• 공업화학
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• 제33권4호
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• pp.402-407
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• 2022

실험계획법을 이용하여 MOF-5 합성공정의 최적화에 대한 연구를 수행하였다. 먼저 전구체의 농도를 최적화 하기 위하여 혼합물 설계법을 이용하였다. 합성에 사용되는 세 가지 전구체인 terephthalic acid, zinc acetate dihydrate, N,N-dimethylformamide의 농도비를 extreme vertices design methods로 최적화 하였다. MOF-5 합성을 위한 최적의 농도는 1 mol : 2.7 mol : 40 mol로 예측되었다. 이후, 온도, 시간 및 교반 속도와 같은 합성 반응 조건이 합성에 미치는 영향을 분석하기 위해 다단계 요인 설계법을 사용하였다. 수행된 통계 분석에 따라 교반 속도는 후속 연구에서 제외되었다. 합성시간과 온도를 고려한 합성 공정 최적화는 중앙 조성 설계법을 이용하였다. 13번의 합성 실험을 통해 도출된 2차 모델 방정식을 이용하여 결과를 추정하였다. 설계에 사용된 모델에 의하면 119 ℃ 및 10.4 h 조건에서 합성된 MOF-5가 최대의 결정화도를 가지는 것으로 예측되었다.

• Bulletin of the Korean Chemical Society
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• 제18권7호
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• pp.703-706
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• 1997

Response surface method was applied to the predicting optimum conditions of benzene synthesis for radiocarbon dating. The weight of carbon dioxide, the temperature of lithium container for producing acetylene and the activation temperature of catalyst which was used for the cyclization of acetylene to benzene were used as experimental factors. The yields of benzene synthesis were measured from twelve experiments which were carried out under various experimental conditions. The polynomial equation was obtained by using three experimental factors and yields. The validity of polynomial equation was confirmed by comparing the calculated yields with the experimental ones.

• 한국전자파학회논문지
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• 제25권5호
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• pp.592-600
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• 2014

본 논문에서는 2차 함수 곡선의 회전체 곡면 위에 있는 배열 안테나의 빔 합성을 위한 Enhanced Adaptive Genetic Algorithm(EAGA)을 제안하였다. 제안된 알고리즘은 더 빠른 수렴 속도와 더 낮은 비용함수 값을 얻기 위해 Adaptive Genetic Algorithm(AGA)과 Invasive Weed Optimization(IWO)을 결합시켰다. 각 안테나 소자의 급전 크기와 위상의 최적화된 값은 EAGA를 통해 구하였으며, 이 결과를 통해 EAGA가 컨포멀 배열 안테나의 패턴 합성 알고리즘으로써 AGA보다 더 우수함을 보였다.

• 대한조선학회논문집
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• 제31권2호
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• pp.91-98
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• 1994

대형구조계에 대하여 구조중량의 최소화를 기하면서 고유진동수 제한조건을 만족시키는 동특성 최적화에 효율적인 한 방법을 제안한다. 일련의 근사최적화문제를 형성하는데 있어서는 고유진동수의 설계파라메터에 대한 감도와 설계파라메터의 역에 대한 감도를 병용하는 근사방법을 사용하며, 설계변수의 변화에 따른 고유진동해석 및 감도계산은 저자가 조선학회논문집 제30권 제3호에 발표한 바 있는 부분구조진동형 합성방법에 의거한다. 설계파라메터에 대한 감도와 설계파라메터의 역에 대한 감도를 병용하는 근사방법은 전자만을 사용하는 근사방법에 비해 적은 회수의 재해석으로 고유진동수 제한조건을 만족하는 설계값을 얻을 수 있다. 또한 설계변경에 따른 재해석시 앞서 발표했던 부분구조진동형 합성방법의 장점을 활용하므로써 효율적인 재해석이 가능하다. 제안된 방법의 유용성은 외팔보유추 구조계 및 선체단순화 2-D FEM모델의 상부구조를 대상으로 한 수치예제를 통하여 검증되었다.

• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2014년도 추계학술대회 논문집
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• pp.464-466
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• 2014

The mechanism synthesis methods, graphical, analytical and computer-aided technique have been proposed for selecting and scaling mechanical system. According to developing computation tools, mechanism could be synthesized much faster and more correct than previous analytical ways by improved techniques. In this paper, the improved synthesis method is proposed to solve body guidance synthesis problem. To perform the mechanism synthesis for body guidance, a planar linkage is modeled as a set of free three bushings located in design space. The values of bushing stiffness and x, y position of bushings yielding a desired functional requirement related to input motion are found by using an optimization technique.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2005년도 춘계학술대회 논문집
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• pp.822-827
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• 2005

Recently engineering systems problems become quite large and complicated. For those problems, design requirements are fairly complex. It is not easy to design such systems by considering only one discipline. Therefore, we need a design methodology that can consider various disciplines. Multidisciplinary Design Optimization (MDO) is an emerging optimization method to include multiple disciplines. So far, about seven MDO methodologies have been proposed for MDO. They are Multidisciplinary Feasible (MDF), Individual Feasible (IDF), All-at-Once (AAO), Concurrent Subspace Optimization (CSSO), Collaborative Optimization (CO), Bi-Level Integrated System Synthesis (BLISS) and Multidisciplinary Optimization Based on Independent Subspaces (MDOIS). In this research, the performances of the methods are evaluated and compared. Practical engineering problems may not be appropriate for fairness. Therefore, mathematical problems are developed for the comparison. Conditions for fair comparison are defined and the mathematical problems are defined based on the conditions. All the methods are coded and the performances of the methods are compared qualitatively as well as quantitatively.

• Journal of Microbiology and Biotechnology
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• 제30권8호
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• pp.1252-1260
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• 2020

(R)-2-(4-hydroxyphenoxy)propionic acid (HPOPA) is a key intermediate for the preparation of aryloxyphenoxypropionic acid herbicides (R-isomer). In order to improve the HPOPA production from the substrate (R)-2-phenoxypropionic acid (POPA) with Beauveria bassiana CCN-A7, static cultivation and H₂O₂ addition were attempted and found to be conducive to the task at hand. This is the first report on HPOPA production under static cultivation and reactive oxygen species (ROS) induction. On this premise, the cultivation conditions and fermentation medium compositions were optimized. As a result, the optimal carbon source, organic nitrogen source, and inorganic nitrogen source were determined to be glucose, peptone, and ammonium sulfate, respectively. The optimal inoculum size and fermentation temperature were 13.3% and 28℃, respectively. The significant factors including glucose, peptone, and H₂O₂, identified based on Plackett-Burman design, were further optimized through Central Composite Design (CCD). The optimal concentrations were as follows: glucose 38.81 g/l, peptone 7.28 g/l, and H₂O₂ 1.08 g/l/100 ml. Under the optimized conditions, HPOPA titer was improved from 9.60 g/l to 19.53 g/l, representing an increase of 2.03-fold. The results obtained in this work will provide novel strategies for improving the biosynthesis of hydroxy aromatics.

• 공업화학
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• 제28권3호
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• pp.286-289
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• 2017

통계적 실험계획법을 이용하여 나노입자 합성 공정의 최적화 방법론을 제시하기 위하여 대상 물질로 제올라이트 4A의 합성을 수행하였다. 실리콘 전구체인 sodium metasilicate (SMS)의 농도를 조절하여 합성한 제올라이트 4A를 XRD, SEM 및 질소흡착법으로 특성분석 하였다. 특히 XRD 분석으로 결정한 결정도로 제올라이트 4A의 합성결과를 판단할 수 있었다. 실험계획법 중 일반요인분석을 이용하여 반응장치, 반응온도 및 반응시간에 따른 주효과도 및 교호작용을 분석하였다. 또한 반응표면분석법을 통하여 결정도 최대치를 가지는 제올라이트 4A를 합성할 수 있는 최적의 조건으로 계산하였다. 구체적으로는 autoclave를 사용하고 반응시간 3 h 및 반응온도 $110^{\circ}C$의 반응조건이 제시되었다. 더욱이 실리콘 전구체로 Ludox를 사용하는 조건하에서, 다양한 결정화도를 가지는 제올라이트 4A에 대한 최적의 합성조건을 모든 범위에서 대하여 표면도와 등고선도를 이용하여 제시하였다.

• 한국경영과학회:학술대회논문집
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• 한국경영과학회/대한산업공학회 2003년도 춘계공동학술대회
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• pp.529-536
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• 2003

The majority of previous studios on tolerance synthesis have viewed the issue as a design methodology to determine optimal component tolerances on behalf of a manufacturer. while meeting given assembly tolerance requirements Although a considerable amount of research has been done on this issue. a couple of important questions still remain unanswered First. how ran a design engineer quantitatively incorporate a customer's perception on a product quality into a tolerance synthesis scheme at the early design stage Second. how ran component tolerances and assembly tolerance be optimized in a simultaneous way? To answer these questions. this article presents the customer-driven concurrent tolerance synthesis which is facilitated by the notion of truncated distribution and the use of mathematical programming techniques. while adopting the major principles of Tagurhl philosophy. The work presented in the article is an effort to gain insight, which can be useful in practice when setting up guidelines for an overall tolerance synthesis.

• 한국소음진동공학회:학술대회논문집
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• 한국소음진동공학회 2001년도 춘계학술대회논문집
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• pp.535-539
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• 2001

In these days. the finite element method(FEM) is a very common method for not only a simple vibration analysis but also the optimization of structures. Since the finite element model may contain thousands of degree of freedom, the eigensolutions require extreme computing power, which will result in a serious time-consuming problem. Thus, many researchers have challenged to find more improved modeling techniques and calculating methods to overcome such problems. The Guyan reduction method and the substructure synthesis method are typical examples of such methods. Of the substructure synthesis method, the component mode synthesis method (CMS) is widely used for dynamic analysis of structure. In this study. for the efficient analysis of jet loom structure. Component Mode Synthesis was carried out. The results of the finite element program developed are compared with those of the commercial package program ANSYS for the validation of the program. The results obtained by the program showed a good agreement with those of ANSYS. The program will be further refined and verified by test to yield more accurate results.