• Title/Summary/Keyword: Surface examination

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Nitrogen Adsorption Analysis of Wood Saccharification Residues

  • Yang, Han-Seung;Tze, William Tai Yin
    • Journal of the Korean Wood Science and Technology
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    • v.45 no.2
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    • pp.232-242
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    • 2017
  • The objective of this study was to examine changes in the porosity and internal structure of wood as it goes through the process of saccharification (extraction of fermentable sugars). This study also examined the use of different drying methods to prepare samples for characterization of internal pores, with particular emphasis on the partially disrupted cell wall. Aspen wood flour samples after dilute acid pretreatment followed by enzymatic hydrolysis were examined for nitrogen adsorption. The resulting isotherms were analyzed for surface area, pore size distribution, and total pore volume. Results showed that freeze drying (with sample pre-freezing) maintains the cell wall structure, allowing for examination of saccharification effects. Acid pretreatment (hemicellulose removal) doubled the surface area and tripled the total volume of pores, which were mostly 10-20 nm wide. Subsequent enzymatic hydrolysis (cellulose removal) caused a 5-fold increase in the surface area and a ~ 11-fold increase in the total volume of pores, which ranged from 5 to 100 nm in width. These results indicate that nitrogen adsorption analysis is a feasible technique to examine the internal pore structure of lignocellulosic residues after saccharification. The information on the pore structure will be useful when considering value-adding options for utilizing the solid waste for biofuel production.

The Effect of Arabic Gum on the Copper Electrodeposition using Titanium Substrate (티타늄 기지을 이용한 구리 전해도금 시 Arabic Gum 첨가제의 영향)

  • Woo, Tae-Gyu;Park, Il-Song;Lee, Hyun-Woo;Seol, Kyeong-Won
    • Korean Journal of Materials Research
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    • v.16 no.12
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    • pp.725-730
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    • 2006
  • The purpose of this study is to identify the effect of additives during copper electrodeposition. Additives such as arabic gum, chloride ions and glue were used in this study. Electrochemical experiments allied to SEM and roughness examination were performed to characterize of the copper foil in the presence of additives. In the production of electrodeposited copper foil, the surface roughness and grain size of the copper foil can be controlled by addition additives. on this study, the more uniform and hemispherical copper crystals are during the initial stages, the smaller crystal size and surface roughness of copper foil are. The surface roughness of copper foil electrodeposited at the current density of 500 $mA/cm^2$ under galvanostatic mode for 60 seconds has a minimum value of 0.136 ${\mu}$m when adding 2 ppm of arabic gum.

Response of Ecosystem Carbon and Water Vapor Exchanges in Evolving Nocturnal Low-Level Jets

  • Hong, Jin-Kyu;Mathieu, Nathalie;Strachan, Ian B.;Pattey, Elizabeth;Leclerc, Monique Y.
    • Asian Journal of Atmospheric Environment
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    • v.6 no.3
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    • pp.222-233
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    • 2012
  • The nocturnal low-level jet makes a significant impact on carbon and water exchanges and turbulent mixing processes in the atmospheric boundary layer. This study reports a case study of nocturnal surface fluxes such as $CO_2$ and water vapor in the surface layer observed at a flat and homogeneous site in the presence of low-level jets (LLJs). In particular, it documents the temporal evolution of the overlying jets and the coincident response of surface fluxes. The present study highlights several factors linking the evolution of low-level jets to surface fluxes: 1) wavelet analysis shows that turbulent fluxes have similar time scales with temporal scale of LLJ evolution; 2) turbulent mixing is enhanced during the transition period of low-level jets; and 3) $CO_2$, water vapor and heat show dissimilarity from momentum during the period. We also found that LLJ activity is related not only to turbulent motions but also to the divergence of mean flow. An examination of scalar profiles and turbulence data reveal that LLJs transport $CO_2$ and water vapor by advection in the stable boundary layer, suggesting that surface fluxes obtained from the micrometeorological method such as nocturnal boundary layer budget technique should carefully interpreted in the presence of LLJs.

EARLY CONNECTIVE TISSUE ATTACHMENT ON DENTIN SURFACE TREATED WITH CITRIC ACID, TETRACYCLINE AND FIBRIN SEALANTS (구연산, 테트라싸이클린, 섬유소 전색제로 처리된 상아질면에 대한 결체조직의 조기부착)

  • Lee, Hea-Ja;Han, Soo-Boo;Ko, Jae-Sung
    • Journal of Periodontal and Implant Science
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    • v.23 no.2
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    • pp.283-299
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    • 1993
  • The purpose of this study was to observe early connective tissue attachment on dentin surface treated with citric acid, tetracycline, and fibrin sealants and compare their conditioning effects on dentin surface. Experimental dentin blocks conditioned with citric acid, tetracycline or fibrin sealant, and only root planned control block were surgically implanted in the pouch under buccal mucoperiosteal flaps of left mandible, right maxilla, left maxilla, right mandible of 18 male rabbits. Rabbits were sacrificed after 1 and 6 hours, 1, 3, 7 and 14 days after implantation and then specimens including dentin block and surrounding soft tissue were obtained, and prepared for light and transmission electron microscopic examination. 1 and 6 hours after dentin block implantation, there was plasma proteins adsorption followed by fibrin clot formation and no differences among specimens. At the 1-day observation interval, delicate fibrin network was observed in the all groups, and there were proliferative fibroblasts, angiogenesis and macrophage in the all 3-day specimens. Cellular aggregates and abundant connective tissue adhered dentin surface and tetracycline or citric acid treated group showed much proliferative fibroblast and abundant collagen fibers at 1 week. But at 2 week, citric acid treated group showed much proliferative fibroblast and abundant collagen fibers. These observations suggested that new connective tissue attachment to dentin was initiated by the adsorption of plasma proteins to the dentin surface and followed by fibrin clot formation. Tetracycline and citric acid seemed to make dentin surface more biologically favorable for the connective tissue attachment.

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AN EXPERIMENTAL STUDY ON THE DIMENSIONAL CHANGES OF RELINED DENTURES AND MECHANICAL PROPERTIES AND SURFACE TEXTURES OF SEVERAL RESINS USED IN DENTURE RELINING (수종 레진으로 의치상 조직면 개조시 의치상의 크기변화와 물리적 성질 및 표면상태 비교 연구)

  • Lee, Chang-Han;Kim, Yung-Soo
    • The Journal of Korean Academy of Prosthodontics
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    • v.28 no.1
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    • pp.25-41
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    • 1990
  • The purpose of this study was to evaluate and compare the dimensional changes of relined dentures with a light-curing resin, a heat-curing resin, and a direct, hard reline resin. And also to measure the transverse strength, impact strength, surface hardness of the three resins used in relining. The surface textures of three resins also of evaluated by using scanning electron microscope. Through analyses on the data from this study, the following conclusions were obtained. 1. Impact strength of heat-curing resin was highest, and direct, hard reline resin higher, light-curing resin lowest. 2. Transverse strength of heat-curing resin was highest, and direct, hard reline resin and light-curing resin was lower and not signiicantly different. 3. Surface hardness of light-curing resin was lighest, heat-curing resin higher, and direct, hard reline resin was lowest. 4. After storage of the relined dentures for 1 day and 1 week in water at room temperature, linear shrinkage of distance between the reference points in the maxillary base relined with direct, hard reline resin was lowest, and those relined with light-curing resin and heat-curing resin were lower and were not significantly different. 5. After storage for 4 weeks in orator at room tempeature, linear shrinkage of distance between ridge crests of dentures relined with heat-curing resin was highest and that of distance between denture borders was not significantly different. 6. The dimensional changes of relined dentures during storage in water was not significant except those of distance between denture borders relined with light-curing resin at 1 day and 1 week storage in water. 7. At low magnification (x40) of SEM examination, the surface textures of three resins were similar except light-curing resin which had some defects. At high magnification (x200), the surface textures of hard, direct reline resin were smooth with little defects, but those of heat-curing resin and light-curing resin w ere irregular.

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Microscopic Examination of Fracture Particles on the Surface of Ir-192 Sealed Source and Ultrasonic Cleaning (Ir-192 밀봉선원의 표면오염 방지)

  • Kuk, Il Hiun;Park, Chun Deuk;Koo, Ja Ho
    • Journal of Radiation Industry
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    • v.9 no.2
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    • pp.91-102
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    • 2015
  • The iridium disc, generally used in industrial radiography, is examined to find the fracture morphology and fine particles remaining on the shear blank surface. Randomly selected 1,200 discs were observed under a scanning electron microscope tilted more than $45^{\circ}$. Fracture surfaces are classified into three groups: (1) surface fall-out, (2) fracture on the edge and (3) multi-step brittle fracture, which shows the mutual relationship between the fracture morphology and remaining particles. Fracture particles were removed by cleaning the discs in a ultrasonic bath with acetone and collected at the bottom. Removed number of the particles were counted for each different group of fracture surfaces. Followings are conclusions: (1) About 80.5% of discs (966/1,200), have sound plastic shear surfaces with particles remained. (2) About 2% discs accompany surface fall-out's having large particles tens of ${\mu}m$, which is stable not to be pulled out even after the considerably long time of ultrasonic cleaning. (3) About 5% discs contain the fractures on the edge and the particles are removed thoroughly within 30 minutes. (4) 234 discs out of 1,200 discs have multi-step fracture surfaces whose particles never removed in a short period of time but come out very slowly. Such a disc having multiple-step fracture is attributed to the promate cause to the 'leaker'. It is noted here that the discs having mutiple-step fractures should be treated separately with special care, and it is need to study how to treat them.

Evaluation of Radiation Exposure to Nurse on Nuclear Medicine Examination by Use Radioisotope (방사성 동위원소를 이용한 핵의학과 검사에서 병동 간호사의 방사선 피폭선량 평가)

  • Jeong, Jae Hoon;Lee, Chung Wun;You, Yeon Wook;Seo, Yeong Deok;Choi, Ho Yong;Kim, Yun Cheol;Kim, Yong Geun;Won, Woo Jae
    • The Korean Journal of Nuclear Medicine Technology
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    • v.21 no.1
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    • pp.44-49
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    • 2017
  • Purpose Radiation exposure management has been strictly regulated for the radiation workers, but there are only a few studies on potential risk of radiation exposure to non-radiation workers, especially nurses in a general ward. The present study aimed to estimate the exact total exposure of the nurse in a general ward by close contact with the patient undergoing nuclear medicine examinations. Materials and Methods Radiation exposure rate was determined by using thermoluminescent dosimeter (TLD) and optical simulated luminescence (OSL) in 14 nurses in a general ward from October 2015 to June 2016. External radiation rate was measured immediately after injection and examination at skin surface, and 50 cm and 1 m distance from 50 patients (PET/CT 20 pts; Bone scan 20 pts; Myocardial SPECT 10 pts). After measurement, effective half-life, and total radiation exposure expected in nurses were calculated. Then, expected total exposure was compared with total exposures actually measured in nurses by TLD and OSL. Results Mean and maximum amount of radiation exposure of 14 nurses in a general ward were 0.01 and 0.02 mSv, respectively in each measuring period. External radiation rate after injection at skin surface, 0.5 m and 1 m distance from patients was as following; $376.0{\pm}25.2$, $88.1{\pm}8.2$ and $29.0{\pm}5.8{\mu}Sv/hr$, respectively in PET/CT; $206.7{\pm}56.6$, $23.1{\pm}4.4$ and $10.1{\pm}1.4{\mu}Sv/hr$, respectively in bone scan; $22.5{\pm}2.6$, $2.4{\pm}0.7$ and $0.9{\pm}0.2{\mu}Sv/hr$, respectively in myocardial SPECT. After examination, external radiation rate at skin surface, 0.5 m and 1 m distance from patients was decreased as following; $165.3{\pm}22.1$, $38.7{\pm}5.9$ and $12.4{\pm}2.5{\mu}Sv/hr$, respectively in PET/CT; $32.1{\pm}8.7$, $6.2{\pm}1.1$, $2.8{\pm}0.6$, respectively in bone scan; $14.0{\pm}1.2$, $2.1{\pm}0.3$, $0.8{\pm}0.2{\mu}Sv/hr$, respectively in myocardial SPECT. Based upon the results, an effective half-life was calculated, and at 30 minutes after examination the time to reach normal dose limit in 'Nuclear Safety Act' was calculated conservatively without considering a half-life. In oder of distance (at skin surface, 0.5 m and 1 m distance from patients), it was 7.9, 34.1 and 106.8 hr, respectively in PET/CT; 40.4, 199.5 and 451.1 hr, respectively in bone scan, 62.5, 519.3 and 1313.6 hr, respectively in myocardial SPECT. Conclusion Radiation exposure rate may differ slightly depending on the work process and the environment in a general ward. Exposure rate was measured at step in the general examination procedure and it made our results more reliable. Our results clearly showed that total amount of radiation exposure caused by residual radioactive isotope in the patient body was neglectable, even comparing with the natural radiation exposure. In conclusion, nurses in a general ward were much less exposed than the normal dose limit, and the effects of exposure by contacting patients undergoing nuclear medicine examination was ignorable.

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Comparative Study of the Ablation Rates of Er: YAG Laser Irradiation on Dentin and Enamel (Er:YAG 레이저를 이용한 법랑질과 상아질의 절삭율 연구)

  • Kim, Kun-A;Ahn, Yong-Woo;Ko, Myung-Yun;Park, June-Sang
    • Journal of Oral Medicine and Pain
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    • v.30 no.1
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    • pp.131-140
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    • 2005
  • The purpose of this study was to examine the ablation rate of Er: YAG laser irradiation on dentin and enamel and to observe the microscopic structures of cavities formed after ablation of enamel and dentin in using a bur and cavities formed after ablation using laser. Er:YAG laser irradiated at 200 mJ, 250mJ, 300mJ at the frequency of 20Hz, 15Hz. The following results were obtained : 1. The ablation rate of dentin groups at power of 3 W-6 W was about $1.103{\sim}2.639mm^3/sec$ and there were no significant differences between power of 4.5 W$\sim$6 W. 2. The ablation rate of enamel groups at power of 3 W-6 W was about $0.413{\sim}0.969mm^3/sec$ and there were no significant differences between power of 4 W$\sim$6 W. 3. With SEM examination of the cavity surface treated with the conventional high speed bur revealed relatively flat appearance almost covered with a debris like smear layer. 4. With SEM examination of the lased surface of dentin groups revealed no smear layer and no debris and openings of dentinal tubules were clearly opened. But the lased surfaces of the groups over 3 W were irregular and particles were loosely attached on it. 5. With SEM examination of the lased surface of enamel groups revealed severely destructed surface at the 6 W group and melting drop materials at the 3 W group. But the lased surface of 4 W group revealed clearly ablated surface. Therefore when cutting teeth using Er:YAG laser, the lasing power which can make effective ablation rate and minimize the thermal effect could be 3W at dentin and 4W at enamel. But, further studies and additional data collection will be necessary for appropriate lasing condition of Er:YAG laser.

The examination of the pores of casting bodies depending on the position of wax pattern in the ring for precious alloys (Ring 내 납형의 위치에 따른 귀금속합금 주조체의 수축공 관찰)

  • Park, Min-Ju;Noh, Hak;Ko, Dae-Jin;Jung, Jong-Hyun
    • Journal of Technologic Dentistry
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    • v.30 no.1
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    • pp.9-15
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    • 2008
  • An investigation was carried out to examine the pores of casting bodies depending on the position of wax pattern in the ring for precious alloy by optical micrographs. From the result of optical micrographs, many pores were found in the Group C that wax pattern is placed in the center of the ring. However, any pores were scarcely found in the Group A, B, D and E that wax patterns are placed out of the center of thermal zone. In comparison with the pores of casting bodies of Group C, many pores were found at the cusp area rather than at the proximal surface. From these examination, it was concluded that wax pattern should be placed out of the center of thermal zone to prevent casting boies from occurring pores.

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Study on Runoff Characteristics of Nonpoint Sources during Rainfall in Anyangchun Watershed (안양천 유역의 강우시 비점오염원에 따른 유출부하특성에 관한 연구)

  • Hwang, Byung-Gi;Yu, Se-Jin;Cha, Young-Ki
    • Journal of Environmental Impact Assessment
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    • v.10 no.3
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    • pp.223-234
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    • 2001
  • In this study, we conducted a survey to examine the runoff characteristics of nonpoint sources, which wash off pollutants from the surface of basin during rainfall and affect water pollution of streams. An Anyangchun basin in the region Ewiwang City was selected as a study site. The basin divided into several subbasins such as Wanggokchun, Ojeonchun, and Anyangchun based on the tributaries, which confluence to the main stream of Anyangchun. Four times of field examination had been carried out between July and August of 2000, and water quality data collected from the surveys had been analysed. The survey includes in-situ flow, DO and PH measurements in the outlet of catchment. Laboratory analysis includes BOD, TN, TP. From the result, pollutant by runoff of nonpoint sources were washed out along with stormwater in the beginning of rainfall, and flowed into streams resulted in stream pollution. In case of BOD, the load from Ojeonchun catchment, most of which included urban areas, took up 50% of the total load from the entire watershed. Thus, by the results, it is clear that runoff load by urban nonpoint sources plays an important role in the control and management of nonpoint sources for the watershed.

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