• Title/Summary/Keyword: Tensile test

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Incorporation of amoxicillin-loaded microspheres in mineral trioxide aggregate cement: an in vitro study

  • Fabio Rocha Bohns;Vicente Castelo Branco Leitune;Isadora Martini Garcia;Bruna Genari;Nelio Bairros Dornelles Junior;Silvia Staniscuaski Guterres;Fabricio Aulo Ogliari;Mary Anne Sampaio de Melo;Fabricio Mezzomo Collares
    • Restorative Dentistry and Endodontics
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    • v.45 no.4
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    • pp.50.1-50.11
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    • 2020
  • Objectives: In this study, we investigated the potential of amoxicillin-loaded polymeric microspheres to be delivered to tooth root infection sites via a bioactive reparative cement. Materials and Methods: Amoxicillin-loaded microspheres were synthesized by a spray-dray method and incorporated at 2.5% and 5% into a mineral trioxide aggregate cement clinically used to induce a mineralized barrier at the root tip of young permanent teeth with incomplete root development and necrotic pulp. The formulations were modified in liquid:powder ratios and in composition by the microspheres. The optimized formulations were evaluated in vitro for physical and mechanical eligibility. The morphology of microspheres was observed under scanning electron microscopy. Results: The optimized cement formulation containing microspheres at 5% exhibited a delayed-release response and maintained its fundamental functional properties. When mixed with amoxicillin-loaded microspheres, the setting times of both test materials significantly increased. The diametral tensile strength of cement containing microspheres at 5% was similar to control. However, phytic acid had no effect on this outcome (p > 0.05). When mixed with modified liquid:powder ratio, the setting time was significantly longer than that original liquid:powder ratio (p < 0.05). Conclusions: Lack of optimal concentrations of antibiotics at anatomical sites of the dental tissues is a hallmark of recurrent endodontic infections. Therefore, targeting the controlled release of broad-spectrum antibiotics may improve the therapeutic outcomes of current treatments. Overall, these results indicate that the carry of amoxicillin by microspheres could provide an alternative strategy for the local delivery of antibiotics for the management of tooth infections.

Flexural Behavior of RC Beam After Completion of Electrochemical Chloride Extraction (전기화학적 염화물 추출 후 철근-콘크리트 보의 휨 거동)

  • Jung Wook Lee;Ki Yong Ann
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.11 no.4
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    • pp.484-492
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    • 2023
  • The structural behaviour of concrete beam was examined by the three points bending test after the completion of the electrochemical chloride extraction (ECE), rather than bond strength mostly measured in previous studies. It was found that the flexural rigidity of concrete was lowered by the ECE, but the strength was enhanced in terms of the maximum load.The flexural rigidity, in the linear elastic range, was reduced by the loss of effective cross-section area. In fact, the inertia moment was substantially subjected to 70 % loss of the cross-section by the tensile strain at the condition of the failure. However, a lower rate of the inertia moment reduction was achieved by the ECE, implying the higher resistance to the cracking, but the higher risk of deformation.

Multiple effects of nano-silica on the pseudo-strain-hardening behavior of fiber-reinforced cementitious composites

  • Hossein Karimpour;Moosa Mazloom
    • Advances in nano research
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    • v.15 no.5
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    • pp.467-484
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    • 2023
  • Despite the significant features of fiber-reinforced cementitious composites (FRCCs), including better mechanical, fractural, and durability performance, their high content of cement has restricted their use in the construction industry. Although ground granulated blast furnace slag (GGBFS) is considered the main supplementary cementitious material, its slow pozzolanic reaction stands against its application. The addition of nano-sized mineral modifiers, including nano-silica (NS), is an alternative to address the drawbacks of using GGBFS. The main object of this empirical and numerical research is to examine the effect of NS on the strain-hardening behavior of cementitious composites; ten mixes were designed, and five levels of NS were considered. This study proposes a new method, using a four-point bending test to assess the use of nano-silica (NS) on the flexural behavior, first cracking strength, fracture energy, and micromechanical parameters including interfacial friction bond strength and maximum bridging stress. Digital image correlation (DIC) was used for monitoring the initiation and propagation of the cracks. In addition, to attain a deep comprehension of fiber/matrix interaction, scanning electron microscope (SEM) analysis was used. It was discovered that using nano-silica (NS) in cementitious materials results in an enhancement in the matrix toughness, which prevents multiple cracking and, therefore, strain-hardening. In addition, adding NS enhanced the interfacial transition zone between matrix and fiber, leading to a higher interfacial friction bond strength, which helps multiple cracking in the composite due to the hydrophobic nature of polypropylene (PP) fibers. The findings of this research provide insight into finding the optimum percent of NS in which both ductility and high tensile strength of the composites would be satisfied. As a concluding remark, a new criterion is proposed, showing that the optimum value of nano-silica is 2%. The findings and proposed method of this study can facilitate the design and utilization of green cementitious composites in structures.

Design of Roof Side Rail by Hot Blow Forming using High Strength Aluminum (핫블로우 포밍을 이용한 고강도 알루미늄 루프 사이드 레일 설계)

  • M. G. Kim;J. H. Lee;D. C. Ko
    • Transactions of Materials Processing
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    • v.32 no.6
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    • pp.311-320
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    • 2023
  • Recently, lightweight of automotive parts has been required to solve environmental problems caused by global warming. Accordingly, research and development are proceeded on manufacturing of parts using aluminum that can replace steel for lightweight of the automotive parts. In addition, high strength aluminum can be applied to body parts in order to meet both requirements of lightening and improving crash safety of vehicle. In this study, hot blow forming of roof side rail is employed to manufacturing of the automotive parts with high strength aluminum tube. In hot blow forming, longer forming times and excessive thinning can be occurred as compared with conventional manufacturing processes. So optimization of process conditions is required to prevent excessive thinning and to uniformize thickness distribution with fast forming time. Mechanical properties of high strength aluminum are obtained from tensile test at high temperature. These properties are used for finite element(FE) analysis to investigate the effect of strain rate on thinning and thickness distribution. Variation of thickness was firstly investigated from the result of FE analysis according to tube diameter, where the shapes at cross section of roof side rail are compared with allowable dimensional tolerance. Effective tube diameter is determined when fracture and wrinkle are not occurred during hot blow forming. Also FE analysis with various pressure-time profiles is performed to investigate the their effects on thinning and thickness distribution which is quantitatively verified with thinning factor. As a results, optimal process conditions can be determined for the manufacturing of roof side rail using high strength aluminum.

Comparison of Resin Impregnation and Mechanical Properties of Composites Based on Fiber Plasma Treatment (섬유 플라즈마 처리에 따른 복합재료의 수지 함침성 및 기계적 특성 비교)

  • Seong Baek Yang;Donghyeon Lee;Yongseok Lee;Dong-Jun Kwon
    • Composites Research
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    • v.36 no.6
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    • pp.388-394
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    • 2023
  • In composites manufacturing, increasing resin impregnation is a key way to speed up the manufacturing process and improve product quality. While resin improvement is important, simple fiber surface treatments can also improve resin flowability. In this study, different plasma treatment times were applied to carbon fiber fabrics to improve the impregnation between resin and fiber. Electrical resistivity measurements were used to evaluate the dispersion of resin in the fibers, which changed with plasma treatment. The effect of fiber surface treatment on resin spreadability could be observed in real time. When inserting a carbon fiber tow into the resin, the amount of resin that soaked into the tow was measured to objectively compare resin impregnation. Five minutes of plasma treatment improved the tensile and compressive strength of the composite by more than 50%, while reducing the void content and increasing the fire point impregnation flow rate. Finally, a dynamic flexural fatigue test was conducted using a portion of the composite used as an architectural composite part, and the composite part did not fail after one million cycles of a 3 kN load.

Deterioration Characteristics of Naturally Aged AA 2026 due to ExpoSure to High Temperatures (자연 시효 처리된 AA 2026의 고온 노출에 따른 물성 열화 특성에 대한 연구)

  • HaNeul Kim;HyeonWoo Kang;ByoungLok Jang;HeeKook Kim
    • Journal of the Korean Society for Heat Treatment
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    • v.37 no.3
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    • pp.114-120
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    • 2024
  • AA 2026, which is used as an aviation material, is an improved version of 2024 and has higher physical properties, and is a material that has the potential to be applied to supersonic aircraft to be developed in the future. However, when an aircraft exceeds supersonic speeds, the surface heats up and the material must be resistant to this. Therefore, this study confirmed the high-temperature properties of AA 2026, an aviation structural material. AA 2026, solution treated at 500℃ for 4hr, was naturally aged at room temperature for more than 168 hr. Changes in microstructure and physical properties were confirmed over several hours of exposure to 100℃, 200℃, and 300℃, respectively. As a result of microstructure analysis, there was no significant change at 100℃, and from 200℃, GPB, a strengthening mechanism, grew and formed an S Phase. It was confirmed that the S Phase grew as the exposure time increased. Through a tensile test, it was confirmed that physical properties deteriorated as the precipitates grew. However, it was confirmed that the properties were stably maintained at 100℃, which is the temperature when the speed of a supersonic aircraft is less than Mach 2.

Measurement and Analysis of the Material Behavior of Corrugated Paperboard for Finite Element Analysis (유한요소해석을 위한 골판지 소재의 물성측정 및 분석)

  • Gyu-Yeol Kang;Duk-Geun Bae;Sun-Jong, Noh;Sim-Won Chin;Woo-Jong Kang
    • Composites Research
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    • v.37 no.3
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    • pp.143-149
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    • 2024
  • This paper measures the mechanical properties of corrugated cardboard, an eco-friendly packaging material, and applies these measurements to the MAT_PAPER model in LS-DYNA for finite element analysis. Although MAT_PAPER is primarily designed for modeling the behavior of paper, this research demonstrates its applicability to corrugated cardboard as well. Tensile, compression, and shear behaviors of a corrugated cardboard were measured and analyzed, and based on these results, six yield surfaces were derived and integrated into the MAT_PAPER model. By comparing the finite element analysis of the material tests and the low velocity collapse analysis of the corrugated cardboard square boxes with each experimental results, it was shown that the behavior of corrugated cardboard could be equivalently considered well by the MAT_PAPER model. However, since the model is not rate-dependent, the high strain rate properties of liner materials were measured and used for strain rate correction. Consequently, this matches well with the results of the high-speed compression tests of the corrugated cardboard square boxes.

Design, simulation and experimental analysis of fiber-reinforced silicone actuators

  • Sina Esmalipour;Masoud Ajri;Mehrdad Ekhtiari
    • Structural Engineering and Mechanics
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    • v.91 no.2
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    • pp.211-225
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    • 2024
  • Soft bending actuators have gained significant interest in robotic applications due to their compliance and lightweight nature. Their compliance allows for safer and more natural interactions with humans or other objects, reducing the risk of injury or damage. However, the nonlinear behaviour of soft actuators presents challenges in accurately predicting their bending motion and force exertion. In this research, a new comprehensive study has been conducted by employing a developed 3D finite element model (FEM) to investigate the effect of geometrical and material parameters on the bending behaviour of a soft pneumatic actuator reinforced with Kevlar fibres. A series of experiments are designed to validate the FE model, and the FE model investigates the improvement of actuator performance. The material used for fabricating the actuator is RTV-2 silicone rubber. In this study, the Cauchy stress was expanded for hyperelastic models and the best model to express the stress-strain behaviour based on ASTM D412 Type C tensile test for this material has been obtained. The results show that the greatest bending angle was achieved for the semi-elliptical actuator made of RTV2 material with a pitch of 1.5 mm and second layer thickness of 1 mm. In comparison, the maximum response force was obtained for the semi-elliptical actuator made of RTV2 material with a pitch of 6 mm and a second layer thickness of 2 mm. Additionally, this research opens up new possibilities for development of safer and more efficient robotic systems that can interact seamlessly with humans and their environment.

Estimation of Safety and Economical Efficiency of Large High Tension Bolted Joints (대직경 고장력볼트 이음부의 안전성 및 경제성 평가)

  • Sung, Ki-Tae;Kyung, Kab-Soo;Lee, Seung-Yong
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.13 no.6 s.58
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    • pp.97-105
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    • 2009
  • This study was conducted for the purpose of examinating the safety and economical efficiency of large high tension bolted joints. The specimen using F10T-M30 large high strength bolts has been selected and static tensile test has been conducted to evaluate the slip characteristics. In addition, finite element analysis has been carried out to estimate the number of required bolts. As a result, the average slip coefficient of M30 high strength bolts exceeded 0.4 - the standard in highway bridge design specification - and has satisfied the slip strength, which is the same as that of M22 high strength bolts. In addition, if F13T-M22 high strength bolts were applied, the number of required bolts decreased by 21%, and if F10T-M30 high strength bolts were applied, the number of required bolts decreased by 46%, that leads to the conclusion that the economical efficiency in accordance with diametering of high strength bolts was now verified.

Experimental Study on Compressive Strength of Concrete Column Retrofitted by Carbon FRP Sheet (탄소섬유시트로 보강된 콘크리트 기둥의 압축성능 평가를 위한 실험연구)

  • Yoo, Youn-Jong;Lee, Kyoung-Hun;Kim, Heecheul;Lee, Young-Hak;Hong, Won-Kee
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.12 no.3
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    • pp.119-126
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    • 2008
  • In 1980 and 1990's most of residential buildings were constructed with relatively low strength concrete of 18 MPa. And, columns were designed considering only vertical loads. In this study, compressive strength tests for low strength RC columns retrofitted by carbon fiber sheets were carried out. Carbon fiber sheet provides constructability and high tensile strength as well as good corrosion resistance characteristics. A pair of carbon sheets were wrapped with ${\pm}60^{\circ}$ angle with respect to longitudinal direction of RC column to increase structural capacity against axial and lateral load simultaneously. Strength and strain patterns and failure modes of specimens were analyzed and prediction equation of increased compressive strength of RC column confined by carbon fiber sheet was proposed based on regression analysis.