• 제목/요약/키워드: Surface range

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Simultaneous Determination and Occurrences of Pharmaceuticals by Solid-Phase Extraction and Liquid Chromatography-Tandem Mass Spectrometry (LC-MS/MS) in Environmental Aqueous Samples

  • Koo, So-Hyun;Jo, Cheon-Ho;Shin, Sun-Kyoung;Myung, Seung-Woon
    • Bulletin of the Korean Chemical Society
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    • 제31권5호
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    • pp.1192-1198
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    • 2010
  • Pharmaceuticals and personal care products (PPCPs) are emerging contaminants in the aquatic environment. Many pharmaceuticals are not completely removed during wastewater treatment, leading to their presence in wastewater treatment effluents, rivers, lakes, and ground water. Here, we developed analytical methods for monitoring ten pharmaceuticals from surface water by LC/ESI-MS/MS. For sample clean-up and extraction, MCX (mixed cation exchange) and HLB (hydrophilic-lipophilic balance) solid-phase extraction (SPE) cartridges were used. The limits of detection (LOD) in distilled water and the blank surface water were in the range of 0.006 - 0.65 and 1.66 - 45.05 pg/mL, respectively. The limits of quantitation (LOQ) for the distilled water and the blank surface water were in the range of 0.02 - 2.17 and 5.52 - 150.15 pg/mL, respectively. The absolute recoveries for fortified water samples were between 62.1% and 125.4%. Intra-day precision and accuracy for the blank surface water were 2.9% - 24.1% (R.S.D.) and -16.3% - 16.3% (bias), respectively. In surface wastewater near rivers, chlortetracycline and acetylsalicylic acid were detected frequently in the range of 0.017 - 5.404 and 0.029 - 0.269 ng/mL, respectively. Surface water near rivers had higher levels than surface water of domestic treatment plants.

다회가공 평면연삭작업에서 표면조도의 실험적 예측 (Experimental Surface Roughness Estimation in Multi-Pass Horizontal Grinding Operations)

  • 최후곤;김재윤;여명구
    • 한국정밀공학회지
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    • 제17권2호
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    • pp.64-72
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    • 2000
  • Surface roughness is one of the most important characteristics in machining processes. This study presents probabilistic models to estimate surface roughness experimentally in multi-pass horizontal surface grinding operations from three independent distributions such as the initial surface roughness distributions of workpiece, the distributions of the wheel radius, and the distributions of distances between major active grains. To specify the model characteristics from surface roughness measurements, either the probability satisfying a given surface roughness or the range of surface roughness satisfying a given probability have been estimated while grinding conditions are fixed. Finally, the relationship between grinding conditions satisfying surface roughness range under a given probability can be established.

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제주도 서남방 동중국해에서 하계 입자성부유물 및 표층퇴적물의 C, N 분포 특성 (The Characteristics of suspended particulate matter and surface sediment of C, N in the Northern East China Sea ill summer)

  • 강문규;최영찬
    • 한국해양환경ㆍ에너지학회지
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    • 제6권4호
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    • pp.13-23
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    • 2003
  • Organic carbon and nitrogen contents in suspended particulate matter (SPM) and surface sediments in seawater were measured in the Northern East China Sea in summer. The distribution of particulate organic carbon(POC) and particulate organic nitrogen(PON) were in the ranges of 54~481㎍/ℓ and 6~85㎍/ℓ, respectively, with relatively high level of concentrations in the western and southern sides of the study area. Also, there has been a significantly positive correlation between POC and PON, gradually increasing toward the deeper range of depth. Average C:N ratios of POC and PON of SPM were 6 in study area. The ratios of POC to PON of SPM increased as the range of depth increased, indicating nitrogen decomposes more rapidly than carbon and is considered to be influenced by the input of detritus from surface sediments. The distribution of total organic matter(TOM), total organic carbon(TOC) and total organic nitrogen(TON) in surface sediments were in the ranges of 3.1~9.6%, 0.282~0.635% and 0.022~0.069%, respectively, with relatively low range in the western and northern sides of the study area. The ratio of TOC to TON of surface sediments were in the range of 9.8~17.4(average of 13), strongly indicating the active role of the input from the terrestrial organic pollutants.

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EPS 엔드밀 가공 시 표면 거칠기에 미치는 가공조건에 관한 연구 (A study on machining conditions on surface roughness in EPS End-milling)

  • 서금희;손민규;윤길상;고영배
    • Design & Manufacturing
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    • 제11권2호
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    • pp.46-50
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    • 2017
  • EPS used in lost foam casting elastic modulus is extremely low. So it is necessary to derive machining conditions for effective cutting. Therefore this study were analyzed end-milling machining conditions to affecting the surface roughness of EPS foam. The machining conditions were set to depth, feed, and RPM at 3-level. And 18experimental conditions were derived using mixed orthogonal array. The most important condition for surface roughness is RPM. In addition, RPM machining condition range test that can realize surface roughness less than $10{\mu}m$ was performed. he range of RPM conditions is more than 15,000. However the range of RPM conditions is a condition that is difficult to use in actual field. In the future variance analysis and experiments are needed to derive the range of machining conditions available.

암반 경계표면의 진동속도 (Vibration Velocity of Rock Mass Boundary Surface)

  • 김일중;김영석
    • 화약ㆍ발파
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    • 제15권4호
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    • pp.11-17
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    • 1997
  • Impulsive vibration velocity is monitored at the surface and the boundary surface of rocks as various impulsive forces of horizontal and vertical directions were given to rocks which had difference in uniaxial compressive strength for investigate to the vibration velocity of rocks according to the impulsive direction and the monitoring site. The vibration velocity of the boundary surface of rocks was about 2.9 times or much larger than that of the surface at the same scaled distance in the case of horizontal impulsive forces, and was above 4.2 times in the case of vertical impulsive forces. The attenuation exponents of the vibration velocity equations in the surface and the boundary surface of rocks make a vast difference with the impulsive directions, but is makes little difference in the case of the same impulsive direction. The ratio of vibration constants of the surface to the boundary surface of rocks is that square and cube root scaled equation is a range of 2.7∼3.0 and 4.9∼5.0 respectively in the case of horizontal impulsive forces, and is a range of 4.2∼5.7 and 7.7∼11.5 respectively in the case of vertical impulsive forces.

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수소가 흡착된 W(011) 표면의 재구성 (Surface Reconstruction on Hydrogen Covered W(011))

  • 김희봉;최원국;홍사용;황정남;정광호
    • 한국진공학회지
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    • 제1권1호
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    • pp.83-87
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    • 1992
  • 최근 Angle Resolved Ultraviolet Photoemission Spectroscopy(ARUPS)를 통하여 Mo(011)과 W(011)의 surface Fermi contour에 관한 연구가 발표되었다. Hydrogen 흡착시 W(011)의 electron contour는 팽창하였다. 이것은 electron contour를 이루는 surface state가 hydrogen 흡착시 higher binding energy로 이동한 결과이다. Surface state의 higher binding energy로의 이동은 결국 band flattening으로 이해되며, 이 band flattening 에 S.E.Trullinger의 long range dipole dipole force와 Kohn anomaly 현상을 부합시켜 W(011) surface에 수소 흡착시 일어나는 reconstruction 현상에 대한 설명을 시도해 보았다.

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7075-T651 Al合金의 表面균열進展에 미치는 應力比의 影響 (The Effect of Stress Ratio on the Surface Crack Growth Behavior in 7075-T651 Aluminum Alloy)

  • 박영조;김정규;신용승;김성민
    • 대한기계학회논문집
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    • 제10권1호
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    • pp.62-69
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    • 1986
  • 본 연구에서는 표면균열의 전파거동에 관한 연구의 일환으로 경량화재료 로서 항공기 구조용으로 널리 사용되고 있는 7075-T651 알루미늄합금을 준비하고 제하탄성 compliance법을 이용하여 표면 및 깊이 방향의 균열진전거동의 특성을 밝히고져 한다.

해면 산란효과에 의한 선박 방사소음 추정치 오차 (Error Characteristics of Ship Radiated Noise Estimation by Sea Surface Scattering Effect)

  • 박규칠;박지현;서철원;최재용;이필호;윤종락
    • 한국소음진동공학회논문집
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    • 제23권6호
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    • pp.563-573
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    • 2013
  • The ship radiated noise level fluctuates by the interference between direct and reflected paths. The effect of sea surface reflection path on interference depends strongly on sea surface roughness. This paper describes error characteristics of ship acoustic signature estimation by sea surface scattering effect. The coherent reflection coefficient which explains a magnitude of sea surface scattering and its resultant interference acoustic field is analyzed quantitatively as a function of a grazing angle, effective surface height, frequency, source-receiver range and depths of source and receiver. Theoretical interference acoustic field is compared with experimental result for two different sea surfaces and five different frequencies by changing source-receiver range. It is found that both matches well each other and a magnitude of interference acoustic field is decreasing by increasing a grazing angle, effective surface height, frequency, and depths of source and receiver and decreasing source-receiver range. For given experimental conditions, the transmission anomaly which is a bias error of ship acoustic signature estimation, is about a range of 1~3 dB. The bias error of an existing ship radiated noise measurement system is also analyzed considering wind speed, source depth and frequency.

스테레오 비젼에 의한 생체표면 3차원 복원의 최적화 연구 (A Study on the Optimization for Three Dimensional Reconstruction of Bio Surface Using by Stereo Vision)

  • 이경채;이언석
    • 전기학회논문지
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    • 제66권1호
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    • pp.107-113
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    • 2017
  • Unlike regular images, there is no ground truth for bio surface images. Result of biosurface imaging is not only significantly affected by the environment and the condition of the bio surface, it requires more detailed expression than regular images. Therefore, unlike algorithms tested on regular images, studies on bio surface images requires a highly precise optimization process. We aim to optimize the graph cut algorithm, known to be the most outstanding among the stereo visions, by considering baseline, lambda, and disparity range. Optimal results were in the range of 1~10 for lambda. The disparity ranged from -30 to -50, indicating an optimal value in a slightly higher range. Furthermore, we verified the tested optimization data using SIFT.

큐폴라 용해로 철피의 열응력 및 피로수명 해석 (Analysis of Thermal Stress and Fatigue Life in the Steel Shell of a Cupola Furnace)

  • 양영수;배강열
    • 한국기계가공학회지
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    • 제19권2호
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    • pp.47-54
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    • 2020
  • Themo-mechanical analysis was carried out using the finite element method for the steel shell of a cupola furnace. When the outer surface of the shell was cooled with water to within the temperature range of 35-80 ℃ during operation of the cupola, the inner surface of the shell was expected to exhibit a temperature of 65-248 ℃ based on heat transfer analysis. The shell was also expected to have an equivalent stress range of 100-280 MPa in the outer surface over the temperature range examined. Upon cooling the shell to obtain an outer surface temperature <80 ℃, the maximum equivalent stress of the shell did not exceed the yield strength. Although the temperature of the outer surface varied between 35 and 80 ℃ periodically due to the cooling control problem, the fatigue stress at the outer surface of the shell was calculated to be within the fatigue strength. During a non-operational period to examine the system between furnace operations, the thermal stress presented in the shell was sufficiently low to reach the desired yield strength and fatigue limit.