• 제목/요약/키워드: Surface Profiling

검색결과 134건 처리시간 0.024초

Al-1%Si/SiO2/PSG 적층 박막에서 potassium 게터링에 관한 연구 (A Study on the Potassium Gettering in Al-1%Si/SiO2/PSG Multilevel Thin Films)

  • 김진영
    • 한국표면공학회지
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    • 제48권5호
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    • pp.233-237
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    • 2015
  • In order to investigate the potassium (K) gettering, Al-1%Si/$SiO_2$/PSG multilevel thin films were fabricated. Al-1%Si thin films and $SiO_2$/PSG passivations were deposited by using DC magnetron sputter techniques and APCVD (atmosphere pressure chemical vapor deposition), respectively. Heat treatment was carried out at $300^{\circ}C$ for 5 h in air. SIMS (secondary ion mass spectrometry) depth profiling analysis was used to determine the distribution of K, Al, Si, P, and other elements throughout the $SiO_2$/PSG passivated Al-1%Si thin film interconnections. Potassium peaks were observed throughout the $SiO_2$/PSG passivation layers, and especially the interface gettering at the $SiO_2$/PSG and at the Al-1%Si/$SiO_2$ interfaces was observed. Potassium gettering in Al-1%Si/$SiO_2$/PSG multilevel thin films is considered to be caused by a segregation type of gettering.

Permeability imaging in granitic rocks based on surface resistivity profiling

  • Sudo Hiroshi;Tanaka Toshikazu;Kobayashi Tsuyoshi;Kondo Tatsutoshi;Takahashi Toru;Miyamoto Masaharu;Amagai Mitsuru
    • 지구물리와물리탐사
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    • 제7권1호
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    • pp.56-61
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    • 2004
  • In order to image the distribution of permeability in granitic rocks, we carried out two-dimensional (2D) resistivity profiling, together with in-situ permeability tests, electrical logging of boreholes, and resistivity measurements of rock core samples in a laboratory. Based on the electrical logging and in-situ permeability data from boreholes, we obtained empirical equations which relate resistivity and permeability of the granitic rocks in the area studied. We then applied the empirical equation to a 2D resistivity section, to produce a 2D permeability section of the granitic rocks. In this paper, we present details of the field data and of the procedure for conversion from the resistivity section to a permeability section. The observed relationship between resistivity and permeability of the rocks is also discussed.

대형 사력댐에서의 전단파속도 평가를 위한 단측선 빔형성기법 (Short-Array Beamforming Technique for the Investigation of Shear-Wave Velocity at Large Rockfill Dams)

  • 조성호;나디아
    • 대한토목학회논문집
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    • 제33권1호
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    • pp.207-218
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    • 2013
  • 대형 사력댐의 내진성능 평가에서 필히 요구되는 입력상수는 사력재료, 코아매질의 전단파 속도이다. 이를 표면파 시험으로 평가하기 위해서는 사력골재의 불연속, 매질의 비균질, 사면 경계면 등 표면파 시험결과의 신뢰도를 떨어뜨리는 조건을 극복해야 한다. 본 연구에서는 이러한 표면파시험의 한계를 극복하기 위하여 기존 빔형성기법의 원리를 응용한 SBF (Short-Array Beamforming) 기법을 제안하였다. SBF 기법은 3~9 m의 짧은 측선과 원거리 발진원을 이용함으로써, 빔형성기법 고유의 장점인 측정자료의 자동화분석뿐만 아니라 근접장 문제의 해결, 국부적 이상대의 발견 등의 기능을 가지도록 개발되었다. 본 연구에서는 이러한 SBF 기법과 IRF(Impulse-Response Filtration) 기법을 활용하여 대형 사력댐의 전단파속도를 신뢰성 있게 평가하는 방법을 정립하였다. 정립된 기법은 사력댐의 사력재료와 유사한 암버럭으로 매립 성토된 철도 노반에서 다운홀 시험, CapSASW (Common-Array-Profiling SASW) 시험과의 비교를 통하여 그 신뢰성과 실용성을 검증하였다.

GENE-EXPRESSION PROFILING OF TITANIUM-CELL INTERACTION

  • Kim, Chang-Su;Hwang, Jung-Won;Ryu, Jae-Jun;Shin, Sang-Wan;Sohn, Sung-Hwa;Kim, Ki-Nam;Kim, Meyoung-Kon
    • 대한치과보철학회지
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    • 제43권3호
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    • pp.393-408
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    • 2005
  • Statement of problem. In the process of bone formation, titanium (Ti) surface roughness is an important factor modulating osteoblastic function. Purpose. This study was carried out to determine the effect of different Ti surface on biologic responses of a human osteoblast-like cell line (MG63). Materials and methods. MG63 cells were cultured on S (smooth), SLA (sandblasted largegrit & acid etching), HA (hydroxyapatite) Ti. The morphology and attachment of the cells were examined by SEM. The cDNAs prepared from total RNAs of MG63 were hybridized to a human cDNA microarray (1,152 elements). Results. The appearances of the surfaces observed with SEM were different in the three types of dental substrates. The surface of SLA and HA were shown to be rougher than S. MG63 cells cultured on SLA and HA were cell-matrix interaction. In the expression of genes involved in osseointegration, upregulated genes were bone morphogenetic protein, Villin, Integrin, Insulin-like growth factors in different surfaces. Downregulated genes were fibroblast growth factor receptor 4, Bcl 2-related protein, collagen, CD4 in different surfaces. Conclusion. The attachment and expression of key osteogenic regulatory genes were enhanced by surface roughness of the dental materials.

Investigation of Nanostructures in Homopolymer and Copolymer Films by Surface Techniques

  • Kang, Minhwa;Lee, Jihye;Lee, Yeonhee
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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    • pp.276-276
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    • 2013
  • Time-Of-Flight Secondary Ion Mass Spectrometry (TOF-SIMS) and Atomic Force Microscopy (AFM) are the useful instruments to measure nanostructures of material surfaces. Surface pattern formation in blending homopolymer and diblock copolymer films was investigated as a function of film thickness and annealing conditions. In this study, surface structures of blending homopolymer [deuterated polystyrene (Mn 20,000), poly (methyl methacrylate) (Mn 18,000)] and diblock copolymer [Poly (deuteratedstyrene(d8)-b-methyl methacrylate) (Mn 19,500-18,100)] films were observed. The AFM result indicated that the nanostructures and film thickness depended on temperature, concentration and solvent. TOF-SIMS depth profiling was obtained for the lamellar morphology of symmetric dPS-b-PMMA which is found to orient parallel to the surface of the substrate. Elemental and molecular depth profiles measured in the negative ion mode by a Cs+ primary ion beam demonstrate variations in hydrogen, deuterium, carbon, oxygen, hydrocarbons and deuterated hydrocarbons within the diblock copolymer according to the depth.

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Roughness Measurement Performance Obtained with Optical Interferometry and Stylus Method

  • Rhee Hyug-Gyo;Lee Yun-Woo;Lee In-Won;Vorburger Theodore V.
    • Journal of the Optical Society of Korea
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    • 제10권1호
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    • pp.48-54
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    • 2006
  • White-light scanning interferometry (WLI) and phase shifting interferometry (PSI) are increasingly used for surface topography measurements, particularly for areal measurements. In this paper, we compare surface profiling results obtained from above two optical methods with those obtained from stylus instruments. For moderately rough surfaces ($Ra{\approx}500\;nm$), roughness measurements obtained with WLI and the stylus method seem to provide close agreement on the same roughness samples. For surface roughness measurements in the 50 nm to 300 nm range of Ra, discrepancies between WLI and the stylus method are observed. In some cases the discrepancy is as large as 109% of the value obtained with the stylus method. By contrast, the PSI results are in good agreement with those of the stylus technique.

푸리에 변환 간섭 해석법을 이용한 구면의 미세 변위 측정 (Profiling of fine displacement of spherical surface using Fourier transform method)

  • 손영준;주신호;권진혁;최옥식
    • 한국광학회지
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    • 제8권3호
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    • pp.199-203
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    • 1997
  • 안구표면과 같은 미세구면의 변위를 알아내기 위하여 Twyman-Green 간섭계를 이용하였으며 반송무늬(carrier fringe)를 형성시켜 푸리에 변환법으로 미세구면의 변위분포를 측정하였다. 기준위치에서 일정한 반송무늬가 형성되도록 한 후 구면이 변화할 때 반송무늬의 변화방향을 관측하였으며, 반송무늬의 변화방향에 의해 구면의 변화방향을 알아내었다. 푸리에 변환법(Fourier transform method)을 이용하여 CCD카메라에서 받아들여진 한 장의 간섭무늬로부터 위상분포를 얻어내고 구면의 변위 분포를 계산하였다. 공간주파수 영역에서 변위에 대한 정보를 분리함으로써 간섭무늬의 배경분포 및 잡음을 제거하였으며, 구면의 변위에 대한 3차원 분포를 이론적인 계산값의 측정오차가 .lambda./10 이내에서 얻어내었다.

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HCD플라즈마를 이용한 반응성 이온플레이팅법에 의한 TiN 코팅 (TiN coatings by HCD plasma enhanced reactive ion plating method)

  • 서용운;황기웅
    • 한국표면공학회지
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    • 제25권3호
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    • pp.133-143
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    • 1992
  • Titanium nitride(TiN) films have been prepared by HCD plasma enhanced reactive ion plating. Density and temperature of the plasma generated by the HCD were investigated. It was shown that parameters such as the substrate bias voltage(0 350V) and N2 flow rate(10 180SCCM) influenced the growth, the growth, the microstructure and the color tone of the film mostly. In order to study the interface region, surface analysis by AES combined with sputter depth profiling was performed. Microhardness of the coated TiN films were measured by micro Vickers hardness tester. Also, the effect of coating parameters on composition, coating surface and fracture morphology, grain size and growth rate were examined.

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Analysis of Biocompatible TiO2 Oxide Multilayer by the XPS Depth Profiling

  • Jang, Jae-Myung;Choe, Han-Cheol
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2017년도 춘계학술대회 논문집
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    • pp.156-156
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    • 2017
  • In this work, analysis of biocompatible TiO2 oxide multilayer by the XPS depth profiling was researched. the manufacture of the TiO2 barrier-type multilayer was accurately performed in a mixed electrolyte containing HAp, Pd, and Ag nanoparticles. The temperature of the solution was kept at approximatively $32^{\circ}C$ and was regularly rotated by a magnetic stirring rod in order to increase the ionic diffusion rate. The manufactured specimens were carefully analyzed by XPS depth profile to investigate the result of chemical bonding behaviors. From the analysis of chemical states of the TiO2 oxide multilayer using XPS, the peaks are showed with the typical signal of Ti oxide at 459.1 eV and 464.8 eV, due to Ti 2p(3/2) and Ti 2p(1/2), respectively. The Pd-3d peak was split into Pd-3d(5/2) and Pd-3d(3/2)peaks, and shows two bands at 334.7 and 339.9 eV for Pd-3d3 and Pd-3d5, respectively. Also, the peaks of Ag-3d have been investigated. The chemical states consisted of the O-1s, P-2p, and Ti-2p were identified in the forms of PO42- and PO43-. Based on the results of the chemical states, the chemical elements into the TiO2 oxide multilayer were also inferred to be penetrated from the electrolyte during anodic process.The structure characterization of the modified surface were performed by using FE-SEM, and from the result of biological evaluation in simulated body fluid(SBF), the biocompatibility of TiO2 oxide multilayer was effective for bioactive property.

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공개정보 기반 타임라인 프로파일링을 위한 확장된 워크플로우 개발 (Expanded Workflow Development for OSINT(Open Source Intelligence)-based Profiling with Timeline)

  • 권희원;진세영;심민선;권혜민;이인수;이승훈;김명주
    • 디지털융복합연구
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    • 제19권3호
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    • pp.187-194
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    • 2021
  • 다양한 형태로 표면 웹에 급증하고 있는 공개정보(OSINT)는 프로파일링 기법을 사용하여 범죄 수사에도 활용할 수 있다. 이러한 기술은 미국 등 외국의 수사기관에서는 상당히 보편화되었으며 일부는 고도화 작업도 진행하고 있다. 반면에 국내의 경우 많이 사용하지 못할 뿐 아니라 수사 인력의 개인적 경험과 지식수준에 따라 획득하는 정보의 양과 질에 있어서 큰 편차를 보이고 있다. 본 논문에서는 가장 잘 알려진 Bazzell의 모델과 달리 한국적 웹 환경을 고려하고 시간 정보까지 제공해주는 한국형 공개정보 기반 프로파일링 기법을 개선된 워크플로우를 중심으로 제시한다. 아울러 프로파일링의 효율성 향상을 목적으로 설계한 검색 데이터베이스의 스키마도 제시한다. 이곳에서 제시한 기법을 사용하면 범죄 수사에서 있어서 일정 수준의 양과 질을 보장하는 검색 결과를 얻을 수 있을 뿐 아니라, 관련 수사 인력에 대한 표준 훈련 과정으로도 사용할 수 있다. 아울러 이 기법을 활용한 범죄 수사의 실효성과 효율성을 높이려면 법률적 기반강화 및 동화된 기술 도입이 더 필요하다.