• Title/Summary/Keyword: Synthesis in water

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The Synthesis of Ester Compound by Lipase in Organic Solvents (유기용매계에서 리파제에 의한 에스테르 화합물 합성)

  • Kim, Boo-Chul;Lee, Jae-Dong;Lee, Tae-Ho
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.23 no.3
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    • pp.496-501
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    • 1994
  • The synthesis of lauryl palmitate from palmitic acid and lauryl alcohol was investigated in organic solvents using lipase. Water-immiscible organic solvent such as hexane, toluenem cyclohexane, and isooctane were found to be suitable of ester synthesis . The effect of water content on the initial rate of conversion was examined . As the content increased, the reaction rate increased. But addition of water in organic solvent decreased therostability of enzyme . The best lauryl palmitate synthesis was achieved with water content of 0.2-0.4% reaction temperature of 4$0^{\circ}C$ and 45$^{\circ}C$ for Candida cylindracea lipase porcine, pancreatic lipase, respectively. when ester synthesis was carried out under the optimum conditions, the conversion yield of palmitate into lauryl palmitate after 70hrs reached 85% and 69 % for the Candida cylindracea lipase and porcine opancreatic lipase, respectivley.

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Influence of Refeeding with Vitamin, Mineral and Fibre on Protein Synthesis and Messenger Ribonucleic Acid Content in the Liver and Muscle of Fasted Chicks

  • Aman Yaman, M.;Kita, K.;Pinontoan, R.;Okumura, J.
    • Asian-Australasian Journal of Animal Sciences
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    • v.11 no.5
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    • pp.545-549
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    • 1998
  • The influence of refeeding with either vitamin, mineral, fibre of water on protein synthesis and mRNA content in the liver and breast muscle of fasted chicks was investigated. At 15 d of age, chicks were fasted for 2 d and then refed either vitamin, mineral, fibre or water. The fractional synthesis rate (FSR) of protein was measured after 30 min of refeeding by using a large dose injection of L - 2, $6[^3H]$ phenylalanine. In the liver, FSR was reduced by fasting and tended to increase but not significantly by refeeding with vitamin or mineral. FSR was not affected by refeeding with fibre or water. There was no influence of fasting and refeeding on ribosomal capacity (the RNA : protein ratio) and ribosomal efficiency (total protein synthesised per total RNA). The absolute synthesis rate (ASR) of liver protein and hepatic mRNA content were reduced by fasting and unchanged by refeeding. In the muscle, FSR, ASR and mRNA content were significantly decreased by fasting and not recovered by refeeding with either vitamin, mineral, fibre or water. It concluded that vitamin, mineral, fibre and water have little capacity to stimulate liver and muscle protein synthesis reduced by fasting.

The Synthesis of Polyamine Polymeric Flocculant and Application of Drinking Water Treatment. (Polyamine 고분자 응집제의 합성과 상수처리의 적용)

  • 신명철;최상준
    • Journal of Environmental Science International
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    • v.7 no.3
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    • pp.409-413
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    • 1998
  • Polyamine was synthesized for the drinking water treatment. Polyamine was produced by the two step polycondensation of dimethytamine(DMA) and epichlorohydrin(EPI) and its properties were characterized. The effects of mole ratio of (DMA1/1EPl), reaction temperature and reaction time on synthesis of polyamine were investigated. Polyamine flocculant was applied to Nak-dong river raw water to examine its efficiency in reducing turbidity. The synthesized polyamine was effective as flocculant for drinking water treatment. The addition of 1 mg/L of polyamlne flocculant caused the reduction of 50% PAC (polyaluminium chloride).

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Antioxidant Effects and Anti-inflammation Effects of Lophatheri Herba Water Extracts Via Reducing iNOS Synthesis Induced by LPS in RAW 264.7 Cell (담죽엽의 항산화 효과와 RAW 264.7 세포에서 LPS로 유도된 iNOS 발현에 미치는 영향)

  • Hwang, Sung-Yeoun;Lee, Sung-Won;Kwon, Kang-Beom;Choi, Won-Jong;Kim, Jae-Hyo;Ahn, Seong-Hun
    • Journal of Physiology & Pathology in Korean Medicine
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    • v.24 no.6
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    • pp.976-982
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    • 2010
  • We studied to know the anti-inflammation effect on water extracts of Lophatheri Herba which was growing in every places in our country. We objected free radical scanvenger effect and nitrite eliminate effect of the Lophatheri Herba water extracts, and the cell viabillity, the effects of Lophatheri Herba water extracts on NO production, iNOS synthesis induced by LPS. Free radical scavenger effects were $27.91{\pm}0.12%$, $38.96{\pm}0.10%$, $46.22{\pm}0.15%$ depend on 0.5, 1.0, 2.0 mg/ml each dose of Lophatheri Herba water extracts. Nitrite eliminate effects were $9.86{\pm}0.3%$, $80.61{\pm}0.23%$, $97.62{\pm}0.56%$ in 0.1, 1.0, 2.0 mg/ml Lophatheri Herba water extracts on pH 1.2. NO production and iNOS synthesis induced by LPS were reduced in RAW 264.7 cell by Lophatheri Herba water extracts. As the above results, Lophatheri Herba water extracts have anti-inflammation effects via NO production decrease, iNOS synthesis decrease mechanism. So Lophatheri Herba water extracts will be used as the protection or treatment in chronic inflammation desease like a asthma, stomatitis etc.

The Effect of pH on Synthesis of Nano-Silica Using Water Glass (물유리를 이용한 나노실리카 제조 시 pH가 미치는 영향)

  • Choi, Jin Seok;An, Sung Jin
    • Korean Journal of Materials Research
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    • v.25 no.4
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    • pp.209-213
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    • 2015
  • Synthesis of nano-silica using water glass in a Sol-Gel process is one of several methods to manufacture nano-silica. In nano-silica synthesized from water glass, there are various metal impurities. However, synthesis of nano-silica using water glass in a Sol-Gel process is an interesting method because it is relatively simple and cheap. In this study, nano-silica was synthesized from water glass; we investigated the effect of pH on the synthesis of nano-silica. The morphology of the nanosilica with pH 2 was flat, but the surface of the nano-silica with pH 10 had holes similar to small craters. As a result of ICP-OES analysis, the amount of Na in the nano-silica with pH 2 was found to be 170 mg/kg. On the other hand, the amount of Na in the nano-silica with pH 10 was found to be 56,930 mg/kg. After calcination, the crystal structure of the nano-silica with pH 2 was amorphous. The crystal structure of the nano-silica with pH 10 transformed from amorphous to tridymite. This is because elemental Na in the nano-silica had the effect of decreasing the phase transformation temperature.

Development and Flight Test of Educational Water Rocket CULV-1 for Implementation of Launch Vehicle Separation Sequence and Imaging Data Acquisition (발사체 분리과정모사 및 단계별 영상획득이 가능한 교육용 물로켓 CULV-1 개발 및 비행시험)

  • Lee, Myeongjae;Park, Taeyong;Kang, Soojin;Jang, Sueun;Oh, Hyunung
    • Journal of Aerospace System Engineering
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    • v.10 no.2
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    • pp.14-21
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    • 2016
  • In this study, we proposed a water rocket CULV-1 (Chosun University Launch Vehicle-1). Unlike a conventional water rocket, CULV-1 can perform the booster rocket, fairing, and payload separation like an actual launch vehicle and also the imaging data acquisition. The conceptual and critical design of the proposed CULV-1 have been performed considering the operation characteristics. The verification tests have been performed from subsystem to system level in accordance with the established test specifications and verification procedures. Through the final launch test of the flight model, we have verified the design effectiveness of the proposed separation mechanisms for water rocket applications and the mission requirements of the CULV-1 also have been complied.

A Study on the Rational Planning of Water Supply and Sewage System for Rural Village Development Projects (농촌마을종합개발사업에서 상하수도시설의 합리적 계획방향에 관한 기초적 연구)

  • Kim, Hwan-Yong
    • Journal of the Korean Institute of Rural Architecture
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    • v.8 no.2
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    • pp.62-71
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    • 2006
  • This study on the rational planning of water supply and sewage system for rural village development projects. Present, when establishment and standard about maintenance of water supply and sewage system were not presented in rural village synthesis development projects, it is real condition that service industry is depending on presenting simple plan in basis planning phase and business enforcement step. This study wishes to present basic data so that can be planned more rationally and enforce and contribute in rural village synthesis development projects water supply and sewage system that is enforced as part of rural village synthesis development projects.

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A New Approach to Synthesis and Photoluminescence of Silicon Nanoparticles

  • Kim, Beomsuk
    • Journal of Integrative Natural Science
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    • v.2 no.1
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    • pp.28-31
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    • 2009
  • We describe the synthesis and characterization of silicon nanoparticles prepared by the soluton reduction of SiCl4. These reactions produce Si nanoparticles with surfaces that are covalently terminated. The resultant organic derivatized Si nanoparticles as well as a probable distribution of Water-soluble Si nanoparticles are observed and characterized by photoluminescence(PL) spectroscopy. This work focuses originally on the organic- and water-soluble silicon nanoparticles in terms of the photoluminescence. Further this work displays probably the first layout of hydrogen terminated Si nanoparticles synthesized in solution at room temperature.

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Flowing Water Editing and Synthesis Based on a Dynamic Texture Model

  • Zhang, Qian;Lee, Ki-Jung;WhangBo, Taeg-Keun
    • Journal of Korea Multimedia Society
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    • v.11 no.6
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    • pp.729-736
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    • 2008
  • Using video synthesis to depict flowing water is useful in virtual reality, computer games, digital movies and scientific computing. This paper presents a novel algorithm for synthesizing dynamic water scenes through a sample video based on a dynamic texture model. In the paper, we treat the video sample as a 2-D texture image. In order to obtain textons, we analyze the video sample automatically based on dynamic texture model. Then, we utilize a linear dynamic system (LDS) to describe the characteristics of each texton. Using these textons, we synthesize a new video for dynamic flowing water which is prolonged and non-fuzzy in vision. Compared with other classical methods, our method was tested to demonstrate the effectiveness and efficiency with several video samples.

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The μ-synthesis and analysis of water level control in steam generators

  • Salehi, Ahmad;Kazemi, Mohammad Hosein;Safarzadeh, Omid
    • Nuclear Engineering and Technology
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    • v.51 no.1
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    • pp.163-169
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    • 2019
  • The robust controller synthesis and analysis of the water level process in the U-tube system generator (UTSG) is addressed in this paper. The parameter uncertainties of the steam generator (SG) are modeled as multiplicative perturbations which are normalized by designing suitable weighting functions. The relative errors of the nominal SG model with respect to the other operating power level models are employed to specify the weighting functions for normalizing the plant uncertainties. Then, a robust controller is designed based on ${\mu}$-synthesis and D-K iteration, and its stability robustness is verified over the whole range of power operations. A gain-scheduled controller with $H_{\infty}$-synthesis is also designed to compare its robustness with the proposed controller. The stability analysis is accomplished and compared with the previous QFT design. The ${\mu}$-analysis of the system shows that the proposed controller has a favorable stability robustness for the whole range of operating power conditions. The proposed controller response is simulated against the power level deviation in start-up and shutdown stages and compared with the other concerning controllers.