• Title/Summary/Keyword: Tensile properties

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Microstructural Evolution and Magnetic Property of Creep-Fatigued Ferritic 9Cr Heat-Resisting Steel (크리프-피로 손상된 페라이트기 9Cr 내열강의 미세조직 발달과 자기적 특성)

  • Kim, Chung-Seok;Kwun, S.I.;Park, Ik-Keun
    • Journal of the Korean Society for Nondestructive Testing
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    • v.27 no.5
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    • pp.417-425
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    • 2007
  • The ferritic 9Cr-1Mo-V-Nb heat-resisting steel was experimentally studied in order to characterize its microstructural evolution during creep-fatigue by coercivity measurement. The creep-fatigue test was conducted at $550\;^{\circ}C$ with the tensile holding time of 60s and 600s, respectively. The coercivity decreased until the failure and the hardness monotonously decreased for the whole fatigue life. As the life fraction of creep-fatigue increased, the $M_{23}C_6$ carbide coarsened following the Ostwald ripening mechanism. However, the MX carbonitrides did not grow during creep-fatigue due to so stable at $550\;^{\circ}C$. The width of martensite lath increased because of the dislocation recovery at the lath boundaries. The magnetic coercivity has an influence on the microstructural properties such as dislocation, precipitates and martensite lath boundaries, which interpreted in relation to microstructural changes. Consequently, this study proposes a magnetic coercivity to quantify the level of damage and microstructural change during the creep-fatigue of ferritic 9Cr-1Mo-V-Nb steel.

Lactobacillus casei strain C1 attenuates vascular changes in spontaneously hypertensive rats

  • Yap, Wei Boon;Ahmad, Faisal Malau;Lim, Yi Cheng;Zainalabidin, Satirah
    • The Korean Journal of Physiology and Pharmacology
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    • v.20 no.6
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    • pp.621-628
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    • 2016
  • Hypertension can be caused by various factors while the predominant causes include increase in body fluid volume and resistance in the circulatory system that elevate the blood pressure. Consumption of probiotics has been proven to attenuate hypertension; however, the effect is much strain-dependent. In this study, a newly isolated Lactobacillus casei (Lb. casei ) strain C1 was investigated for its antihypertensive properties in spontaneously hypertensive rats (SHR). Lactic acid bacteria (LAB) suspension of 11 log colony-forming unit (CFU) was given to SHR (SHR+LAB, n=8), and phosphate buffer saline (PBS) was given as a control in SHR (SHR, n=8) and in Wistar rats as sham (WIS, n=8). The treatment was given via oral gavage for 8 weeks. The results showed that the weekly systolic blood pressure (SBP), mean arterial pressure (MAP), diastolic blood pressure (DBP) and aortic reactivity function were remarkably improved after 8 weeks of bacterial administration in SHR+LAB. These effects were mostly attributed by restoration of wall tension and tensile stress following the bacterial treatment. Although not statistically significant, the level of malondialdehye (MDA) in SHR+LAB serum was found declining. Increased levels of glutathione (GSH) and nitric oxide (NO) in SHR+LAB serum suggested that the bacterium exerted vascular protection through antioxidative functions and relatively high NO level that induced vasodilation. Collectively, Lb. casei strain C1 is a promising alternative for hypertension improvement.

Preparation and characterization of PVDF/alkali-treated-PVDF blend membranes

  • Liu, Q.F.;Li, F.Z.;Guo, Y.Q.;Dong, Y.L.;Liu, J.Y.;Shao, H.B.;Fu, Z.M.
    • Membrane and Water Treatment
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    • v.7 no.5
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    • pp.417-431
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    • 2016
  • Poly(vinylidene fluoride) (PVDF) powder was treated with aqueous sodium hydroxide to obtain partially defluorinated fluoropolymers with expected properties such as improving hydrophilicity and fouling resistance. Raman spectrum and FT-IR results confirmed the existence of conjugated carbon double bonds after alkaline treatment. As the concentration increased, the degree of defluorination increased. The morphology and structure of membranes were examined. The permeation performance was investigated. The results showed that membrane's hydrophilicity increased with increase of the percentage of alkaline treated PVDF powder. Moreover, in terms of the water contact angle, it decreased from $92^{\circ}$ to a minimum of $68^{\circ}$; while water up take increased from 128 to 138%. Fluxof pure water and the cleaning efficiency increased with the increase of alkaline treated PVDF powder. The fouling potential also decreased with the increase of the percentage of alkaline treated PVDF powder. The reason that makes blending PVDF show different characteristics because of partial defluorination, which led the formation of conjugated C = C bonds and the inclusion of oxygen functionalities. The polyene structure followed by hydroxide attack to yield hydroxyl and carbonyl groups. Therefore, the hydrophilicity of blending membrane was improved. The SEM and porosity measurements showed that no obvious variations of the pore dimensions and structures for blend membranes were observed. Mechanical tests suggest that the high content of the alkaline treated PVDF result in membranes with less tolerance of tensile stress and higher brittleness. TGA results exhibited that the blend of alkaline treated PVDF did not change membrane thermal stability.

Polyethersulfone (PES) ultrafiltration (UF) membranes loaded with silver nitrate for bacteria removal

  • Basri, H.;Ismail, A.F.;Aziz, M.
    • Membrane and Water Treatment
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    • v.2 no.1
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    • pp.25-37
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    • 2011
  • PES UF membranes containing silver were prepared to impart antibacterial properties for waste water treatment. Asymmetric membranes for antibacterial application were prepared from polyethersulfone (PES) and silver nitrate ($AgNO_3$) (PES/$AgNO_3$=15/2 by weight) solution in N-Methyl-2-pyrrolidone (NMP) via simple wet phase inversion technique. These membranes were characterized by polyvinylpyrrolidone (PVP) and polyethylene glycol (PEG) of different molecular weights (1000 ppm in water) at room temperature and on operating pressure of 5 bars. It was observed that the water flux of PES-$AgNO_3$ membrane is slightly lower than virgin PES but still increased linearly with the increment of pressure applied. The morphology of the resulting membranes was examined using Field-Emission Scanning Electron Microscope (FESEM) coupled with Energy Dispersive Spectroscopy (EDS). Elemental analysis using EDS proved that silver is successfully loaded on the membrane surfaces. Due to the success of loading silver on membrane surfaces, antibacterial activities were evaluated via agar diffusion method against Escherichia coli (E.coli) and Staphylococcus aureus (S.aureus) culture. By incorporating 2 wt% of silver nitrate, PES-$AgNO_3$ showed significant inhibition ring on both E.coli and S.aureus. Filtration of E.coli solution (OD 0.31) showed satisfactory rejection data with ~100% inhibition growth after 24 hours incubation at $37^{\circ}C$. Resultant membranes also exhibit better tensile strength (compared to virgin PES) up to 71% may be due to the suggested interactions. The residual silver during fabrication was measured using ICP-MS and result showed that the residual silver content of PES-$AgNO_3$ membrane was only ~1% of the original silver added in the polymer solution. These studies have shown that PES-$AgNO_3$ UF membranes are potential in improving the filtration in water treatment.

Full-range plasticity of novel high-performance low-cost stainless steel QN1803

  • Zhou, Yiyi;Chouery, Kim Eng;Xie, Jiang-Yue;Shu, Zhan;Jia, Liang-Jiu
    • Steel and Composite Structures
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    • v.35 no.6
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    • pp.739-752
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    • 2020
  • This paper aims to investigate cyclic plasticity of a new type of high-performance austenitic stainless steel with both high strength and high ductility. The new stainless steel termed as QN1803 has high nitrogen and low nickel, which leads to reduction of cost ranging from 15% to 20%. Another virtue of the new material is its high initial yield strength and tensile strength. Its initial yield strength can be 40% to 50% higher than conventional stainless steel S30408. Elongation of QN1803 can also achieve approximately 50%, which is equivalent to the conventional one. QN1803 also has a corrosion resistance as good as that of S30408. In this paper, both experimental and numerical studies on the new material were conducted. Full-range true stress-true strain relationships under both monotonic and cyclic loading were obtained. A cyclic plasticity model based on the Chaboche model was developed, where a memory surface was newly added and the isotropic hardening rule was modified. A user-defined material subroutine was written, and the proposed cyclic plasticity model can well evaluate full-range hysteretic properties of the material under various loading histories.

A study on the structural behaviour of functionally graded porous plates on elastic foundation using a new quasi-3D model: Bending and free vibration analysis

  • Kaddari, Miloud;Kaci, Abdelhakim;Bousahla, Abdelmoumen Anis;Tounsi, Abdelouahed;Bourada, Fouad;Tounsi, Abdeldjebbar;Bedia, E.A. Adda;Al-Osta, Mohammed A.
    • Computers and Concrete
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    • v.25 no.1
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    • pp.37-57
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    • 2020
  • This work investigates a new type of quasi-3D hyperbolic shear deformation theory is proposed in this study to discuss the statics and free vibration of functionally graded porous plates resting on elastic foundations. Material properties of porous FG plate are defined by rule of the mixture with an additional term of porosity in the through-thickness direction. By including indeterminate integral variables, the number of unknowns and governing equations of the present theory is reduced, and therefore, it is easy to use. The present approach to plate theory takes into account both transverse shear and normal deformations and satisfies the boundary conditions of zero tensile stress on the plate surfaces. The equations of motion are derived from the Hamilton principle. Analytical solutions are obtained for a simply supported plate. Contrary to any other theory, the number of unknown functions involved in the displacement field is only five, as compared to six or more in the case of other shear and normal deformation theories. A comparison with the corresponding results is made to verify the accuracy and efficiency of the present theory. The influences of the porosity parameter, power-law index, aspect ratio, thickness ratio and the foundation parameters on bending and vibration of porous FG plate.

Study on Mechanical Properties of Hybrid Resins by Milk Casein and Waterborne Polyurethane for Safety Management of Industrial Disaster (Milk casein과 수용성 폴리우레탄 resin을 이용한 산업 안전 방재용 하이브리드 film의 합성 및 기계적 물성에 관한 연구)

  • Lee, Joo-Youb;Kim, Ki-Jun
    • Journal of the Korean Applied Science and Technology
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    • v.29 no.2
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    • pp.356-363
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    • 2012
  • In this study we synthesis Hybrid resin(WPC) by milk casein and waterborne polyurethane(WPU). Then we experiment how casein effect to Hybrid resins in Full-Grain leather coatings. According to measured data for solvent resistance, WPU resin and Hybrid resins had good property. As test of tensile strength, WPU had most low strength(2.130 $kg_f/mm^2$) and WPC-3(WPU 91: casein resin 9) had most high strength(2.191 $kg_f/mm^2$). Also we knew that most good property of abrasion is WPC-3(50.090 mg.loss). In elongation case, WPU had most good result(637 %) in this experiment.

Effect of Special Heat Treatments and Alloying Element(Ni) on Strengthening and Toughening of Ductile Cast Iron (구상흑연주철의 강인화에 미치는 특수열처리와 합금원소의 영향)

  • Kim, Sug-Won;Choi, Young-Seon
    • Journal of Korea Foundry Society
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    • v.10 no.4
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    • pp.299-308
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    • 1990
  • Ductile cast iron has a good ductility and ductility and toughness than those of gray cast iron, because the shape of graphite is spheroidal. It has been reported that the strengthening and toughening of the ductile cast iron was resulted from the good modification of various matrix structures obtained by the heat treatment or addition of alloying elements. This study aims to investigate the effect of various special heat treatment(Cyclic Heat Treatment, Intermediate Heat Treatment, Step Quenching), austempering and alloying element(Ni) on the strength and toughness of ductile cast iron. The results obtained from this study are summarized as follows. 1) With addition of Ni, the amount of pearlite or bainite were increased and the morphologies of pearlite or bainite became finer by special heat treatments. 2) As the Ni added and not added ductile cast iron were treated by austenitizing at $900^{\circ}C$ and $840^{\circ}C$, in the latter the austenite was mostly formed in the vicinity of eutectic cell boundary, but in the former on the whole matrix. 3) In cyclic heat treatment, the volume fraction of pearlite was increased and the shape of pearlite was fined with increase of the number of cycle. 4) The shape of pearlite was mostly bar type in the intermediate heat treatment, but spheroidal type in step quenching. 5) The mechanical properties of ductile cast iron containing 1.5%Ni austempered at $400^{\circ}C$ for 25min. after austenitizing at $900^{\circ}C$ for 15min. were a good value of hardness 105(HRB), impact energy 12.5(kg.m), tensile strength 112($kg/mm^2$) and elongation 6.8(%).

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Development of a High Strength Al-Si-Mg Alloy for Rheo-diecasting (레오다이캐스팅을 위한 고강도 Al-Si-Mg 합금설계)

  • Park, Kyu-Sup;Jang, Young-Soo;Choi, Byoung-Hee;Kang, Byung-Kuen;Kim, Hae-Soo;Choi, Sang-Ho;Hong, Chun-Pyo
    • Journal of Korea Foundry Society
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    • v.32 no.2
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    • pp.98-103
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    • 2012
  • Recently, development of Al-based alloys for high mechanical performance has been an important issue in automotive industry. The present study focused on the design of a high strength Al-based alloy for rheo-diecasting. The research was based on thermodynamic calculation and experimentals to optimize the alloy compositions. Two important considerations were carried out: i) to obtain uniform slurry with fine and globular microstructures for rheo-diecasting, ii) to be strengthend by T6 heat treatment. In order to evaluate the effect of Si content on the slurry microstructure and castability, thermodynamic calculation and fluidity test were carried out. The effects of various alloying components, such as Mg, Cu and Zn, on age hardenability were also investigated. The mechanical properties of the rheo-diecasting products using the newly developed alloy are 324MPa in tensile strength, 289MPa in yield strength, and 11.2% in elongation after T6 heat treatment.

Fabrication Technology of Turbo Charger Housing for Riser Minimizing by Fusion S/W Application and its Experimental Investigation (압탕 최소화를 위한 터보차저하우징의 융합 S/W 응용 제조기술 및 실험적 검증)

  • Lee, Hak-Chul;Seo, Pan-Ki;Jin, Chul-Kyu;Seo, Hyung-Yoon;Kang, Chung-Gil
    • Journal of Korea Foundry Society
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    • v.37 no.1
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    • pp.1-13
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    • 2017
  • The purpose of this study is to increase the part recovery rate (to more than 70%) during the casting of a ductile cast iron turbo charger housing using a heater around the riser. Before creating a casting mold, various runner and riser systems were designed and analyzed with a casting simulation analysis tool. The design variables were the heater temperature, top insulation, riser location, riser diameter and the riser shape. During the feeding from the riser to the part, the reverse model was better than the forward model. When heating the riser (above $600^{\circ}C$), solidification of the riser was delayed and the feeding effect was suitable compared to that without heating. At a higher heating temperature, less solidification shrinkage and porosity were noted inside the part. On the basis of a casting simulation, eight molds were fabricated and casting experiments were conducted. According to the experimental conditions, external and internal defects were analyzed and mechanical properties were tested. The ultimate tensile strength and elongation outcome were correspondingly more than 540MPa and 5% after a heat treatment. In addition, a maximum part recovery rate of 86% was achieved in this study.