• 제목/요약/키워드: Temperature control curing

검색결과 142건 처리시간 0.031초

의치상용 자가중합레진의 중합조건에 따른 파괴인성 (FRACTURE TOUGHNESS OF SELF-CURING DENTURE BASE RESINS WITH DIFFERENT POLYMERIZING CONDITIONS)

  • 정수양;김지혜;양병덕;박주미;송광엽
    • 대한치과보철학회지
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    • 제43권1호
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    • pp.52-60
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    • 2005
  • Purpose. The intent of this study was to evaluate the effects of curing conditions on self-curing denture base resins to find out proper condition in self-curing resin polymerization. Materials and methods, In this study, 3 commercial self-curing denture base resins are used Vertex SC, Tokuso Rebase and Jet Denture Repair Acrylic. After mixing the self curing resin, it was placed in a stainless steel mold(3$\times$6$\times$60mm). The mold containing the resin was placed under the following conditions: in air at 23$^{\circ}C$; or in water at 23$^{\circ}C$; or in water at 23$^{\circ}C$ under pressure(20psi); or in water at 37$^{\circ}C$ under pressure(20psi) or in water at 50$^{\circ}C$ under pressure(20psi) , or in water at 65$^{\circ}C$ under pressure(20psi), respectively. Also heat-curing denture base resin is polymerized according to manufactures' instructions as control. Fracture toughness was measured by a single edge notched beam(SENB) method. Notch about 3mm deep was carved at the center of the long axis of the specimen using a dental diamond disk driven by a dental micro engine. The flexural test was carried out at a crosshead speed 0.5mm/min and fracture surface were observed under measuring microscope. Results and conclusion . The results obtained were summarized as follows : 1. The fracture toughness value of self-curing denture base resins were relatively lower than that of heat-curing denture base resin. 2. In Vertex SC and Jet Denture Repair Acrylic, higher fracture toughness value was observed in the curing environment with pressure but in Tokuso Rebase, low fracture toughness value was observed but there was no statistical difference. 3. Higher fracture toughness value was observed in the curing environment with water than air but there was no statistical difference. 4. Raising the temperature in water showed the increase of fracture toughness.

Thermal cracking assessment for nuclear containment buildings using high-strength concrete

  • Yang, Keun-Hyeok;Mun, Jae-Sung;Kim, Do-Gyeum;Chang, Chun-Ho;Mun, Ju-Hyun
    • Computers and Concrete
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    • 제26권5호
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    • pp.429-438
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    • 2020
  • To shorten the construction times of nuclear facility structures, three high-strength concrete mixtures were developed with specific consideration given to their curing temperatures, their economic efficiency, and the practicality of their quality control. This study was conducted to examine the temperature rise profiles of these three concrete mixtures and the potential for early-age thermal cracking in the primary containment vessel of a nuclear reactor with a wall thickness of 1200 mm. The one-layer placement height of the concrete for the primary containment vessel was increased from the conventional 3 m to 3.5 m. A nonlinear finite element analysis (FEA) was conducted using the thermal properties of concrete determined from the isothermal hydration and adiabatic hydration tests, and tuned through comparisons made with temperature rise profiles obtained for 1200-mm-thick mock-up wall specimens cured at temperatures of 5, 20, and 35℃. The hydration heat performance of the three concrete mixtures and their potential to produce thermal cracking in nuclear facilities indicate that the mixtures have considerable potential for practical application to the primary containment vessel of a nuclear reactor at various curing temperatures, fulfilling the minimum requirements of the ACI 301 and minimizing the likelihood of the occurrence of thermal cracks.

Urea-Formaldehyde 수지가공포에 있어 Resorcinol의 유리 Formaldehyde 포착효과 (Effect of Resorcinol as Free Formaldehyde Scavenger for Fabric Finished with Urea-formaldehyde Precondensate.)

  • Kang, In-Sook;Kim, Sung-Reon
    • 한국염색가공학회지
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    • 제9권2호
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    • pp.41-49
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    • 1997
  • To control free formaldehyde release from fabric finished with N-methylol compounds, resin finished cotton fabric was treated with resorcinol solution, dried and cured. Factors affecting to control formaldehyde release have been investigated. It was shown that the aftertreatment with resorcinol greatly suppressed the free formaldehyde release. Up to concentration of about 5% of resorcinol, the concentration of resorcinol effected on the control of free and evolved formaldehyde. And at high concentration of resorcinol, however, the concentration became rather insensitive to contol formaldehyde release. Addition of some salt catalysts such as ammonium chloride, zinc nitrate, sodium acetate and ammonium acetate, was effective in decreasing formaldehyde release. Considering the effect on the control of formaldehyde and crease recovery, ammonium acetate was concidered to be the best catalyst. It was observed that the optimum curing temperature for the resorcinol treatment was about 15$0^{\circ}C$, and that the curing time did not affected formaldehyde release over three minutes. Although the treatment of resorcinol had a little adverse effect on crease recovery of resin finished fabric, this effect could be negligible.

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Effects of Hardener and Extender Contents on Curing Behavior of Urea-Melamine-Formaldehyde Resin

  • Eom, Young-Geun;XU, Guang-Zhu;Lee, Young-Kyu;Kim, Hyun-Joong
    • Journal of the Korean Wood Science and Technology
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    • 제36권5호
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    • pp.42-48
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    • 2008
  • This study was conducted to discuss the effects of hardener and extender contents on peak temperature, reaction enthalpy (${\Delta}H$), gelation time, viscosity change, and pH value in three types of UMF (urea-melamine- formaldehyde) resin with the help of perpHecT LogR meter, differential scanning calorimetry (DSC), and advanced rheometric expansion system (ARES), The results indicated that the pH value of Control A steeply decreased to 5,2 in the early stage but relatively remained constant thereafter as in Synthesis 1 and Synthesis 2, The peak temperature and time decreased as well, whereas ${\Delta}H$ and viscosity increased with the increase of hardener content. On the other hand, ${\Delta}H$ was not changed up to the extender content of 5% and then decreased with its further addition, And the pH value and peak temperature showed no change with the increase of extender content at the hardener content of 5% in three types of UMF resin, The effect of hardener content in this experiment, however, appeared more conspicuous in Control A than in the other two types of Synthesis 1 and Synthesis 2, These results might be caused by higher molecular weight with longer chains of methylene ($-CH_2-$) and methylene ($-CH_2-O-CH_2-$) ether bridges or much more branched chains in Control A.

큐어링 후 저장에 따른 고구마 저장뿌리 단백질체의 비교분석 (Comparative proteome profiling in the storage root of sweet potato during curing-mediated wound healing)

  • 신호용;지창윤;김호수;정정성;최성환;곽상수;김윤희;이증주
    • Journal of Plant Biotechnology
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    • 제50권
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    • pp.1-10
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    • 2023
  • 고구마(Ipomoea batatas L. Lam)는 영양소, 가공 식품, 동물 사료 및 색소 재료의 유용한 공급원으로 이용 가능한 경제적으로 중요한 대표적인 뿌리 작물이다. 일반적으로 고구마의 저장 뿌리는 수확 후 저장 기간 동안 다양한 미생물과 질병에 의한 부패에 노출되기 쉽다. 수확 후 큐어링은 저장기간 동안 상처를 치유하고 미생물에 의한 부패를 방지하기 위한 가장 적합한 수단으로 알려져 있다. 본 연구에서는 큐어링과 연관된 분자적 기작에 관여하는 단백질들을 확인하기 위해, 큐어링 처리 후 저장기간 동안 단백질체의 변화를 분석하였다. 33℃ (큐어링) 및 15℃ (대조군)에서 3일 동안 처리하고 8주의 저장 기간이 지난 후 2D 전기영동 분석을 통해 단백질 spot의 변화를 확인한 결과, 31개 단백질 spot의 발현량이 차이 나는 것을 확인하였으며, 이들 중 15개의 단백질 spot을 동정하여 그 특성을 분석하였다. 동정된 단백질 중 alphaamylase (spot 1)는 큐어링 처리구에서만 발현량이 증가하였으며, probable aldo-keto reductase 2-like (spot 3) 및 hypothetical protein CHGG_01724 (spot 4)는 큐어링 및 대조구에서 동시에 발현량이 증가하였으나, sporamin A (spot 10)는 큐어링 및 대조구에서 발현량이 감소하였다. 한편, 대조구에서 enolase (spot 14)는 발현량이 증가하였으나, chain A of actinidin-E-64 complex+ (spot 19), ascorbate peroxidase (spot 22) 및 여러 sporamin 단백질들(spot 20, 21, 23, 24, 27, 29, 30 및 31)은 발현량이 감소하였다. 본 연구의 결과는 고구마 저장 뿌리에서 큐어링 처리와 관련된 단백질의 동정 및 수확 후 저장 기간동안 병 저항성과 관련된 기작에 대한 이해를 높이며, 향후 저온 저장 능력이 향상된 신품종 개발을 위한 후보 유전자의 도출에도 기여할 수 있을 것이다.

콘크리트 포장 양생제의 적정살포량 결정 연구 (Determination of Proper Application Rate of Curing Compound for Cement Concrete Pavement)

  • 김장락;서영찬;안성순
    • 한국도로학회논문집
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    • 제7권2호
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    • pp.45-55
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    • 2005
  • 시멘트 콘크리트 포장은 시공초기의 품질관리가 포장의 장기공용성에 큰 영향을 주는 것으로 알려져 있다. 따라서 시공초기에 발생되는 문제점을 최소화하기 위한 다양한 연구가 국내외에서 활발하게 진행되고 있다. 일반적으로 시멘트 콘크리트의 품질관리에서 양생은 중요한 사항이며, 포장용 시멘트 콘크리트에서도 양생시에 양생제를 사용하여 슬래브 표면에 불투수 막을 형성하여 수분증발을 방지하는 피막양생 (membrane curing)을 많이 사용하고 있다. 양생제의 역할은 콘크리트 표면의 수분증발억제에 있다. 국내에서 사용되고 있는 양생제는 시공품질관리 측면에서 살포량이 적정한지에 대한의문이 계속 제기되어 왔다. 본 연구에서는 시멘트 콘크리트 포장 시공시 살포되는 양생제의 양을 조정하여 다양한 살포량에 따른 증발량 관측을 통해 양생제 살포량과 수분증발량 변화와의 상관관계를 제시하였다. 이를 위해 2002년과 2003년 여름철에 고속도로 시공현장에서 4회에 걸쳐 다양한 양생제 살포량$(0에 따른 증발량 콘크리트 포장의 온도변화, 콘크리트 표면의 강도발현속도(초음파 전달속도) 등을 측정하였다. 본 연구에서 얻은 결론은 현재 국내 시공현장에서의 양생제 살포량은 약 $160ml/m^2$으로 나타났고, 수분증발은 억제하고 적정한 보습효과를 얻기 위한 최적 양생제 살포량은 약 $400ml/m^2$인 것으로 분석되었다. 강도발현속도 시험결과 양생제의 살포량의 변화가 장기강도에 큰 영향을 미치지 않는 것으로 판단되었다.

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치과 3D 프린팅용 자외선 경화 레진에 광원의 두 가지 파장에 따른 경화 및 항온수조 침적에 따른 변형률의 비교 분석 (Comparative analysis of strain according to two wavelengths of light source and constant temperature bath deposition in ultraviolet-curing resin for dental three-dimensional printing)

  • 김동연;이광영;강후원;양천승
    • 대한치과기공학회지
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    • 제42권3호
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    • pp.208-212
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    • 2020
  • Purpose: This study aimed to analyze the shrinkage and expansion strain of ultraviolet (UV)-cured resin according to the wavelength of the light source and compare the shrinkage and expansion. Methods: We prepared the mold with according to the ISO 4049 specimen. The size of the circle in the mold was prepared with a height of 6.02 mm and a diameter of 4 mm. UV-curable resin for three-dimensional (3D) printing was injected into the circular mold. The control group was irradiated with a wavelength of 400~405 nm using UV-curing equipment (400 group), and the experimental group was irradiated with a wavelength of 460~465 nm (460 group). Both groups were produced ten specimens. The produced specimen was first measured with a digital micrometer. After the first measurement, the specimen was immersed in a constant temperature water bath for 15 days, after which the second measurement was performed, and the third measurement was taken after 30 days. The measured values were analyzed using the independent sample t-test (α=0.05). Results: In the non-immersion water tank, the contraction was 0.9% in the 400 group and 1.3% in the 460 group. In the constant temperature bath, the expansion was high at -0.4% in the 400 group for 15 days, and the smallest expansion was -0.03% for the 400 group for 30 days. There were significant differences between the two groups (p<0.05). Conclusion: The 400 group had a lower UV resin specimen strain than the 460 group. Therefore, it is recommended to use the wavelength required by the UV-curing resin.

석유계 피치가 첨가된 고온 탄소복합재용 페놀수지의 열 유변학적 거동 연구 (Thermo-rheological behaviors of Phenolic Resins Blended with Petroleum-based Pitches for High Temperature Carbon Composites)

  • 양재연;국윤수;서민강;김병석
    • Composites Research
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    • 제33권6호
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    • pp.329-335
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    • 2020
  • 본 연구에서는 각각에 다른 연화점을 갖는 석유계 피치의 열 유변학적 특성을 연구하였으며, 이를 함침용 페놀수지에 석유계 피치를 첨가하여 B-stage 형태의 페놀수지/석유계 피치 혼합물을 제조하였다. 그 결과, 연화점이 다른 석유계 피치는 QI의 함량이 증가할수록 피치의 유동성이 감소하였고, 고체의 점탄성 특성을 나타내었다. 또한, 다른 연화점을 갖는 석유계 피치를 페놀수지에 첨가함으로써, 페놀수지의 경화거동과 열 유변학적 특성에 미치는 영향에 대해 고찰하였을 때, 다른 연화점의 석유계 피치를 첨가함에 따라 페놀수지의 경화속도 및 경화거동을 조절할 수 있었으며, 이 중 P-Pitch 2가 첨가된 페놀수지 혼합물의 경우 동일한 경화 온도조건에서 다른 혼합물에 비해 유동성이 높은 것을 확인할 수 있었다.

요통치료에서 보법의 영향 (The Influence of Walking on Low Back Pain)

  • 박서희;장상철;나삼식;안훈모
    • 대한의료기공학회지
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    • 제14권1호
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    • pp.63-82
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    • 2014
  • This study is aimed to verify effects of Walking in treating hospitalized patients with low back pain in the Korean medicine hospital. The method of this study is choosing patients whose chief complaints were low back pain in the Korean medicine hospital in Gyeonggi Province. People who agreed to take Walking treatment were classified into experimental group and control group. Both experimental group and control group were treated with Korean medicine. In addition, experimental group performed Walking program more often. Changes of temperature difference taken by digital infrared thermal imaging(DITI) were used as measuring tools. The summary of this study's result is as in the following. There was significant difference in the experimental group which performed Walking treatments but not in the control group resulting from examining the change of temperature difference between left and right Yongchon. As known from the results above, Walking program is meaningful in curing the low back pain.

매스콘크리트 교각의 수화열에 의한 온도 및 응력 거동에 대한 3차원 유한요소 해석 (A 3-dimensional Finite Element analysis of the Temperature and Stress Development in Mass Concrete Pier due to Heat of Hydration)

  • 주영춘;김은겸;신치범
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1998년도 가을 학술발표대회 논문집(III)
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    • pp.928-933
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    • 1998
  • The temperature and stress behaviour of mass concrete pier at early ages was analysed based on the finite element method. The pier investigated is a three-dimensional structure of which the cross-sectional shape varies from a circle to an ellipsoid along the longitudinal axis. In order to obtain the transient temperature and stress distributions in the structure, a three dimensional method was adopted, because the structure of this type cannot be modeled accurately by a two-dimensional method. Temperature analysis was performed by taking into consideration of the cement type and content, boundary and environment conditions including the variations of atmospheric temperature and wind velocity. The results of this study may be useful for the temperature control to restrain thermal cracking and the construction management to design the resonable curing method of mass concrete structure.

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