• 제목/요약/키워드: Swelling ratio

검색결과 432건 처리시간 0.026초

알칼리수용액안에서 셀룰로오스섬유가 팽윤할 때 장력이 미치는 영향 (Effect of Stretching on Cellulose Fiber Swelling in Alkali Aqueous Solutions)

  • 최철호
    • 한국염색가공학회지
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    • 제4권3호
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    • pp.91-96
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    • 1992
  • The crystalline character of NaOH and KOH-cellulose complex having different tension ratio was studied using X-ray diffraction analysis. Cellulose crystalline lattices in tension alkali treatment cotton were identified by measuring and indexing the 101, 101, and 002 reflections. According as alkali treatment tension ratio increased on, cellulose gave rise to the formation of I rather than cellulose II. It seemed that a part of the fine structure of cellulose increased orientation with antiparaell and parallel chain crystal structure. The high tension ratio alkali treatment cotton resulted in lower dye sorption and in higher breaking strength and crease recovery.

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비지분말 첨가에 의한 설기떡의 품질특성 (Quality Characteristics of Sulgidduk with added Soybean Curd Residue Powder)

  • 임성미;이군자
    • 한국식품조리과학회지
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    • 제22권5호통권95호
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    • pp.583-590
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    • 2006
  • This study was carried out to investigate the acceptable ratio of Sulgidduk with added soybean curd residue powder. The moisture content of Sulgidduk with added soybean curd residue powder (0${\sim}$ 10%) ranged from 40.54 ${\sim}$41.38%, and there were no significant differences between the addition of soybean curd residue powder and control. There were also no significant differences in swelling power and pore ratio from control to the addition of 4% soybean curd residue powder. However, these decreased with increasing addition of soybean curd residue powder of more than 6%. The L (lightness) value decreased with increasing addition of soybean curd residue powder, but the a (redness) and b (yellowness) values increased significantly. As the amount of soybean curd residue powder increased, the hardness, cohesiveness, springiness and gumminess decreased, and, the decrease was especially significant with addition of more than 6%. With increases in the storage period, the hardness, springiness and gumminess increased, while cohesiveness decreased for all additions of soybean curd residue powder. In sensory evaluations, Sulgidduk with the addition of 4% soybean curd residue powder was the most preferred with regard to overall quality. These results indicated that the Sulgidduk with 2% and 4% added soybean curd residue powder exhibited the best quality.

Evaluation of Physical Properties as Magnesium Stearate Blendedin Hydrophilic Matrix Tablets

  • Choi, Du-Hyung;Jung, Youn-Jung;Wang, Hun-Sik;Yoon, Jeong-Hyun;Jeong, Seong-Hoon
    • Journal of Pharmaceutical Investigation
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    • 제41권2호
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    • pp.83-90
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    • 2011
  • Main objectives of this study were to investigate the effects of a lubricant, magnesium stearate, as blended in a hydrophilic matrix tablet and to identify significant factors using a tablet ejection force and a swelling property. The characteristics of tablet ejection were evaluated with three different compression forces (30, 40, and 60 MPa) and two controlled factors, amount of magnesium stearate and its mixing time. A hydrophilic model drug (terazosin HCl dihydrate) was regarded as a default factor. Tablet swelling was also evaluated. The optimal amount of PEG compared to PEO was set to be 88.50% w/w. As the amount of magnesium stearate was varied from 0.79% to 2.20% w/w, the amount of PEO and PEG was adjusted to meet the tablet's total weight while maintaining the ratio between the two excipients constant. As the mixing time of magnesium stearate was increased, the tablet ejection force and the swelling property were decreased. As the amount of magnesium stearate was increased, the tablet ejection force and the swelling property were decreased since the increased mixing time and the amount of magnesium stearate induced hydrophobic properties of the matrix tablet more effectively. The ejection force of the tablet increased as a result of increase in the compression force, which means that the breaking of tablet/die-wall adhesion energy was also increased when the compression energy was increased. The results gavea valuable guide how to choose suitable amount of the lubricant with processing conditions for the development of hydrophilic matrix formulations.

왕겨숯을 이용하여 제조한 보드의 물성 (Physical and Mechanical Properties of Board Made from Carbonized Rice Husk)

  • 황정우;오승원
    • Journal of the Korean Wood Science and Technology
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    • 제45권1호
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    • pp.62-71
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    • 2017
  • 본 연구는 쌀의 도정과정에서 발생되는 농업부산물인 왕겨를 탄화시켜 만든 왕겨숯을 톱밥과 혼합하여 밀도별, 수지첨가율별 및 톱밥첨가율별로 보드를 제조하고 기초물성을 측정하여 보드 재료로서의 이용가능성을 검토하였다. 수분흡수율은 수지첨가량 25%일 때 80.09%로 가장 낮은 값을 나타냈고, 밀도가 증가하고 톱밥첨가량이 감소할 때 수분흡수율이 감소하는 경향을 나타냈다. 또한 측정된 두께팽윤율은 KSF 3104 파티클보드의 품질규정에 만족시키고 있어 치수안정성 부분에서 건축내장재로 활용가능성이 확인되었다. 박리강도는 수지첨가량 25%일 때 $0.244N/mm^2$으로 KSF 3104 파티클보드의 품질기준을 만족시켰지만, 나머지 조건에서는 현저하게 낮은 값을 나타내 조건을 충족시키지 못하였다. 밀도, 수지첨가율, 톱밥첨가율이 증가할수록 경도도 증가하는 경향을 나타냈다.

폐기물매립장에서 다짐에너지와 팽윤도에 의한 토양-벤토나이트 혼합토의 투수계수 특성에 관한 연구 (A Study on Characteristics of Hydraulic Conductivity in the Soil-Bentonite Mixed Soils with Compaction Energy and Swelling in the Landfill)

  • 이종민;이재영
    • 한국지하수토양환경학회지:지하수토양환경
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    • 제6권4호
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    • pp.61-72
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    • 2001
  • 폐기물 매립장에는 발생되는 침출수의 유출을 방지하기 위하여 매립장의 바닥 또는 측면에 투수계수가 1x$10^{7}$cm/sec이하인 차수재를 설치한다. 본 연구는 폐기물 매립장 차수재인 토양-벤토나이트 차수재 (혼합토)를 대상으로 하여 현장토의 토성에 따른 벤토나이트의 배합비와 투수계수의 특성을 파악하고 벤토나이트의 팽윤도 및 다짐방법이 차수층의 투수특성에 미치는 영향을 파악하였다. 연구결과 동일조건에서 최대건조밀도는 SC계열의 혼합토가 CL계열의 혼합토보다 높게 나타났고, 최적함수비는 그 반대의 경향을 나타냈으며, 다짐방법별로는 최대건조밀도의 경우 D다짐시가 높게 나타났고, 최적함수비는 A다짐시의 경우가 높게 나타났다. 다짐에너지에 따른 최대건조밀도의 차이는 SC계열의 혼합토가 더 큰 것으로 나타났고, 최적함수비의 경우는 CL계열의 혼합토가 더 큰 차이를 보이는 것으로 나타났으며 팽윤도에 따른 최대건조밀도 및 최적함수비의 차이는 미미하였다. 벤토나이트의 배합비 및 팽윤도가 증가함에 따라 투수계수는 낮은 값을 나타내었고 동일조건에서는 CL계열의 혼합토와 D다짐시 낮은 투수계수를 나타내었다. 그러나 투수계수는 팽윤도보다는 벤토나이트의 배합량에 의해 더 많은 영향을 받는 것으로 나타났고 동일조건에서 SC계열의 혼합토와 A다짐시 더 큰 차이를 나타내었다. 투수시험결과에 따른 시공시 경제성을 검토한 결과 팽윤도가 낮은 벤토나이트를 배합한 경우가 더 경제적인 것으로 나타났는데 이는 팽윤도별 재료단가의 큰 차이에 비해 투수계수 감소효과가 기대에 미치지 못하기 때문인 것으로 판단된다.

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조직 확장기용 생분해성 하이드로젤의 제조 및 특성분석 (Preparation and Characterization of Biodegradable Hydrogels for Tissue Expander Application)

  • 육군영;김예태;임수진;;;박기남;박정숙;허강무
    • 폴리머
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    • 제34권3호
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    • pp.253-260
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    • 2010
  • 본 연구에서는 조직확장 응용을 위한 생체적합성 생분해성 하이드로젤을 제조하고, 그 기본특성을 분석하였다. 친수성 고분자인 poly(ethylene glycol)의 양 말단에 다양한 몰비의 D,L-lactide와 glycolide를 개환 중합시켜 PLGA-PEG-PLGA 삼중공중합체를 합성한 뒤 비닐기를 도입하여 하이드로젤 제조 시 swelling/degradation controllers(SDC)로 사용하였다. 합성한 SDC와 PEG diacrylate를 사용하여 라디칼 중합으로 제조한 하이드로젤은 건조된 상태에서도 유연하고 탄성을 보였으며 분해테스트에서는 SDC의 조성과 SDC/PEG의 몰비에 따라 다양한 팽윤지연시간과 분해기간을 갖는 것으로 나타났다. 그 밖에 기계적 물성과 팽윤압력을 측정하였고, 이식시험을 통해 이식용 하이드로젤을 사용목적에 맞게 이식하거나 삽입하였을 때의 생체 조직의 국소적인 병리적 양상을 육안관찰과 현미경적 관찰을 통하여 평가하였다.

Oral tissue response to soft tissue expanders prior to bone augmentation: in vitro analysis and histological study in dogs

  • Yoo, Jung Min;Amara, Heithem Ben;Kim, Min Kyoung;Song, Ju Dong;Koo, Ki-Tae
    • Journal of Periodontal and Implant Science
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    • 제48권3호
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    • pp.152-163
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    • 2018
  • Purpose: To determine whether the swelling and mechanical properties of osmotic self-inflating expanders allow or not the induction of intraoral soft tissue expansion in dogs. Methods: Three different volumes (0.15, 0.25, and 0.42 mL; referred to respectively as the S, M, and L groups) of soft tissue expanders (STEs) consisting of a hydrogel core coated with a silicone-perforated membrane were investigated in vitro to assess their swelling behavior (volume swelling ratio) and mechanical properties (tensile strength, tensile strain). For in vivo investigations, the STEs were subperiosteally inserted for 4 weeks in dogs (n=5). Soft tissue expansion was clinically monitored. Histological analyses included the examination of alveolar bone underneath the expanders and thickness measurements of the surrounding fibrous capsule. Results: The volume swelling ratio of all STEs did not exceed 5.2. In tensile mode, the highest mean strain was registered for the L group ($98.03{\pm}0.3g/cm$), whereas the lowest mean value was obtained in the S group ($81.3{\pm}0.1g/cm$), which was a statistically significant difference (P<0.05). In addition, the S and L groups were significantly different in terms of tensile strength ($1.5{\pm}0.1g/cm$ for the S group and $2.2{\pm}0.1g/cm$ for the L group, P<0.05). Clinical monitoring showed successful dilatation of the soft tissues without signs of inflammation up to 28 days. The STEs remained volumetrically stable, with a mean diameter in vivo of 6.98 mm, close to the in vitro post-expansion findings (6.69 mm). Significant histological effects included highly vascularized collagen-rich fibrous encapsulation of the STEs, with a mean thickness of $0.67{\pm}0.12mm$. The bone reaction consisted of resorption underneath the STEs, while apposition was observed at their edges. Conclusions: The swelling and mechanical properties of the STEs enabled clinically successful soft tissue expansion. A tissue reaction consisting of fibrous capsule formation and bone loss were the main histological events.

실험적 관절염 흰쥐 모델에서 고삼추출액이 척수와 척수신경절의 CGRP 면역반응 신경원에 미치는 영향 (The Effects of Sophorae radix Extracts on CGRP Immunoreactive Neurons of Spinal Cord and Ganglia in Experimental Arthritic Rat Model)

  • 신현종;이광규;육상원;이상룡;고병문;이창현
    • 동의생리병리학회지
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    • 제16권1호
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    • pp.117-123
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    • 2002
  • To investigate the antiinflammatory and analgesic effects of Sophorae radix extracts administered to the arthritic rat model, immunohistochemical stains for CGRP in the L4, L5 and L6 spinal cord and ganglia were done, and paw swelling thickness were measured. Complete Freund,s Adjuvant(CFA) were injected to subcutaneous tissue of left foot paw of rats to induce arthritis. Sophorae radix extracts was administered immediately after CFA injection for 10 days. The spinal cord and ganglia were frozen sectioned(30㎛). These sections were stained by CGRP immunohistochemical staining method, and observed with light microscope. The results were as follows : 1. The change of paw swelling thickness of experimental group decreased from 4 day to 10day after CFA injection compared to control group. 2. The change of differential leukocytes counts of experimental group increased the ratio of lymphocytes. and decreased the ratio of neutrophils compared to control group. 3. The change of CGRP immunoreactive nerve fiber of dorsal horn of experimental group was dense stained compared to control group. 4. The number of CGRP immunoreactive neurons of L4 and L5 spinal cord of experimental group was less than in those control group. These results suggested that Sophorae radix extracts reduces the number of CGRP immunoreactive neurons and nerve fibers of spinal cord and ganglia, and decrease paw swelling thickness in arthritic rat model, which may be closely related to analgesic and antiinflammatory effects of Sophorae radix.

실리카 나노입자의 표면처리와 이를 포함한 열가소성 폴리우레탄 복합소재의 특성 (Surface Treatment of Silica Nanoparticles and the Characteristics of their Composites with Thermoplastic Polyurethane Elastomer)

  • 유선화;송현제;김창근
    • 폴리머
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    • 제36권6호
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    • pp.721-726
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    • 2012
  • 해수에서 사용되는 음향 소나 시스템의 호스 소재로 열가소성 폴리우레탄 탄성체가 사용되고 있다. 장기간 소나 운용을 위해서는 향상된 기계적 물성과 해수 및 오일에 의한 낮은 팽윤도를 갖는 소재가 요구된다. 해수 적용에 적합한 향상된 물성의 복합재료를 개발하기 위해 실리카 나노입자 표면에 폴리우레탄을 그래프트시킨 TPU-g-silica 나노입자를 제조하고 이를 폴리우레탄과 혼련하여 복합재료를 제조하였다. 실리카 나노입자를 포함한 폴리우레탄 복합재료는 실리카 입자의 표면 처리에 상관없이 폴리우레탄보다 향상된 인장강도와 낮은 팽윤도를 나타내었다. 폴리우레탄 복합재료들이 같은 함량의 실리카 입자를 포함한 경우, TPU-g-silica를 포함한 복합재료가 표면처리를 하지 않은 실리카 입자를 포함한 복합재료에 비해 보다 향상된 인장강도와 낮은 팽윤도를 나타내었다. 장시간 오일에 함침 후 인장강도를 측정한 결과 폴리우레탄에 비해 TPU-g-silica를 포함한 복합재료가 높은 인장강도를 유지하였다.

히드록시프로필셀룰로오스와 카르보폴을 이용한 부유성 히드로겔 매트릭스의 제조 및 in Vitro 평가 (Preparation and in vitro Evaluation of a Buoyant Hydrogel Matrix with Hydroxypropylcellulose and Carbopol)

  • 김상헌;이민성;최영욱
    • Journal of Pharmaceutical Investigation
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    • 제26권2호
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    • pp.137-144
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    • 1996
  • The study was carried out for the preparation and evaluation of a buoyant hydrogel matrix (BHM), which is buoyant in a neutral or in pH 2.0 buffer solution, by the aspects of buoyancy, swelling, and drug release. Physical mixtures of HPC and CP in various molar ratio were employed as a mucoadhesive polymer which swells and controls the rate of drug release. Anhydrous citric acid and sodium bicarbonate in the molar ratio of 1:3 were employed as effervescing agents which provide a buoyancy for the mucoadhesive polymeric matrix. The buoyancy in vitro was expressed as both floating time$(T_{fl})$ and surfing time$(T_{sf})$, which are the time required for floating from the bottom to the surface of the medium and the time to keep the floated state at the surface of medium during release studies, respectively. A close relationship was observed between the buoyancy and the amount of effervescing agent added. $T_{fl}$ of the buoyant hydrogel matrices were decreased to about 10 seconds linearly with increasing the amount of effervescing agent in the range of 5 to 15%. $T_{sf}$ of the buoyant hydrogel matrices were varied from 1 to 3 hr depending on the amount of effervescing agent. The swelling was observed by changes in diameter of the buoyant hydrogel matrices in distilled water or acidic buffer solution, resulted in dependences on pH and the amount of effervescing agents. The release of hydrochlorothiazide from the buoyant hydrogel matrices were followed by apparent zero-order kinetics, while the buoyant hydrogel matrices were floated at the surface and maintaining their swollen shapes.

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