• Title/Summary/Keyword: Surface hardness method

Search Result 506, Processing Time 0.027 seconds

AN EFFECT OF Nd : VAG LASER IRRADIATION ON THE MICROHARDNESS OF ROOT SURFACE (Nd : YAG layer 조사가 치근면의 미세경도에 미치는 영향)

  • Ahn, Jae-Hyeun;Kim, Byung-Ok;Han, Kyung-Yoon
    • Journal of Periodontal and Implant Science
    • /
    • v.25 no.3
    • /
    • pp.614-622
    • /
    • 1995
  • Root caries is very frequently developed on exposed root surface after periodontal surgical treatment. In order to determine the anti-caries effect of Nd : YAG laser irradiation on periodontally exposed root surface, 40 mandibular molar teeth that had been extracted due to excessive periodontal destruction were used as the experimental teeth. All teeth were treated by the same procedure as conventional periodontal root treatment, ie thorough scaling, root planing and root conditioning with tetracycline HCl(100mg/ml, 5min.). Within middle one third of root, mesial half surface(20) or distal half surface(20) was randomly irradiated at various power of 1.0W, 2.0W, 3.0W and 4.0W for 60 seconds by non-contact(5mm) delivery of a pulsed Nd : YAG laser(EN.EL.EN060, Italy). The microhardness was measured by Vikers microhardness tester(Wilson, USA) at 2mm/second of jog speed under 100gm load. The difference of microhardness between irradiated side and non-irradiated side was statistically analyzed ANOVA and Duncan's method. Following results were obtained ; 1. The microhardness(Knoop hardness number) was significantly higher in laser irradiated surface than non-irradiated surface(p<0.05). 2. There was no significant difference in microhardness between experimental groups classified by different laser power(p>0.1). The results suggest that Nd : YAG laser irradiation on exposed root suface after periodontal therapy may inhibit the root caries development by enhancing surface microhardness.

  • PDF

Biocompatibility and Surface Characteristics of PEO-treated Ti-40Ta-xZr Alloys for Dental Implant Materials

  • Yu, Ji-Min;Cho, Han-Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
    • /
    • 2018.06a
    • /
    • pp.23-23
    • /
    • 2018
  • In this study, new titanium alloys were prepared by adding elements such as tantalum (Ta), zirconium (Zr) and the like to complement the biological, chemical and mechanical properties of titanium alloys. The Ti-40Ta-xZr ternary alloy was formed on the basis of Ti-40Ta alloy with the contents of Zr in the contents of 0, 3, 7 and 15 wt. %. Plasma electrolytic oxidation (PEO), which combines high-voltage sparks and electrochemical oxidation, is a novel method to form ceramic coatings on light metals such as Ti and its alloys. These oxide film produced by the electrochemical surface treatment is a thick and uniform porous form. It is also composed of hydroxyapatite and calcium phosphate-based phases, so it has the characteristics of bone inorganic, non-toxic and very high bioactivity and biocompatibility. Ti-40Ta-xZr alloys were homogenized in an Ar atmosphere at $1050^{\circ}C$ for 1 hour and then quenched in ice water. The electrochemical oxide film was applied by using a power supply of 280 V for 3 minutes in 0.15 M calcium acetate monohydrate ($Ca(CH_3COO)_2{\cdot}H_2O$) and 0.02 M calcium glycerophosphate ($C_3H_7CaO_6P$) electrolyte. A small amount of 0.0075M zinc acetate and magnesium acetate were added to the electrolyte to enhance the bioactivity. The mechanical properties of the coated surface of Ti-40Ta-xZr alloys were evaluated by Vickers hardness, roughness test, and elastic modulus using nano-indentation, and the surface wettability was evaluated by measuring the contact angle of the coated surface. In addition, cell activation and differentiation were examined by cell culture of HEK 293 (Human embryonic kidney 293) cell proliferation. Surface properties of the alloys were analyzed by scanning electron microscopy(FE-SEM), EDS, and X-ray diffraction analysis (XRD).

  • PDF

Prediction and development on technics of landslide prospecting by seismic refraction(PS-1) (소형 탄성파탐사기(PS-1)을 이용한 산사태예지기술개발)

  • 김재헌
    • Journal of the Korean Professional Engineers Association
    • /
    • v.25 no.4
    • /
    • pp.102-108
    • /
    • 1992
  • This study was carried to find out the soil characteristics of landslide site and to develope landslide prediction method by seismic refraction prospecting. For these aims, landslide condition and travel time were investigated at 68 Landslide sites over the country during 1990 to 1991. The results were as follows. 1. The surface of rupture was included mainly in C layer. Its Hardness was less than 3kg / $\textrm{cm}^2$ at the upper pare of landslide. 2. When the profile line length was 20m, the range of travel time was 40 to 90 msec. The travel time did not differ between bedrocks. 3. Refraction distance ranged from 1 to 7m and mean of that was 2.5m. Travel time was increased according to receiving distance without large variance in the refraction distance but that was appeared large variance out of the refraction distance on slope that has shallow soil depth and discontinuous ground surface. Therefore, the spread distance must be shorten to 10-l5m. 4. The seismic velocity at the first layer(layer of rupture) was less than 500m1sec by degree of weathering and the velocity at the second layer decreased in order of Granite> Granitic gneiss >Sedimentary rock. 5. The first layer observed by seismic refraction was contained C layer that has parent material and weathered rocks of hardness 10-20kg/$\textrm{cm}^2$. 6. Among the range of seismic velocity was less than 200m/sec in 63% of the total plots, 200-300m/sec in 34% and 300-500m /sec in 3%. 7. There was a proportional relationship between seismic prospecting soil depth and executive soil depth, and seismic propection soil depth was about 10 to 20cm deeper than the order.

  • PDF

Coatings Properties and Efficiency Performance of Cr-DLC Films Deposited by Hybrid Linear Ion Source for Hydraulic Gear Pump (하이브리드 선형이온원에 의한 유압 기어펌프용 Cr-DLC코팅막의 특성과 효율성능)

  • Cha, Sun-Yong;Kim, Wang-Ryeol;Park, Min-Suk;Kwon, Se-Hun;Chung, Won-Sub;Kang, Myung-Chang
    • Journal of Powder Materials
    • /
    • v.17 no.6
    • /
    • pp.456-463
    • /
    • 2010
  • This paper describes the results of the application of Cr-Diamond-like carbon (DLC) films for efficiency improvement through surface modification of spur gear parts in the hydraulic gear pump. Cr-DLC films were successfully deposited on SCM 415 substrates by a hybrid coating process using linear ion source (LIS) and magnetron sputtering method. The characteristics of the films were systematically investigated using FE-SEM, nano-indentation, sliding tester and AFM instrument. The microstructure of Cr-DLC films turned into the dense and fine grains with relatively preferred orientation. The thickness formed in our Cr buffer layer and DLC coating layer were obtained the 487 nm and $1.14\;{\mu}m$. The average friction coefficient of Cr-DLC films considerably decreased to 0.15 for 0.50 of uncoated SCM415 material. The hardness and surface roughness of Cr-DLC films were measured 20 GPa and 10.76 nm, respectively. And then, efficiency tests were performed on the hydraulic gear pump to investigate the efficiency performance of the Cr-DLC coated spur gear. The experimental results show that the volumetric and mechanical efficiency of hydraulic gear pump using the Cr-DLC spur gear were improved up to 2~5% and better efficiency improvement could be attributed to its excellent microstructure, higher hardness, and lower friction coefficient. This conclusion proves the feasibility in the efficiency improvement of hydraulic gear pump for industrial applications.

Effects of Oxygen Plasma-treated Graphene Oxide on Mechanical Properties of PMMA/Aluminum Hydroxide Composites (산소 플라즈마 처리된 그래핀 산화물이 PMMA/수산화알루미늄 컴포지트의 기계적 물성에 미치는 영향)

  • Kim, Hyo-Chul;Jeon, Son-Yeo;Kim, Hyung-Il;Choi, Ho-Suk;Hong, Min-Hyuk;Choi, Ki-Seop
    • Polymer(Korea)
    • /
    • v.35 no.6
    • /
    • pp.565-573
    • /
    • 2011
  • The nanocomposites containing graphene oxide (GO) were prepared in order to improve the mechanical properties of poly(methyl methacrylate)/aluminum hydroxide (PMMA/AH) composites. GO was prepared from graphite by oxidation of Hummers method followed by exfoliation with thermal treatment. The surface of GO was modified by oxygen plasma in various exposure times from 0 to 70 min to improve interfacial compatibility. Compared with PMMA/AH composites, the nanocomposites containing GO modified with oxygen plasma for the exposure time up to 50 min showed significant increases in flexural strength, flexural modulus, Rockwell hardness, Barcol hardness, and Izod impact strength. The morphology of fracture surface showed an improved interfacial adhesion between PMMA/AH composites and GO, which was properly treated with oxygen plasma. The mechanical properties of nanocomposites were deteriorated by increasing the content of GO above 0.07 phr due to the nonuniform dispersion of GO.

A Study on the Overlay Welding Process Optimization of GTAW by Double Torch (GTAW Double Torch의 육성용접 공정최적화에 관한 연구)

  • Lim, Byung-Chul;Son, Young-San
    • Journal of the Korea Academia-Industrial cooperation Society
    • /
    • v.17 no.3
    • /
    • pp.73-78
    • /
    • 2016
  • In this study, GTAW was carried out on austenitic STS316 stainless steel. Overlay welding with the stellite-base filler metal was implemented using a double torch. The response variable was calculated on the measured Vickers hardness for process optimization using the Taguchi method and its response variable was then analyzed about effect on overlay welding characteristics. The optimal process design by the Taguchi method is extremely effective in the overlay welding process for the multiple response variables. In addition, the effects of contribution rate about each response variable was analyzed easily. The conditions of the optimal process were 105A, 18V, pre-heat treatment at $200^{\circ}C$, and post weld heat treatment at $100^{\circ}C$. The Vickers hardness of the specimens produced under the optimal condition of GTAW by the double torch was 8.19% higher than that by a single torch.

Development of Low-Temperature Storage Method of Sweet Persimmons (단감의 저온저장방법(低溫貯藏方法) 개발(開發)에 관(關)한 연구(硏究))

  • Chung, J.H.;Suh, S.R.
    • Journal of Biosystems Engineering
    • /
    • v.19 no.3
    • /
    • pp.232-246
    • /
    • 1994
  • This study was conducted to develop the long-tenn storage method to minimize the black spot occurred on the surface of persimmons stored in the films at low temperature. The storage experiments were done with different films and persimmon varieties at $0^{\circ}C$ storage condition for 5 months, and then the physical and chemical characteristics of persimmons were tested monthly. The results were as follows : 1. The film 160 made from zeolites showed highest performance in well storings sweet persimmons for 5 months, compared with other films by eyesight. The initial moisture condensation inside the films seemed to cause the black spots on persimmons, and the effect of the film holes was never significant to prevent the black spots. 2. The sugar content was ranged from $14^{\circ}Brix$ to $15^{\circ}Brix$ regardless of film types and persimmom varieties, and it changed little for storage of 5 months. 3. The decrease rate of persimmom weight in the film 160 and 180 was 0.3% for storage of 5 months, while those in other films reached to 2%. The decrease rate of persimmon weight was least in the film 160 and 180. 4. The hardness of Fuyu least decreased in the films 160 and 380. It was changed from 36 kg/cnf to 8-27 $kg/cm^2$, and that of Charyang was from 31 $kg/cm^2$ to 8-10 $kg/cm^2$ for storage of 5 months. The hardness of Charyang rapidly decreased as storage period increased. 5. The average rate of black spot(defect rate) of Fuyu measured by a computer image processing system was least in the film 160 by 0.5%, but those in other films was ranged from about 5% to 20% for storage of 5 months. The rate of black spot of Charyang was less than that of Fuyu among most of films. 6. The intensity, hue, and saturation in persimmon color changed according to storage period. Especially, the intensity of persimmon colors decreased as storage period increased, but it was least in the film 160. 7. An integrated long-term storage method of sweet persimmons was suggested in the basis of the experiments and literature reviews.

  • PDF

Effect of Plasma Density on the Tribological Properties of Amorphous Carbon Thin Films (비정질 탄소박막의 트라이볼로지 특성에 미치는 플라즈마 밀도의 영향)

  • Park, Y.S.;Lee, J.D.;Hong, B.
    • Journal of the Korean Vacuum Society
    • /
    • v.20 no.5
    • /
    • pp.333-338
    • /
    • 2011
  • In this work, we have fabricated the amorphous carbon (a-C:H) thin film by using unbalanced magnetron sputtering method with the magnetron source of inside/outside electromagnetic coils as the protective coating materials. We have investigated the tribological properties of amorphous carbon films prepared with various electromagnetic coil currents for the change of the plasma density, such as hardness, friction coefficient, adhesion, and surface roughness. Raman and HRTEM were used to study the microstructure of carbon films. In the result, the hardness and adhesion properties of a-C:H films were improved with increasing electromagnetic coil current due to the increase of the plasma density to the substrate. Thus, these results can be explained by the increase of $sp^2$ bonding and cluster number in the amorphous carbon film, related to the improved bombardment around substrate and the increased substrate temperature.

Mechanical Properties of OFC Copper Fabricated by Multi-Axial Diagonal Forging (MADF) (다축대각단조(MADF) 가공한 구리의 기계적 성질)

  • Kwon, S.C.;Kim, S.T.;Kim, D.V.;Lee, J.K.;Seo, S.J.;Yoon, T.S.;Jeong, H.T.
    • Transactions of Materials Processing
    • /
    • v.27 no.4
    • /
    • pp.250-256
    • /
    • 2018
  • Oxygen-free copper (OFC) was prepared as a 90 mm cube and then processed with Multi-Axial Diagonal Forging - Initialization of Prior manufacturing History (MADF). The MADF process has been newly developed as a severe plastic deformation method. The MADF process consists of upset forging with a thickness reduction of 30% and diagonal forging with a diagonal angle of $135^{\circ}$. 1 cycle process consists of a 12 passes forging process. In order to analyze the characteristic changes according to the number of iterations, 1, 2, and 3 cycles of the MADF process were performed. The OFC specimens were MADF processed without surface cracks up to 3 cycles. The microstructure, hardness and tensile test of processed materials were analyzed to study the change of material properties according to the amount of MADF process. The results showed that the MADF process effectively refined the microstructure and increased the strength of OFC. In the case of specimens processed for more than 2 cycles, the grains of all measurement regions were refined to be less than $7{\mu}m$ of grain size. The 1 cycle MADF processed OFC showed the highest mechanical properties with the hardness of 132 HV and tensile strength of 395 MPa. Hardness and strength seemed to be saturated when processed over 2 cycles.

Stable Desalination of Hardness Substances through Charge Control in a Capacitive Deionization System (축전식 탈염 시스템에서 전하량 제어를 통한 경도물질의 안정적인 탈염)

  • Kim, Yoon-Tae;Choi, Jae-Hwan
    • Applied Chemistry for Engineering
    • /
    • v.30 no.4
    • /
    • pp.472-478
    • /
    • 2019
  • A stable desalination method of the hardness substance such as $Ca^{2+}$ by controlling the total charge (TC) supplied to the membrane capacitive deionization (MCDI) cell was studied. The adsorption (1.5 V) and desorption (0.0 V) were repeated 30 times while varying the TC in the adsorption process. The concentration and pH of effluent, adsorption and desorption amounts, current densities and cell potentials were analyzed in the desalination process. The maximum allowable charge (MAC) of the carbon electrode used in MCDI cell was measured to be 46 C/g. As a result of operation at TC (40 C/g) below the MAC value, electrode reactions did not occur, resulted in the stable desalination characteristics for a long-term operation. When operating at TCs (50, 60 C/g) above the MAC value, however, the concentration and pH of effluent varied greatly. Also, the scale was formed on the electrode surface due to electrode reactions, and the electric resistance of the cell gradually increased. It was thus concluded that it is possible to remove stably the hardness substance without any electrode reactions by controlling the charge supplied to MCDI cell during the adsorption process.