• Title/Summary/Keyword: TEM Journal

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Dielectric Band-Pass Filter with Attenuation Poles at Desired Frequencies

  • Lee, Moon-Que
    • KIEE International Transactions on Electrophysics and Applications
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    • v.4C no.6
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    • pp.268-271
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    • 2004
  • An analytic design formula is proposed for a TEM mode dielectric bandpass filter with attenuation poles at desired frequencies in the stop band. In order to sustain the constant ripple in the passband due to attenuation poles, the initial resonant frequencies of the various resonators adopted in a filter with attenuation poles are newly calculated. The proposed design theory is verified by designing various bandpass filters with attenuation poles in the stop band.

Principles and Analysis of Electron Diffraction Patterns in Transmission Electron Microscopy : Utilization of Microcomputers (전자회절도형의 원리와 분석 : Microcomputer의 이용)

  • Sung, Chang-Mo
    • Applied Microscopy
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    • v.21 no.1
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    • pp.108-120
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    • 1991
  • Principles of electron diffraction patterns in transmission electron microscope are described for beginners in terms of reciprocal lattices and Ewald sphere. Analysis of both ring patterns and spot patterns are illustrated with practical examples as well as basic calibrations of TEM. Especially convergent beam electron diffraction method is emphasized for the determination of lattice parameters, microstrains, and thickness of thin foil followed by a review of microcomputer programs for the electron diffraction analyses explained in this paper.

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Synthesis of Trimetallic Au@Pb@Pt Core-shell Nanoparticles and their Electrocatalytic Activity toward Formic Acid and Methanol

  • Patra, Srikanta;Yang, Hae-Sik
    • Bulletin of the Korean Chemical Society
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    • v.30 no.7
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    • pp.1485-1488
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    • 2009
  • A facile, seed-mediated preparation method of trimetallic Au@Pb@Pt core-shell nanoparticles is developed. Au nanoparticles are the template seeds onto which sequentially reduced Pb and Pt are deposited. The trimetallic core-shell structure is confirmed by UV-Vis spectroscopy, TEM and EDS analysis, and cyclic voltammetry. The trimetallic Au@Pb@Pt core-shell nanoparticles show high electrocatalytic activity for formic acid and methanol electrooxidation.

Hydrothermal Synthesis of Mesostructured Vanadium Oxide and Application of UV-Ozone Treatment

  • Chang, Ju-Yeon;Jung, Duk-Young
    • Bulletin of the Korean Chemical Society
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    • v.24 no.5
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    • pp.613-616
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    • 2003
  • Effect on hydrothermal treatment of lamellar vanadium oxides was investigated and the formation of hexagonal and cubic mesophase was found. This lamellar materials were prepared by mixing of cetyltrimethylammonium-bromide and pH-controlled sodium metavanadate solution. Thermal method and UV/O₃treatment were applied to extract organic template. The structure of resulting product was studied by powder X-ray diffraction and transmission electron microscopy (TEM).

In-situ HRTEM Studies of Alumina-Aluminum Solid-Liquid Interfaces

  • Oh, Sang-Ho;Scheu, Christina;Ruhle, Manfred
    • Applied Microscopy
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    • v.36 no.spc1
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    • pp.19-24
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    • 2006
  • The alumina-aluminum solid-liquid interfaces were directly observed at atomic scale by heating the alumina single crystal in high-voltage electron microscope (HVEM) owing to the electron beam damage processes, Atomic ordering in the first several layers of the liquid was clearly resolved adjacent to the alumina surface and its relevance to the single crystal growth was examined with the real-time observations.

Domain Wall Motions in Ferromagnetic Thin Film Induced by Laser Heating Pulse

  • Park, Hyun Soon
    • Applied Microscopy
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    • v.48 no.4
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    • pp.128-129
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    • 2018
  • Soft ferromagnetic materials are utilized for various electromagnetic devices such as magnetic recording heads and magnetic shielding. In situ observation of magnetic microstructures and domain wall motions are prerequisite for understanding and improving their magnetic properties. In this work, by the Fresnel (out-of-focus) method of Lorentz microscopy, we observe the domain wall motions of polycrystalline Ni/Ti thin film layers triggered by single-shot laser pulse. Random motions of domain walls were visualized at every single pulse.

Application of Biosynthesized Silver Nanoparticles Against a Cancer Promoter Cyanobacterium, Microcystis aeruginosa

  • El-Sheekh, Mostafa Mohamed;El-Kassas, Hala Yassin
    • Asian Pacific Journal of Cancer Prevention
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    • v.15 no.16
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    • pp.6773-6779
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    • 2014
  • Background: Nanotechnology opens new applications in many fields including medicine. Among all metallic nanoparticles, silver nanoparticles (silver NPS) have proved to be the most effective against a large variety of organisms including toxic cyanobacteria. Materials and Methods: Silver NPs were biosynthesized in vivo with different alga species namely, Spirulina piatensis, Chlorella vulgaris and Scenedesmus oh/iquus following two scenarios. First: by suspending a thoroughly washed algae biomass in 1 mM aqueous $AgN0_3$ solution. Second: by culturing them individually in culture media containing the same concentration of $AgN0_3$. Silver NPs were characterized using UV-Vis spectroscopy, transmission electron microscopy (TEM), energy dispersive analysis (EDX) and Fourier transform infra-red (FfIR) spectroscopy. The biosynthesized silver NPs were tested for cytotoxic activity against a cancer promoter cyanobacteruim Microcystis aeruginosa, considering effects on cell viability and chlorophyll content. Results: The surface plasmon band indicated the biosynthesis of silver NPs at ~400 nm. Transmission electron microscopy (TEM) revealed that the silver NPs had a mean average size below 100 nm. Energy-dispersive analysis X-ray (EDX) spectra confirmed the presence of silver element. FfIR spectral analyses suggested that proteins and or polysaccharides may be responsible for the biosynthesis of silver NPs and (-COO-) of carboxylate ions is responsible for stabilizing them. The toxic potentialities ofthe biosynthesized silver NPs against the cancer promoter cyanobacterium, Microcystis aeruginosa showed high reduction in viable cells count and the total chlorophyll content. Conclusions: The potential activity of the biosynthesized silver NPs from the studied algae species against Microcystis aernginosa cells is expected to be mainly mediated by the release of silver ions (Ag+) from the particle surface and bioactive compounds as indicated by FfIR analysis.

Study for Facilitated Olefin Transport Phenomena Using Silver Oxide (Silver Oxide를 이용한 올레핀 촉진수송 현상 연구)

  • Ji, Dahye;Kang, Sang Wook
    • Membrane Journal
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    • v.25 no.1
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    • pp.1-6
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    • 2015
  • It was known that the polarlized surface of silver nanoparticles could be interacted revesibly with olefin molecules for facilitated olefin transport. However, it was thought that it can be regenerated by interaction between oxide surface of AgNPs and olefin molecules because the surface of the silver nanoparticles is easily oxidized in the air. In order to investigate the effect of the silver oxide, 5 wt% AgO or $Ag_2O$ was dispersed in polymer PVP solutions and 0.005~0.02% electron acceptor as TCNQ or p-BQ were added to fabricate the separation membrane. After the addition of the electron acceptor, it was expected to improve the polarity on the surface of the silver oxide and the degree of dispersion. The characteristics of the separation membrane were identified by the gas permeance, XPS and TEM.

Preparation of Lysine-Coated Magnetic Fe2O3 Nanoparticles and Influence on Viability of A549 Lung Cancer Cells

  • Ma, Yu-Hua;Peng, Hai-Ying;Yang, Rui-Xia;Ni, Fang
    • Asian Pacific Journal of Cancer Prevention
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    • v.15 no.20
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    • pp.8981-8985
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    • 2014
  • Objective: To explore the effect of lysine-coated oxide magnetic nanoparticles (Lys@MNPs) on viability and apoptosis of A549 lung cancer cells. Methods: Transmission electron microscopy (TEM), vibrating sample magnetometer (VSM) and Zeta potentiometric analyzer were employed to characterize Lys@MNPs. Then Lys@MNPs and lung cancer A549 cells were co-cultured to study the effect of Lys@MNPs on cell viability and apoptosis. The pathway of Lys@MNPs entering A549 cells was detected by TEM and cell imaging by 1.5 T MRI. Results: Lys@MNPs were 10.2 nm in grain diameter, characterized by small size, positive charge, and superparamagnetism. Under low-dose concentration of Lys@MNPs (< $40{\mu}g/mL$), the survival rate of A549 cells was decreased but remained higher than 95% while under high-dose concentration ($100{\mu}g/mL$), the survival ratewas still higher than 80%, which suggested Lys@MNPs had limited influence on the viability of A549 cells, with good biocompatibility and and no induction of apoptosis. Moreover, high affinity for cytomembranes, was demonstrated presenting good imaging effects. Conclusion: Lys@MNPs can be regarded as a good MRI negative contrast agents, with promising prospects in biomedicine.