• Journal of Power System Engineering
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• v.20 no.3
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• pp.11-16
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• 2016

The effect of carbides on the tensile properties in 0.5C-17Cr-0.5Ni martensitic stainless steel was studied. With the increase of austenitizing temperature, the volume fraction of residual carbide was decreased rapidly. In tempered specimens after quenching, the volume fraction of total carbide was decreased with the increase of austenitizing temperature. In tempered specimens after quenching, strength was decrease and elongation was increased with the increase of austenitizing temperature. Tensile strength was increase and elongation was decreased with the increase of volume fraction of residual and total carbides. With the increase of austenitizing temperature, the tensile properties of mod. 0.5C-17Cr-0.5Ni martensitic stainless was affected greatly by residual carbide than tempered carbide.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2006.05a
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• pp.95-96
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• 2006

This study examined the effects of the tempering temperatures($360-420^{\circ}C$) on the mechanical properties of the carbon tool steel (SK4M) for flat spring. Hardness test, tensile test and fatigue test were performed at room temperature($20^{\circ}C$). The tensile strength and yield strength of $390^{\circ}C\;and\;420^{\circ}C$ tempered SK5M were 0.93-0.97 times and 0.81-0.87 times those of $360^{\circ}C$ tempered SK5M, respectively. The fatigue limit of $360-420^{\circ}C$ tempered SK5M were 35-40% of tensile strength of $360-420^{\circ}C$ tempered SK5M, respectively.

• Korean Journal of Metals and Materials
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• v.47 no.7
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• pp.406-415
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• 2009

A study was conducted on the effects of carbon, tungsten, and vanadium on the wear properties and surface roughness of four High Speed Steel (HSS) rolls manufactured by the centrifugal casting method. Hot-rolling simulation tests were carried out using a high-temperature wear tester capable of controlling speed, load, and temperature. HSS rolls contained a large amount (up to 25 vol.%) of carbides such as MC, $M_{2}C$, $M_{7}C_{3}$, and $M_{6}C$ carbides formed in the tempered martensite matrix. The matrix consisted mainly of lath tempered martensite when the carbon content in the matrix was small, and contained a considerable amount of plate tempered martensite when the carbon content increased. The high-temperature wear test results indicated that the wear properties and surface roughness of the rolls improved when the amount of hard MC carbides formed inside solidification cells increased. The rolls distribution was also homogeneous. The best wear properties and surface roughness were obtained from a roll where a large amount of MC carbides was homogeneously distributed in the lath tempered martensite matrix. The proper contents of carbon equivalent, tungsten equivalent, and vanadium were 2.0~2.3%, 9~10%, and 5~6%, respectively.

• Journal of Welding and Joining
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• v.34 no.3
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• pp.61-68
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• 2016

Characteristics of dissimilar metal welds between alloy steel ASTM A387 Gr. 91 and carbon steel ASTM A516 Gr.70 made with Flux cored arc welding(FCAW) have been evaluated in terms of microstructure, mechanical strength, chemical analysis by EDS as well as corrosion test. Three heat inputs of 15.0, 22.5, 30.0kJ/cm were employed to make joints of dissimilar metals with E91T1-B9C wire. Post-weld heat treatment was carried out at $750^{\circ}C$ for 2.5 h. Based on microstructural examination, tempered martensite and lower bainite were formed in first layer of weld metal. The amount of tempered martensite was decreased and the amount of lower bainite was increased with increasing heat input and layer. Heat affected zone of alloy steel showed the highest hardness due to the formation of tempered Martensite and lower Bainite. Tensile strengths of dissimilar welds decreased with increasing heat inputs. Dissimilar welds seemed to have a good hot cracking resistance due to the low HCS index below 4. The salt spray test of dissimilar metals showed that the corrosion rate increased with increasing heat inputs due to the increase of the amount of lower Bainite.

• Korean Journal of Materials Research
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• v.25 no.12
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• pp.666-671
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• 2015

In this study, we investigated the effect of the residual carbides and tempered carbides precipitated by tempering treatment after quenching on the pitting corrosion of mod. 440A martensitic stainless steel. In quenched specimens and tempered specimens after quenching of mod. 440A martensitic stainless steel, the volume fraction of the residual carbides and total carbides decreased with the increase of the austenitizing temperature. Pitting resistance increased with the increase of austenitizing temperature. With the increase of the volume fraction of the residual and total carbides, the pitting resistance of mod. 440A martensitic stainless steel was decreased. The pitting resistance of mod. 0.5C-17Cr-0.5Ni 440A martensitic stainless steel had stronger affected by residual carbides than precipitated carbides produced by tempering.

• Journal of the Korean Society for Heat Treatment
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• v.23 no.3
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• pp.156-162
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• 2010

The modified 9Cr-1Mo steel (P91 steel) is very popular as a boiler tube material of the USC (Ultra-Supercritical) power plants. The steels were tempered in the temperature range of 400 to $650^{\circ}C$ and the mechanical tests, such as impact and hardness tersts were performed at the room temperature for the tempered steels. A drop in the impact value (embrittlement) and the hardeness increase were simultanously observed in the range of temperature between $475^{\circ}C$ and $600^{\circ}C$, particularly at $550^{\circ}C$. TEM observation shows the hardening was caused by $M_2C$, resulting in the embrittlement. And the maximum volume fraction of $M_3C$ was also observed at $550^{\circ}C$, Therefore, the embrittlement seems to be caused by both the $M_2C$ and $M_3C$.

• Applied Microscopy
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• v.45 no.3
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• pp.170-176
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• 2015

In this work, various electron microscopy and analysis techniques were used to investigate the microstructural evolution of a 9% Cr tempered martensite ferritic (TMF) steel T91 upon ultrasonic nanocrystalline surface modification (UNSM) treatment. The micro-dimpled surface was analyzed by scanning electron microscopy. The characteristics of plastic deformation and gradient microstructure of the UNSM treated specimens were clearly revealed by crystal orientation mapping of electron backscatter diffraction (EBSD), with flexible use of the inverse pole figure, image quality, and grain boundary misorientation images. Transmission electron microscope (TEM) observation of the specimens at different depths showed the formation of dislocations, dense dislocation walls, subgrains, and grains in the lower, middle, upper, and top layers of the treated specimens. Refinement of the $M_{23}C_6$ precipitates was also observed, the size and the number density of which were found to decrease as depth from the top surface decreased. The complex microstructure and microstructural evolution of the TMF steel samples upon the UNSM treatment were well-characterized by combined use of EBSD and TEM techniques.

• Nuclear Engineering and Technology
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• v.46 no.3
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• pp.413-422
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• 2014

Presented in this study are the variations of microstructures and mechanical properties with tempering and Post-Weld Heat Treatment (PWHT) conditions for SA508 Gr.4N steel used as Reactor Pressure Vessel (RPV) material. The blocks of model alloy were austenitized at the conventional temperature of $880^{\circ}C$ then tempered and post-weld heat treated at four different conditions. The hardness and yield strength decrease with increased tempering and PWHT temperatures, but impact toughness is significantly improved, especially in the specimens tempered at $630^{\circ}C$. The sample tempered at $630^{\circ}C$ with PWHT at $610^{\circ}C$ shows optimum mechanical properties in hardness, strength, and toughness, excluding only the transition property in the low temperature region. The microstructural observation and quantitative analysis of carbide size distribution show that the variations of mechanical properties are caused by the under-tempering and carbide coarsening which occurred during the heat treatment process. The introduction of PWHT results in the deterioration of the ductile-brittle transition property by an increase of coarse carbides controlling cleavage initiation, especially in the tempered state at $630^{\circ}C$.

• Journal of the Korean Society of Industry Convergence
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• v.22 no.6
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• pp.681-688
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• 2019

SM45C steel, which is widely used for mechanical structure, was carburized at 870℃ for 4 hours and tempered at 300℃ and 400℃ for 1, 3 and 6 hours. The tempered materials were evaluated for tensile test, hardness test and impact test. In particular, the hardness and the absorption energy were evaluate the reliability by the Weibull statistical analysis. 300℃-1h specimen is considered to be the best heat treatment condition in the tensile stress and the observation of fracture surface. 300℃-1h specimen showed larger shape and scale parameter than the other specimens, and Rockwell hardness variance was small and showed the best characteristics. 400℃-3h specimen showed larger shape and scale parameter than the other specimens, the dispersion of impact absorption energy is small, and showed excellent characteristics.

• Bulletin of the Society of Naval Architects of Korea
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• v.21 no.1
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• pp.35-42
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• 1984

In the present study, rotating bending fatigue tests have been carried out in three kinds of carbon steel specimens; an annealed low carbon steel, an annealed high carbon steel and quenched-tempered high carbon steel; with a small artificial surface defect that might exist in real structures. Fatigue crack lengths have been observed by a method of replication in order to investigate the growth characteristic of fatigue crack in the viewpoints of strength of materials and fracture mechanics. The main results obtained are as follows: 1) The effect of a small surface defect upon the reduction of fatigue limit is considerably large, and the rate of fatigue limit reduction grows in the following order; annealed low carbon steel(mild steel), annealed high carbon steel, quenched-tempered high carbon steel. 2) When the growth rate of surface crack length(2a) was investigated in the viewpoints of fracture mechanics based upon $ ${\Delta}K_{\varepsilon}$, the dependence of stress level and of surface defect size disappear, and there exists a linear relationships between d(2a)/dN and ${\Delta}K_{{\varepsilon}t},\;\Delta_{{\varepsilon}t}\sqrt{{\pi}a}$, on log. plot, i.e, $d(2a)/dN={C{\cdot}{\Delta}K_{\varepsilon}}^3_t$, where ${\Delta}_{{\varepsilon}t}\sqrt{{\pi}a}$ a is the cyclic total strain intensity factor range.