • /
    • pp.439-444
    • /
    • 2024
  • This study investigates the post-thermal treatment effects on the efficiency of silicon heterojunction solar cells, specifically examining the influence of annealing on p-type microcrystalline silicon oxide and ITO thin films. By assessing changes in carrier concentration, mobility, resistivity, transmittance, and optical bandgap, we identified conditions that optimize these properties. Results reveal that appropriate annealing significantly enhances the fill factor and current density, leading to a notable improvement in overall solar cell efficiency. This research advances our understanding of thermal processing in silicon-based photovoltaics and provides valuable insights into the optimization of production techniques to maximize the performance of solar cells.

Studies on Dismantlement Property of Dismantlable Polyurethane Adhesive (우레탄계 해체성 접착제의 해체특성에 관한 연구)

  • Kim, Dong Ho;Chung, Ildoo;Kim, Gu Ni
    • Journal of Adhesion and Interface
    • /
    • v.11 no.1
    • /
    • pp.26-34
    • /
    • 2010
  • We synthesized polyurethane adhesive having thermal characteristic could be debonded by heat treatment and made a dismantlable polyurethane adhesive including thermally expansive bead. We used dynamic mechanical thermal analyzer (DMA) to confirm thermal characteristic and investigated bond strength, dismantlement property of dismantlable polyurethane adhesive by content of thermally expansive bead, heating trigger and treatment conditions. The dismantlable polyurethane adhesive could be expanded by hot-air or microwave treatment and the dismantlement of the specimens became easier as the weight fraction of the thermally expansive bead increased. At the dismantlable polyurethane adhesive, the content of thermally expansive bead 40% was suitable for both bond strength and dismantlement, in case of using hot-air treatment as trigger for dismantlement, bonded joints were separated easily at $160^{\circ}C$ for 30 min and in case of using microwave as trigger, bonded joints were separated easily by irradiating microwave for 4 min.

HEAT-TREATMENT OF LARGE-SCALE GLASS BACKPLANES IN A MUFFLE FURNACE (머플 가열로에서의 대면적 유리기판의 가열공정에 대한 열적 연구)

  • Kim, D.H.;Son, G.;Hur, N.;Kim, B.K.;Kim, H.J.;Park, S.H.
    • Journal of computational fluids engineering
    • /
    • v.17 no.4
    • /
    • pp.16-23
    • /
    • 2012
  • Current display manufacturing processes apply thermal treatment of glass backplanes widely for hydrogen degassing, crystallization of thin-films, tempering, forming, and precompaction. Estimation of the characteristics of transient heating stages and thermal non-uniformities on a single glass substrate or in a stack of glasses are extremely helpful to understand non-homogeneity of mechanical and electronic features of nano/micro structures of end products. Based on simple heat transfer models and using an electric muffle furnace, temperature variations in a glass stack were predicted and measured for glass backplanes of $1.5{\times}1.85m^2$ in size and 0.7 mm in thickness. Except for the period of putting glass backplanes into the furnace, thermal radiation was the major heating mechanism for the treatment and theoretical predictions agreed well to the experimental temperatures on the backplanes. Using the theoretical model, thermal fields for a glass stack of glass-size, $2.2{\times}2.5m^2$, and of the number of sheets, 1 to 12, were calculated for practical design and manufacturing of the muffle furnace for large-scale displays, e.g. up to $8^{th}$ generation.