• Applied Microscopy
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• v.25 no.1
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• pp.130-138
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• 1995

TEM specimen preparation methods have been examined to characterize Cu oxide particles in the polyimide film. Polyimide films were prepared by coating polyamic acid onto Cu films which had been deposited on TEM-mask and glass substrates and Cu foil, followed by thermal curing. In case of TEM-mask, direct observation was possible without further preparation. In other cases, TEM specimen were made by separating polyimide film from the substrate. Polyimide films were removed from glass and Cu foil by dissolving glass in HF solution and Cu foil in $H_{2}SO_{4}$ solution. TEM-mask observation confirms that fine $Cu_{2}O$ particles precipitate in the polyimide as a result of reaction of polyamic acid with Cu. However $Cu_{2}O$ particle reacts with HF and $H_{2}SO_{4}$ solution during dissolving the substrate and interpretation could be misled. It is concluded characterization of $Cu_{2}O$ particle in polyimide using TEM-mask is better than other methods.

• Korean Journal of Poultry Science
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• v.16 no.2
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• pp.61-71
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• 1989

The purposes of this study were to investigate the genetic variations by backcrossing in commercial chickens. Backcrossing was carried out successively back to parent stock (P.S). Heritabilities and genetic correlation coefficients were estimated to verify the genetic variations. The data obtained from a breeding programme with commercial chickens (I strain) were collected from 1955 to 1987 at Poultry Breeding Farm, Seoul National University. Data came from a total of 1230 female offspring. The results obtained are summarized as follows： 1. The general performance ($Mean\pmStandard deviation$) of each trait was $663.94\pm87.11$g for 8 weeks body weight, $1579.1\pm155.43$g for 20 weeks body weight, $2124.1\pm215.3$g for 40 weeks body weight, $2269.1\pm242.94$g for 60 weeks body weight, $168.43\pm12.94$ day for a9e at sexual maturity (SM), $214.52\pm29.82$ eggs , for total egg number to 60 weeks of age (TEN), $61.45\pm3.48$ g for average weight (AEW), $13180.7\pm1823.22$ g for total egg mass to 60 weeks of age(TEM). All traits, except 10 weeks body weight and AEW, were significant for the degrees of backcross (p＜0.01). 2. The pooled estimates of heritabilities derived from the sire, dam and combined variance components were 0.47~0.52 for age at sexual maturity (SM), 0.07~0.37 for total egg number (TEN), 0.40~0.54 for average egg weight (AEW), 0.18~0.27 for total egg mass (TEM). High heritability estimates were found for SM and AEW. TEN and TEM were estimated to be a lowly heritable traits. Heritability estimates from dam components were higher than those from sire components. These differences might be due to non-additive genetic effect and maternal effect. 3. The estimates of heritabilities and standard errors derived from combined variance components for different degrees of backcross were $0.47\pm0.11$ (BCO), $0.42\pm0.16$ (BC1), $0.51\pm0.29$ (BC2) for TEN, $0.59\pm0.20$ (BCO), $0.43\pm0.17$ (BC1), $0.35\pm0.18$ (BC2) for AEW, $0.28\pm0.12$(BC0), $0.20\pm0.11$(BC1), $0.18\pm0.14$ (BC2) for TEM. Heritability estimates for AEW and TEM were decreased by backcrossing while those for SM and TEN remained constant. Since backcrossing contributes to increased homozygosity, the genetic variation of the traits (AEW and TEM) decreased . 4. The pooled estimates of genetic correlation coefficients were -0.55 between SM and TEN, 0.20 between SM and AEW, -0.29 between TEN and AEW, 0.82 between TEM and TEN, 0.31 between TEM and AEW, -0.42 between TEM and SM. The genetic correlation between TEM and TEN was higher than that between TEM and AEW, and it was suggested that egg mass was strongly affected by egg number. Also, age at sexual maturity(SM) contributes to egg mass(TEM). 5. When backcrossing was carried out successively, the genetic correlation between TEM and TEN increased (BC0：0.79, BC1：0.82, BC2：0.91) but those between TEM and SM decreased (BC0：-0.54, BC1：-0.36, BC2：-0.09) with successive backcrosses.

• The Proceeding of the Korean Institute of Electromagnetic Engineering and Science
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• v.13 no.1
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• pp.51-62
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• 2002

EMI/EMS 측정을 위해서는 주변 전자파 잡음(background noise)이 낮은 야외시험장(Open Area Test Site)이 가장 바람직하나, 근래 전자(전기 기기 사용의 증가와 방송.무선통신 시스템의 다양화로 인한 인공잡음(artificial noise)의 증대로 조건에 부합된 부지 선정이 어렵고, 설치 비용이 매우 크며 날씨 변화에 따라 시험 계획이 변경 될 수도 있는 단점이 있다. 전자파 분-무반사실(Semi Anechoic Chamber)은 대부분의 환경 잡음을 감쇠시키므로 야외시험장처럼 장소의 구애를 받지 않아 도시나 혹은 제품 생산지 가까이에 설치 운용이 가능하다. 그러나 큰 설치 공간과 많은 시설 유지 비용을 필요로 하며, 저주파 대역에서는 반사에 의한 공진을 완전히 제거할 수 없어 성능이 떨어진다. 또한, 최근 컴퓨터 CPU의 동작주파수가 급속하게 높아지고 PCS, IMT-2000 등과 같은 이동전화의 사용주파수도 계속해서 높아짐에 다라 미연방통신위원회(Federal Communication Commission)에서는 5㎓까지의 복사 방출 시험을 요구하고 있다. IEC 61000-4-3 복사 내성 시험규격도 휴대폰 주파수인 2㎓까지 확장되었으며 IMT-2000, Bluetooth 등 새로운 이동통신서비스가 속속 개발됨에 따라 18㎓ 까지 시험 주파수가 확장되는 추세이다. 그러나, 현재 국내 각 연구실에서 보유하고 있는 야외시험장이나 전자파 반-무반사실의 경우 1㎓이상에서의 시험이 곤란하여 수 ㎓주파수대역에서 시험이 가능한 복사 및 내성시험 시설이 필요하게 되었다. 이러한 문제점들을 해결하기 위해 고안된 대용 측정 시설 중 대표적인 것이 TEM 셀이나 GTEM셀과 같은 TEM 도파관(waveguide) 형태의 장비들이다. 이들은 본래 EMS 측정을 위한 장비이지만 협소한 공간이나 외부와의 전자파 간섭의 우려가 없고, 설치가 비교적 자유로워 여러 연구기관에서 도파관 원리를 이용한 측정 방식을 연구(개발하여 범용적인 전자파 적합성 측정 장비로서 활용하고 있다. 야외시험장과 무반사실 등이 안테나에 의한 피시험기기 주변 공간에서의 1점 측정으로 인해 시험 시간이 많아 소요되는 공통적인 단점이 있는 반면, TEM 도파관에 의한 측정은 일단 피시험기기의 모델링 정보만 얻어지면 계산에 의해 EMI 측정을 바로 할 수 있다. <표 1>에서 현재 상용화되어 사용되고 있는 TEM/GTEM 셀, 야외 시험장 및 전자파 무반사실에 대해 EMI 측정과 관련된 몇 가지 사안에 대해 비교하였다. 본 문서에서는 야외시험장이나 전자파 반-무반사실 등과 같은 기존 EMI/EMS 측정 시설의 단점을 보완하고, 광대역 특성을 갖는 대용 측정 시설로서의 TEM 도파관에 대해 소개하고 야외시험장 결과와의 상관관계 알고리즘 및 표준화 동향에 대해 기술하였다. 2절에서는 대표적인 TEM 도파관 구조의 측정 시설인 TEM 셀과 GTEM 셀의 전기적.구조적 특징에 대해 간단히 기술하고, 3절에서는 TEM 셀과 GTEM 셀에서이 측정결과를 이용하여 야외 시험장 결과를 얻어내는 상관관계 알고리즘에 대해 기술하였다. 4절에서는 IEC/CISPR와 TC77에서의 표준화 활동을 중심으로 현재 진행중인 TEM 도파관 관련 표준화 동향과 내용에 대해 기술하고자 한다.

• Proceedings of the Materials Research Society of Korea Conference
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• 2007.05a
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• pp.14.1-14.1
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• 2007

• Bulletin of the Korean Chemical Society
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• v.34 no.3
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• pp.788-792
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• 2013

A shortcoming of using transmission electron microscopy (TEM) for structural analysis via electron diffraction is the relatively large error of the measurements as compared to X-ray diffraction. To reduce these errors, various internal standard methods from earlier studies have been widely used. We developed a new device to facilitate the application of internal standard methods in preparation of TEM grids used for nanopowder analysis. Through the application of a partial mask on the TEM grid, both the internal standards and the research materials can be loaded on the same grid. Through this process, we conducted a TEM analysis that compared synthetic hydroxyapatite (HAp) nanopowder to bone apatite from a bovine femur. We determined that the accuracy of the d-spacing measurements of the HAp and bone powders could be improved to better than 1% after statistical treatments of the experimental data. By applying a quarter mask, we loaded four different nanoparticles on a single TEM grid, with one section designated for the internal standard.

• Journal of The Institute of Information and Telecommunication Facilities Engineering
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• v.2 no.1
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• pp.45-51
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• 2003

본 논문에서는 TEM Cell 의 최적 설계방법을 제안한다. 임피던스 부정합을 최소화 시키기 위해 Cell 내부의 특성 임피던스를 $50{\Omega}$으로 유지하며, 동시에 중심 도체판(septum)의 길이와 도체판 날개(winglet)의 각을 변화 시킴으로써 내부 전자파의 균일도(Uniformity)를 최대로 하는 TEM Cell의 최적설계방법을 제안하며 (1+1)ES를 적용하여 시험영역을 최대로 하는 최적 설계 변수들을 제시한다.

• The Journal of Korean Institute of Communications and Information Sciences
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• v.25 no.1B
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• pp.48-55
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• 2000

The design techniques of an asymmetric TEM (ATEM) cell for calibrating E/H filed probes are presented in this paper. The authors describe the techniques to obtain not only the arbitrary frequency and second resonant frequency, but also the test space with $\pm$2dB filed uniformity. We could design an ATEM cell that the measured data, electric filed distribution inside the cell, impedance matching and resonant frequencies, agree with the calculated results.

• Korean Journal of Materials Research
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• v.10 no.7
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• pp.478-481
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• 2000

Single phase $Pb(Mg_{1/3}Nb_{2/3})O_3$ ceramics doped by 10 mol% of electron donors such as $La^3,\; Pr^{3+,4+},\; Nd^{3+},\; Sm^{3+}$, were synthesized and their B-site cationic ordering structures were investigated by XRD and TEM. In the XRD patterns, only fundamental reflections were observed for the undoped $Pb(Mg_{1/3}Nb_{2/3})O_3$, while the (h/2 $\textsc{k}$/2ι/2)(h,$\textsc{k}$,ι all odd) superlattice reflections resulting from the 1:1 ordering induced unit cell doubling were also observed for the donor-doped $Pb(Mg_{1/3}Nb_{2/3})O_3$. In the TEM selected area diffraction patterns, the (h/2 k/2 l/2)(h,k,l all odd) superlattice reflection spots as well as the fundamental reflection spots were observed for all the samples, but the relative intensities of the superlattice reflection spots to the fundamental reflection spots were significantly enhanced by the donor-doping. In the TEM dark-field images, antiphase boundaries were observed only for the donor-doped $Pb(Mg_{1/3}Nb_{2/3})O_3$. It was therefore experimentally verified that doping by electron donors such as $La^3,\; Pr^{3+,4+},\; Nd^{3+},\; Sm^{3+}$, enhances the B-site cationic 1:1 ordering in $Pb(Mg_{1/3}Nb_{2/3})O_3$. These experimental results were interpreted in terms of the charge compensation mechanism.

• YAKHAK HOEJI
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• v.39 no.3
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• pp.276-282
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• 1995

Compared to the first and second-generation cephalosporins, the third-generation cephalosporins are remarkably stable against hydrolysis by the $\beta$-lactamases produced by aerobic gram-negative bacilli, such as Enterobacteriaceae. Among these bacteria, the most prevalent plasmid-encoded $\beta$-lactamase is TEM-1 $\beta$-lactamase belonging to class A or group 2b. This enzyme is produced constitutively and is principally active against peniciflins and old cephalosporins rather than third-generafion cephalosporins, carbapenems and mmobactams. However, new TEM type $\beta$-lactamases including TEM-9 and TEM-12 evolved through point mutations in a gene encoding $\beta$-lactamase have been discovered from patients during chemotherapy. These $\beta$-lactamases are known to be capable of hydrolyzing most of the third-generatim cephalosporins. To study the prevalence of $\beta$-lactamases from clinical isolates collected in Korea. the minimal inhibitory concentratims(MICs) of several third-generation cephalosporins against 628 clinical isolates were determined by agar dilution methods, and $\beta$-lactamas-producing bacteria were isolated by use of cefinase disc. By polymerase chain reaction (PCR) method, clinical isolates harboring a gene for TEM type $\beta$-lactamase were identified among the $\beta$-lactamase producing strains. Twentiy three percent of the clinical isolates was resistant to the thirdgeneration cephalosporins, and more than 90% of resistant cells produced various $\beta$-lactamases. TFM type $\beta$-lactamases were dominant in gram-negative bacilli, such as Escherichia coli, Klebsiella pneumoniae, Enterobacter species. These results suggest the necessity of the development of new cephalosporins which are stable against $\beta$-lactamases like TEM.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.11 no.11
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• pp.975-983
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• 1998

A duplexer filter operating at 1.9 GHz band for personal communication system is designed and fabricated using $lambada$/4 TEM mode dielectric resonator. The transmitting band pass filter is designed in the type of the elliptic function band rejection filter by 3 dielectric resonators with 5 additional capacitors and 3 inductors. The receiving band pass filter is designed by 3 dielectric resonators with 5 additional capacitors which give additional series resonance. The parameters which are evaluated by design theory are practically applied to the duplexer filter construction and the simulation.