• Korean Journal of Materials Research
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• v.5 no.2
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• pp.184-190
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• 1995

IN 617 was crept under stresses of 107 and 180 MPa with monotonic deformation to strains of $\varepsilon$= 0.03 - 0.30 at 1073K. In order to determine the distances between the subgrain boundaries, the deformed specimens were examined at magnifications of one hundred thousand times by TEM. In cases . where TEM observations were not possible, subgrain angles($\theta$_{s}=sin^{-1}$(b/s))were measured by Kikuchi diffraction lines. The $\theta$_{k}$ converted from s values measured directly by TEM agreed very well with those measured from Kikuchi lines. Therefore, it was found that the $\theta$_{k}$ values could be used in obtaining s, especially in cases where it is impossible to measure s by TEM.

• Korean Journal of Microbiology
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• v.36 no.3
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• pp.221-227
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• 2000

This study was performed to investigate the biological characteristics of twenty isolates of extended spectnlm $\beta$-lactamase (ESBL) producing Klebsiellapnezm~onia collected kom the various clinical specimens of three hospitals in Pusan. Isoelectric focusing (IEF) and PCR were used to determine the types of $\beta$-lactamase gene in this study. Twenty isolates of ESBL producing Klebsiellnp~ieun~or~iae could be divided by PCR, such as TEM type (I1 strains), SHV type (8 strains); non TEM non SHV type (1 strain). In the isoelechic focusing test, the PI of TEM type was 5.2-6.0 and that of SHV type was 6.9-7.4. According to the pI value and PCR bands, twenty strains of ESBL Klebsiellapneumoniae were divided into 5 types: TEM type @I 5.2-6.0; 1080 bp on PCR band), TEM + SHV type (pI 5.2-6.0; andpI 7.0-7.4; 1080 bp and 599 bp on PCR band), SHV type (pl7.0-7.4; 599 bp on PCR band), non TEM non SHV type, and otber type (PCR result was SHV type but pI was not detected).

• Korean Journal of Materials Research
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• v.13 no.9
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• pp.598-605
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• 2003

The optimized conditions for the cross-sectional TEM sample preparation using tripod polisher and ion-beam miller was confirmed by AFM and TEM. For the TEM observation of interfaces including InGaN layers like InGaN/GaN MQW structures, the sample preparation by the only tripod polishing was useful due to the reduction of artifacts. On the other hand, in case of the thick nitride films like ELO, PE, and superlattice, both tripod polishing and controlled ion-beam milling were required to improve the reproducibility. As a result, the ion-beam milling with the $60^{\circ}$modulation showed the minimum height difference between film and sapphire interface and the ion-beam milling of the $80^{\circ}$modulation showed the broad observable width.

• Korean Journal of Materials Research
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• v.3 no.2
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• pp.193-196
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• 1993

A procedure for preparing cross-sectional specimens for transmission electron microscopy(TEM)by focused ion beam(FIB)milling of specific regions of semiconductor devices is outlined. This technique enables TEM specimens to be pripared at precisely preselected area. In-situ #W thin film deposition on the top surface of desired site is complementally used to secure the TEM specimens to be less wedge shaped, which is main shortcoming of previous FIB-assisted TEM sample preparation technique. This technique is quite useful for the TEM sample priparation for fault finding and the characterization of fabrication process associated with submicron contact technologies.

• Applied Microscopy
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• v.32 no.4
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• pp.311-317
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• 2002

There is great requirement on the TEM specimen preparation method with particle size selectivity as a prerequisite for the quantitative structure analysis on the materials such as gibbsite powder, which generally forms a large agglomerate and shows a variation of transition process depending on their sizes. In this experiment, we made an attempt to give a methodology for the TEM specimen preparation of powder with the size selectivity. After mixing 1 wt% gibbsite powder with ethanol solvent, gibbsite suspension was prepared by application of ball-milling and ultrasonification with addition of 0.25 vol% dispersion agent, Darvan C, which was diluted into distilled water by the ratio 1:19. Appling the static sedimentation method to gibbsite suspension after estimation of the sedimentation time by the measurement of accumulative concentration variation, we acquired TEM specimens with well-dispersed and size selected gibbsite particles in nm scale. Overall picture of each sample was taken by SEM and morphology of each dispersed particle was imaged by TEM. Raw and processed gibbsite powders were also examined by XRD to investigate whether they were suffered from phase change during the process or not.

• Applied Microscopy
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• v.34 no.2
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• pp.95-102
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• 2004

The TEM samples prepared by ion milling have the advantage that thin area can be obtained from almost any materials. However, it has the disadvantage that the amount of thin area can often be quite limited. For the cross-sectioned samples and grossly heterogeneous materials, the thickness of less than $0.1{\mu}m$ can be achieved by mechanical grinding and polishing (tripod polisher) and then the TEM samples may be ion-milled for final thinning or cleaning. These approaches were described in this paper. Examples of TEM observations were taken from cross-section samples of thin films on silicon and sapphire, from diffusion layers between $Mo_5Si_3\;and\;Mo_2B$, and from rapidly solidified 304 stainless steel powders embedded in electroplated copper.

• The Journal of Engineering Geology
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• v.21 no.3
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• pp.213-219
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• 2011

Transient/time-domain electromagnetic (TEM) soundings were carried out on reclaimed land, since the TEM sounding has good resolution of a conductive and thin overburden. The reclamation material is marine clay dredged from the seafloor, which is currently undergoing consolidation in the upper part of the dredged layer. The conductivity of the marine-origin clay is generally more than 0.3 S/m. The aim of the TEM sounding was to determine the depths of weathered and soft rocks overlain by thick and conductive overburden. The TEM responses were measured at delay times of 0.050-20.575 ms with a $30{\times}30$ m coincident loop array. Data from the TEM inversion and core logging indicate that the resistivities of the conductive overburden are less than 2 ${\Omega}$-m, while those of the weathered and soft rocks are 10-20 and 70 ${\Omega}$-m, respectively. The depth to weathered rock is 26-58 m and the depth to soft rock is 46-75 m.

• Applied Microscopy
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• v.25 no.1
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• pp.130-138
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• 1995

TEM specimen preparation methods have been examined to characterize Cu oxide particles in the polyimide film. Polyimide films were prepared by coating polyamic acid onto Cu films which had been deposited on TEM-mask and glass substrates and Cu foil, followed by thermal curing. In case of TEM-mask, direct observation was possible without further preparation. In other cases, TEM specimen were made by separating polyimide film from the substrate. Polyimide films were removed from glass and Cu foil by dissolving glass in HF solution and Cu foil in $H_{2}SO_{4}$ solution. TEM-mask observation confirms that fine $Cu_{2}O$ particles precipitate in the polyimide as a result of reaction of polyamic acid with Cu. However $Cu_{2}O$ particle reacts with HF and $H_{2}SO_{4}$ solution during dissolving the substrate and interpretation could be misled. It is concluded characterization of $Cu_{2}O$ particle in polyimide using TEM-mask is better than other methods.

• ETRI Journal
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• v.11 no.3
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• pp.65-72
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• 1989

투과 전자 현미경 (Transmission Electron Microscope : TEM))의 단면 시료 관찰은 반도체 소자의 미세화에 따른 공정 평가, failure analysis 분야에 최근 많이 사용되고 있으나 TEM관찰을 위한 반도체 소자의 시료 제작 기술이 반도체 재료의 특성상 매우 어렵기 때문에 만족할만한 연구 성과가 미흡한 실정이다. 여기에서는 확산 공정 기술 개발에 따른 시료의 TEM 관찰에 필요한 단면 관찰용 시료 제작 기술에 대한 연구 결과를 정리 하였다.

• The Journal of Korean Institute of Communications and Information Sciences
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• v.15 no.11
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• pp.898-908
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• 1990

This paper applies the moment method to analyze the transverse electromagnetic(TEM) cell with an inner conductor (septum) of arbitrary rectangular shape and location by employing quast static approximation. The EM field and the characteristic impedance so obtained are shown to be in good agreement with the available data from the previously published papers about the typical TEM cell structure with center septum of zero thickness.