• Title/Summary/Keyword: Teflon

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Elemental Analysis of Coal by Inductively Coupled Plasma Mass Spectrometry (誘導結合플라스마 質量分析法에 의한 石炭의 元素 分析)

  • 이용근;고인형;이동수
    • Journal of Korean Society for Atmospheric Environment
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    • v.8 no.3
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    • pp.155-161
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    • 1992
  • A simple, fast yet sensitive method is described for the determination of fifty elements in coal by inductively coupled plasma mass spectrometry. The method involves complete dissolution of coal with mixed acid $(HNO_3, HF, HClO_4)$ in hish pressure Teflon bomb and subsequent inductively coupled plasma mass spectrometric(ICP-MS) measurement. The accuracy of the method, being evaluated by the analysis of NIST SRMs (1632a, 1632b) is better than 20% RSD for most elements. The limits of detection defined by two times $\sigma$ (standard deviation of operational blank) are in order of sub-ppm to ppm, which are low enough to quantitate most elements. However, the determiantions for few elements such as V, As, Se are severely interfered by molecular ions such that their accurate determiantions are not possible. Analytical results for twentyon coals from eight countries including six ones world major coal producing, Korea, Japan, China, I.C.S., U.S.A., Canada, Australia, and South Africa are presented. While the results for major elements agree well with the existing ones, those for a few trace elements disagree considerably. The existing values are considerably higher. It is not possible to judge which are more accurate. However, the exisisting values are more likely to be errorous inasmuch as they are obtained without using high purity reagents and clean laboratory techniques.

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A Study on the Coatings for CP System in the Environment in which Thin Layer of Extremely Acidic Fluids are Formed

  • Chang, H.Y.;So, I.S.;Jin, T.F.;Kim, Y.S.;Yoo, Y.R.;Kang, M.S.
    • Corrosion Science and Technology
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    • v.5 no.1
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    • pp.5-14
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    • 2006
  • A lot of parts in FGD (Flue Gas Desulphurization) systems of fossil-fuel power plants show the environments in which are highly changeable and extremely acidic corrosive medium according to time and locations, e.g. in duct works, coolers and re-heaters etc.. These conditions are formed when system materials are immersed in fluid that flows on them or when exhausted gas is condensed into thin layered medium to contact materials of the system walls and roofs. The environments make troublesome corrosion and air pollution problems that are occurred from the leakage of the condensed solution. The frequent shut-down and repairing works of FGD systems also demand costs and low efficiencies of those facilities. In general, high corrosion resistant materials have been used to solve this problem. However, even the super alloys and Teflon linings sometimes have not been good enough to preventing corrosion. Further more, they are expensive and not easily repairable in short periods of operation stops. In this work, new technology that is effective, economical and easily repairable has proposed to solve the corrosion problems in FGD facilities. This technology contains cathodic protection, coatings and remote monitoring-controlling systems.

Freeze Drying Process and Pore Structure Characteristics of Porous Cu with Various Sublimable Vehicles (다양한 동결제를 이용하여 동결건조 공정으로 제조한 Cu 다공체의 기공구조 특성)

  • Lee, Gyuhwi;Oh, Sung-Tag;Suk, Myung-Jin;Jeong, Young-Keun
    • Journal of Powder Materials
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    • v.27 no.3
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    • pp.198-202
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    • 2020
  • The effect of sublimable vehicles on the pore structure of Cu fabricated by freeze drying is investigated. The 5 vol% CuO-dispersed slurries with camphene and various camphor-naphthalene compositions are frozen in a Teflon mold at -25℃, followed by sublimation at room temperature. After hydrogen reduction at 300℃ and sintering at 600 ℃, the green bodies of CuO are completely converted to Cu with various pore structures. The sintered samples prepared using CuO/camphene slurries show large pores that are aligned parallel to the sublimable vehicle growth direction. In addition, a dense microstructure is observed in the bottom section of the specimen where the solidification heat was released, owing to the difference in the solidification behavior of the camphene crystals. The porous Cu shows different pore structures, such as dendritic, rod-like, and plate shaped, depending on the composition of the camphornaphthalene system. The change in pore structure is explained by the crystal growth behavior of primary camphor and eutectic and primary naphthalene.

Fabrication of Transimpedance Amplifier Module and Post-Amplifier Module for 40 Gb/s Optical Communication Systems

  • Lee, Jong-Min;Min, Byoung-Gue;Kim, Seong-Il;Lee, Kyung-Ho;Kim, Hae-Cheon
    • ETRI Journal
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    • v.31 no.6
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    • pp.749-754
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    • 2009
  • The design and performance of an InGaAs/InP transimpedance amplifier and post amplifier for 40 Gb/s receiver applications are presented. We fabricated the 40 Gb/s transimpedance amplifier and post amplifier using InGaAs/InP heterojunction bipolar transistor (HBT) technology. The developed InGaAs/InP HBTs show a cut-off frequency ($f_T$) of 129 GHz and a maximum oscillation frequency ($f_{max}$) of 175 GHz. The developed transimpedance amplifier provides a bandwidth of 33.5 GHz and a gain of 40.1 $dB{\Omega}$. A 40 Gb/s data clean eye with 146 mV amplitude of the transimpedance amplifier module is achieved. The fabricated post amplifier demonstrates a very wide bandwidth of 36 GHz and a gain of 20.2 dB. The post-amplifier module was fabricated using a Teflon PCB substrate and shows a good eye opening and an output voltage swing above 520 mV.

Design of Plano-Convex Lens Antenna Fed by Microstrip Patch Considering Integration with Microwave Planar Circuits

  • Yu, Seung-Gab;Yeon, Dong-Min;Kim, Yong-Hoon
    • Journal of electromagnetic engineering and science
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    • v.1 no.1
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    • pp.67-72
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    • 2001
  • In this paper, the plano-convex lens antenna fed by a single patch is studied for a microwave remote-traffic monitoring sensor with constraints of small size and low cost. Measurement of an AUT (Antenna Under Test) involves the considerations of a triangular groove for matched layer and metallic shielding effects. A formulation for extracting the parameters of a piano-convex lens antenna, based on geometrical optics, is introduced using Fermat`s principle of the equi-phased ray condition. Teflon ($\varepsilon_{{\gamma}}$/ =2.0) is chosen as a material of a plano-convex lens antenna for adjustment of aberrations on the lens surfaces automatically. A fabricated plano-convex lens shows 3-dB beamwidth of 7.5 degree and side-lobe level of -29 dB with an aperture distribution of the parabolic-squared taper on pedestal. This lens supports easier integration with the planar microwave circuits by using a microstrip single patch as a primary feeder of the lens antenna.feeder of the lens antenna.

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An Approach to Estimate Dielectric Constant of Low-Loss Materials Using Dielectric Slab Loaded Cylindrical Cavity Resonators (유전체 슬랩이 삽입된 원통형 공진기를 이용한 저손실 물질의 유전 상수 측정)

  • Lee, Won-Hui
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.19 no.10
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    • pp.1115-1121
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    • 2008
  • In this paper, dielectric slab loaded cylindrical cavity resonator measurement technique is presented to determine the dielectric constant of a dielectric material. The dielectric constant is measured by the resonant frequency deviation of empty and dielectric slab loaded cavity. Characteristic equations are derived by th exact field analysis. The measurement configurations are formed using HP8719A vector network analyzer and an experimental cylindrical metallic cavity with circular cross-section. The validity of the theory is confirmed by experiments and CST MWS 4.0(3D simulator). The results were in the whole satisfactory. The measured dielectric constant of teflon and bakelite are 2.03 and 4.44, respectively.

A Photoelastic Study on the Stress Intensity Factor of Circular Disk with an Are-crack (광탄성법에 의한 원고형상크랙을 갖는 원판의 응력확대계수에 관한 연구)

  • Lee, Chi-Woo;Kim, Tae-Gyu;Yang, Jang-Hong;O, Se-Uk
    • Journal of Ocean Engineering and Technology
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    • v.2 no.2
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    • pp.96-103
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    • 1988
  • The stress distribution in the vicinity of the crack tip in the fracture mechanics is ordenarily indicated by the stress intensity factor. In the analysis of stress intensity factors, there are many theoretical and experimental methods. The stress analysis in photoelastic technique is usually made by using the difference of the principal stress of isochromatic fringe patterns. In this paper, the teflon molding technique is adopted to make a test specimen with a circular arc-crack, and that upgraded the accuracy of experiment. As the result, the experimental values of the stress intensity factors for the circular disk with a straight crack are coincided with the theoretical values. But, there is quite a difference between this expermental results on the finite plate for circular arc-crack and its theoretical values on the infinite one. Therefore, a boundary condition with regard to the loading condition on finite disk must be considered.

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A Free-Space Method for Measurement and Analysis of Dielectric Characteristics of Electromagnetic Absorbing Materials at Microwave Frequencies (자유공간 기법을 적응한 마이크로파 대역 전파흡수재의 유전 특성 분석)

  • 배근식
    • Journal of the Korea Institute of Military Science and Technology
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    • v.6 no.2
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    • pp.73-82
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    • 2003
  • For measurements and analysis of dielectric characteristics of planar slabs of microwave absorbing materials, I have applied a free-space method in the frequency range of 8~14 GHz. The measurement system for free-space method consists of transmit and receive antennas, mode transitions, precision coaxal cables, the network analyzer, and a computer Special Spot-focused horn lens antenna was used to eliminate diffraction effects. Diffraction effects at the edges of the sample are minimized by satisfying the condition for minimum transverse dimension of the plate and the beamwidth of the antennas at the focus. The time-domain gating feature of the network analyzer and the thru, reflect, and line(TRL) calibration technique were used to eliminate the effects of undesirable multiple reflections. The complex coefficients of reflection and transmission, $S_{11}$ and $S_{21}$, of planar samples were measured for standard materials such as Teflon, Rexolite$\textregistered$ 2200. The results were compared with existing measurement method. And I applied a free-space method for measurement to measure dielectric constants of some electromagnetic absorbing materials. Dielectric properties for the same samples were also measured with a 7mm coxial transmission line method for purposes of comparison with the free-space method.

Electrical characteristics of insulating materials for HTS bushing immersed in $LN_2$

  • Choi, J.H.;Kim, W.J.;Shin, H.S.;Kim, S.H.
    • Progress in Superconductivity and Cryogenics
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    • v.13 no.4
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    • pp.10-13
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    • 2011
  • For the operation of high temperature superconducting (HTS) power equipments, it is necessary to develop insulating materials and high voltage (HV) insulation technology at cryogenic temperature of bushing. In this paper, the surface flashover characteristics of various insulating materials in $LN_2$ are studied. These results are studied at both AC and impulse voltage under a non-uniform field. The negative impulse breakdown voltage of GFRP is slightly higher than the positive impulse breakdown voltage. The use of glass fiber reinforced plastic (GFRP) and polytetrafluoroethylene (PTFE, Teflon) as insulation body for HTS bushing should be much desirable. Especially, GFRP is excellent material not only surface flashover characteristics but also mechanical characteristics at cryogenic temperature. The surface flashover is most serious problem for the shed design in $LN_2$ and operation of superconducting equipment.

An Experimental Study on Regime Limit and Pressure Drop of Dry-plug Flow in Round Mini-channels (원형 미소 채널 내 드라이 플러그류의 유동 영역 한계와 압력 강하에 관한 실험적 연구)

  • Lee, Chi-Young;Lee, Sang-Yong
    • Proceedings of the KSME Conference
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    • 2008.11b
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    • pp.2583-2588
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    • 2008
  • In the present experimental study, the regime limit and pressure drop of dry-plug flow (dry wall condition at the gas portions of plug flow) in round mini-channels has been investigated. The air-water mixture was flowed through the round mini-channels made of Teflon, where the tube diameters ranged from 1.26 to 2.06 mm. For the present experimental range, with decreasing of the tube diameter, the transition between the plug and slug flows (wet and dry) happened at the higher gas superficial velocity region, which were in good agreement with the previous flow pattern maps tested. On the other hand, the transition between the wet- and dry-plug flows was little affected by the change of the tube diameter. In the pressure drop of dry-plug flows, among the correlations tested, the Lee and Lee's (2008) correlation best fitted the measured pressure drop data within the mean deviation of 10% for the present experimental range.

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