• 폴리머
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• 제25권2호
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• pp.160-167
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• 2001

특성이 서로 다른 polyimide (PI) 전구체와 polyamideimide (PAI) 블렌드물을 solvent casting법으로 제조한 후 열처리하여 다양한 조성의 PI/PAI 복합체를 제조하였다. Poly(amic acid) (PAA)를 전구체로 사용한 PAA/PAI 복합체의 경우 산-염기에 의한 ionic force 또는 수소 결합에 의한 분자간력으로 인하여 좋은 혼화성을 나타냈지만, poly(amic dimethyl ester) (PAME)를 전구체로 사용한 PAME/PAI 복합체는 약화된 분자간력으로 인하여 상분리가 뚜렷하게 발생함을 편광 현미경을 통해 관찰하였다. 전구체의 종류에 관계없이 이미드화된 복합체의 인장 탄성 계수는 선형치보나 증가하였으나 PAI 매트릭스 영역에서의 인장강도 및 전 혼합 조성에서의 파단 변형률은 감소하였다 상대적으로 낮은 유리 전이 온도를 가진 PAI에 의한 가소화 때문에 열적 이미드화 과정 중에 PI 분자쇄의 재정렬이 촉진됨을 편광현미경 및 X-선 회절 결과로부터 확인하였다.

• 대한안전경영과학회:학술대회논문집
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• 대한안전경영과학회 2009년도 추계학술대회
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• pp.471-481
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• 2009

This study is deal with the high frequency induction hardening (HF at $850^{\circ}C$, 120kHz & 50kW condition) SM45C steel. (1) The HF specimen which was tempered at $150^{\circ}C$, did not appear any tempering effect. A brittle fracture occurred at rounded area of the tensile specimen. AE amplitude distribution showed between 45~60dB. (2) The HF specimen which was tempered at $300^{\circ}C$, slip and fracture occurred at the hole area of the tensile specimen. As it passes the yield point, the AE energy increased intermittently and AE amplitude distribution showed between 70~85dB. In addition, after the maximum tensile load, it showed high amplitude and energy distribution. The AE amplitude showed between 45~70dB. (3) The HF specimen which was tempered at $450^{\circ}C$, a brittle fracture occurred as if it is torn in the direction of $45^{\circ}$ on parallel area over the both sides of the tensile specimen, which led to several peak to be appeared in AE energy. It was found that the AE amplitude was relatively low and the AE energy was high.

• Corrosion Science and Technology
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• 제2권6호
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• pp.266-271
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• 2003

Safety diagnosis of various structural components and facilities is indispensable for preventing catastrophic failure of material by time-dependent and environment accelerating degradation. Also, this diagnosis of operating components should be done periodically for safe maintenance and economical repair. However, conventional standard methods for mechanical properties have the problems of bulky specimen, destructive procedure and complex procedure of specimen sampling. So, a non-destructive and simple mechanical testing method using small specimen is needed. Therefore, an advanced indentation technique was developed as a potential method for non-destructive testing of in-field structures. This technique measures indentation load-depth curve during indentation and analyzes the mechanical properties related to deformation such as yield strength, tensile strength and work-hardening index. In this paper, we characterized the tensile properties including yield and tensile strengths of the V-modified Cr-Mo steels in petro-chemical and thermo-electrical plants. And also, the effects of hydrogen-assisted degradation of the V-modified Cr-Mo steels were analyzed in terms of work-hardening index and yield ratio.

• 대한금속재료학회지
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• 제47권1호
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• pp.1-6
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• 2009

Magnesium alloys are drawing a lot of attention and have been extensively studied. The major obstacle to the practical application of the alloys is the poor formability at room temperature, originating basically from the insufficient number of slip system. Development of a proper texture is one promising solution to improve the formability. In the present work, after extrusion and full annealing, microstructures, texture developments and tensile properties of AZ31 Mg alloys are studied. After full annealing strong <1010>||ED fiber texture and weak <1120>+<1230>||ED fiber texture (c-axes in the radial direction) were developed. The textures are distinctly influencing the tensile properties, which can be understood in terms of the activation of basal slip modes. With the random orientation, which is developed in the $45^{\circ}$ sample to the extrusion direction, the better workability can be achieved at room temperature.

• 한국초전도ㆍ저온공학회논문지
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• 제24권1호
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• pp.8-12
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• 2022

Recently, research on applying composite materials to various industrial fields is being actively conducted. In particular, composite materials fabricated by Fused Deposition Modeling 3D printers have more advantages than existing materials as they have fewer restrictions on manufacturing shape, reduce the time required, weight. With these advantages, it is possible to consider utilizing composite materials in cryogenic environments such as the application of liquid oxygen and liquid hydrogen, which are mainly used in an aerospace and mobility. However, FDM composite materials are not verified in cryogenic environments less than 150K. This study evaluates the characteristics of composite materials such as tensile strength and strain using a UTM (Universal Testing Machine). The specimen is immersed in liquid nitrogen (77 K) to cool down during the test. The specimen is fabricated using 3D print, and can be manufactured by stacking reinforced fibers such as carbon fiber, fiber glass, and aramid fiber (Kevlar) with base material (Onyx). For the experimental method and specimen shape, international standards ASTM D638 and ASTM D3039 for tensile testing of composite materials were referenced.

• 한국염색가공학회지
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• 제34권2호
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• pp.102-108
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• 2022

The physicochemical properties of stainless steel fibers which were modified by oxygen plasma treatment were analyzed through microscopy and XPS analysis. The wettability of the surface of the stainless steel fiber was observed by measuring water contact angle to find out the effect of the plasma treatment time on the surface characteristics of the stainless steel fiber. In addition, in order to understand the effect of oxygen plasma treatment on the deterioration of the stainless steel fiber properties, the physical properties due to plasma treatment was investigated by measuring the weight reduction, tensile strength, elongation, tensile modulus of the stainless steel fibers according to the treatment time. As a result, the stainless steel fiber surface was etched by the oxygen plasma and the surface became more wettable by the introduction of hydrophilic functional groups. However the physical properties of the stainless steel fiber were not significantly deteriorated even if the surface of the stainless steel fiber made hydrophilic.

• 한국압력기기공학회 논문집
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• 제19권1호
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• pp.11-19
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• 2023

Additive manufacturing technology, called as 3D printing, is one of fourth industrial revolution technologies that can drive innovation in the manufacturing process, and thus should be applied to nuclear industry for various purposes according to the manufacturing trend change in the future. In this paper, we performed tensile tests of 3D printed stainless steel 316L as-built specimens manufactured by two types of technology; DED (Directed Energy Deposition) and PBF (Powder Bed Fusion). Their mechanical properties (tensile strength, yield strength, elongation and reduction of area) were compared. As a result of comparison, the mechanical properties of the PBF specimens were slightly better than those of DED specimens. In the same additive type of specimens, the tensile and yield strength of specimens in the X and Y direction were higher than those in the Z direction, but the elongation and ROA were lower.

• 한국수소및신에너지학회논문집
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• 제33권2호
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• pp.176-182
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• 2022

Since the various characteristics of the polymer electrolyte membrane are not clearly identified, it is difficult to predict and design applications for various conditions. In this study, as a previous study on the aging of the polymer electrolyte membrane, a study was conducted on the change of mechanical properties according to the aging of the polymer electrolyte membrane. Through the tensile test of Nafion 117, the mechanical properties change due to aging was confirmed. As a result of the tensile test, it was confirmed that the aged Nafion 117 had reduced tensile strength. Through DSC measurement, aged Nafion confirmed that the glass transition temperature and enthalpy change were low, which is thought to be the effect of molecular motion and transition due to the lapse of time. The effect is thought to cause a difference in the amount of change in enthalpy, resulting in a difference in mechanical properties during tension.

• 마이크로전자및패키징학회지
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• 제27권3호
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• pp.77-81
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• 2020

차세대 디스플레이 시장을 선도하기 위해서는 롤러블(rollable), 폴더블(foldable) 디스플레이와 같은 플렉서블(flexible) OLED 디스플레이의 상용화 및 양산화가 필수적이나, 실제 공정 및 굽힘 과정에서 발생하는 극심한 박막 내부 응력 변화로 인한 기계적 파손 문제가 심각한 상황이다. 따라서, 플렉서블 디스플레이 구조에 사용되는 박막 재료의 기계적 물성을 파악하는 것은 제품의 강건한 설계 및 구조 최적화에 필수적이다. 본 논문에서는 물 표면 플랫폼을 이용한 나노 박막 인장 시험법을 적용하여 플렉서블 디스플레이 패널에 적용되는 금속 및 세라믹 박막 소재들의 인장 물성을 정량적으로 측정하였다. 스퍼터링(Sputtering)으로 증착된 Mo, MoTi 나노 박막과, 플라즈마 강화 화학 기상 증착법(Plasma Enhanced Chemical Vapor Deposition, PECVD)으로 증착된 SiN_x 나노 박막의 탄성 계수와 인장 강도 및 연신율을 측정하는 데 성공하였다. 결과적으로 박막의 증착 조건 및 두께에 따라 기계적 물성이 크게 변화할 수 있음을 확인하였으며, 측정된 인장 물성은 기계적으로 강건한 롤러블, 폴더블 디스플레이의 설계를 위한 응력 해석 모델링 데이터로 활용될 수 있을 것으로 기대한다.

• 보존과학회지
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• 제32권2호
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• pp.223-234
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• 2016

2액형 에폭시 수지는 문화재 보존처리에 매우 광범위하게 사용되고 있으나 사용 시 주제와 경화제의 배합비율에 따라 경화특성, 기계적 강도, 화학 구조 등이 달라질 수 있고 대상 문화재의 안정성에 영향을 미칠 수 있다. 설문조사 결과, 보존처리 실무자들은 소량의 에폭시수지를 눈대중으로 혼합하거나 가사시간을 줄이기 위해 인위적으로 경화제를 과량 첨가하는 경우가 있는 것으로 조사되었다. 이 연구에서는 속경화형 2종과 일반경화형 2종의 에폭시수지를 대상으로 주제에 대한 경화제의 비율을 0.25~4배로 설정하여 각 경우의 경화특성, 기계적 강도, 화학 작용기를 분석하였다. 그 결과 속경화형 에폭시수지는 경화제가 0.5~2배일 때 높은 반응열과 함께 경화반응이 빠르게 나타났으며, 경화제 비율이 제조사에서 공시된 정비율보다 적을 때 더 높은 기계적 강도가 나타났고 에폭시의 가교결합도 활발히 일어난 것으로 관찰되었다. 일반경화형 에폭시수지는 대부분 경화반응열이 낮고 느린 반응속도로 경화가 진행되며, 경화제가 정비율 이하에서 가장 높은 기계적 강도를 나타냈다. 그러나 경화제 비율이 2배 이상 일 때는 경화속도가 매우 느려지고 접착강도도 낮아지는 것으로 나타났다. 따라서 배합비가 정비율 이하에서는 비교적 빠른 반응속도와 유사한 기계적 강도를 나타내는 반면 정비율 이상에서는 물성이 급격하게 저하되므로 구현하고자 하는 성능에 영향을 미칠 수 있을 것으로 판단된다.