• Title/Summary/Keyword: Surface Profiling

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A Study on the Potassium Gettering in Al-1%Si/SiO2/PSG Multilevel Thin Films (Al-1%Si/SiO2/PSG 적층 박막에서 potassium 게터링에 관한 연구)

  • Kim, Jin Young
    • Journal of the Korean institute of surface engineering
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    • v.48 no.5
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    • pp.233-237
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    • 2015
  • In order to investigate the potassium (K) gettering, Al-1%Si/$SiO_2$/PSG multilevel thin films were fabricated. Al-1%Si thin films and $SiO_2$/PSG passivations were deposited by using DC magnetron sputter techniques and APCVD (atmosphere pressure chemical vapor deposition), respectively. Heat treatment was carried out at $300^{\circ}C$ for 5 h in air. SIMS (secondary ion mass spectrometry) depth profiling analysis was used to determine the distribution of K, Al, Si, P, and other elements throughout the $SiO_2$/PSG passivated Al-1%Si thin film interconnections. Potassium peaks were observed throughout the $SiO_2$/PSG passivation layers, and especially the interface gettering at the $SiO_2$/PSG and at the Al-1%Si/$SiO_2$ interfaces was observed. Potassium gettering in Al-1%Si/$SiO_2$/PSG multilevel thin films is considered to be caused by a segregation type of gettering.

Permeability imaging in granitic rocks based on surface resistivity profiling

  • Sudo Hiroshi;Tanaka Toshikazu;Kobayashi Tsuyoshi;Kondo Tatsutoshi;Takahashi Toru;Miyamoto Masaharu;Amagai Mitsuru
    • Geophysics and Geophysical Exploration
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    • v.7 no.1
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    • pp.56-61
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    • 2004
  • In order to image the distribution of permeability in granitic rocks, we carried out two-dimensional (2D) resistivity profiling, together with in-situ permeability tests, electrical logging of boreholes, and resistivity measurements of rock core samples in a laboratory. Based on the electrical logging and in-situ permeability data from boreholes, we obtained empirical equations which relate resistivity and permeability of the granitic rocks in the area studied. We then applied the empirical equation to a 2D resistivity section, to produce a 2D permeability section of the granitic rocks. In this paper, we present details of the field data and of the procedure for conversion from the resistivity section to a permeability section. The observed relationship between resistivity and permeability of the rocks is also discussed.

Short-Array Beamforming Technique for the Investigation of Shear-Wave Velocity at Large Rockfill Dams (대형 사력댐에서의 전단파속도 평가를 위한 단측선 빔형성기법)

  • Joh, Sung-Ho;Norfarah, Nadia Ismail
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.33 no.1
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    • pp.207-218
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    • 2013
  • One of the input parameters in the evaluation of seismic performance of rockfill dams is shear-wave velocity of rock debris and clay core. Reliable evaluation of shear-wave velocity by surface-wave methods requires overcoming the problems of rock-debris discontinuity, material inhomogeneity and sloping boundary. In this paper, for the shear-wave velocity investigation of rockfill dams, SBF (Short-Array Beamforming) technique was proposed using the principles of conventional beamforming technique and adopted to solve limitations of the conventional surface-wave techniques. SBF technique utilizes a 3- to 9-m long measurement array and a far-field source, which allowed the technique to eliminate problems of near-field effects and investigate local anomalies. This paper describes the procedure to investigate shear-wave velocity profile of rockfill dams by SBF technique and IRF (Impulse-response filtration) technique with accuracy and reliability. Validity of the proposed SBF technique was verified by comparisons with downhole tests and CapSASW (Common-Array-Profiling Spectral-Analysis-of-Surface-Waves) tests at a railroad embankment compacted with rock debris.

GENE-EXPRESSION PROFILING OF TITANIUM-CELL INTERACTION

  • Kim, Chang-Su;Hwang, Jung-Won;Ryu, Jae-Jun;Shin, Sang-Wan;Sohn, Sung-Hwa;Kim, Ki-Nam;Kim, Meyoung-Kon
    • The Journal of Korean Academy of Prosthodontics
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    • v.43 no.3
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    • pp.393-408
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    • 2005
  • Statement of problem. In the process of bone formation, titanium (Ti) surface roughness is an important factor modulating osteoblastic function. Purpose. This study was carried out to determine the effect of different Ti surface on biologic responses of a human osteoblast-like cell line (MG63). Materials and methods. MG63 cells were cultured on S (smooth), SLA (sandblasted largegrit & acid etching), HA (hydroxyapatite) Ti. The morphology and attachment of the cells were examined by SEM. The cDNAs prepared from total RNAs of MG63 were hybridized to a human cDNA microarray (1,152 elements). Results. The appearances of the surfaces observed with SEM were different in the three types of dental substrates. The surface of SLA and HA were shown to be rougher than S. MG63 cells cultured on SLA and HA were cell-matrix interaction. In the expression of genes involved in osseointegration, upregulated genes were bone morphogenetic protein, Villin, Integrin, Insulin-like growth factors in different surfaces. Downregulated genes were fibroblast growth factor receptor 4, Bcl 2-related protein, collagen, CD4 in different surfaces. Conclusion. The attachment and expression of key osteogenic regulatory genes were enhanced by surface roughness of the dental materials.

Investigation of Nanostructures in Homopolymer and Copolymer Films by Surface Techniques

  • Kang, Minhwa;Lee, Jihye;Lee, Yeonhee
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.276-276
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    • 2013
  • Time-Of-Flight Secondary Ion Mass Spectrometry (TOF-SIMS) and Atomic Force Microscopy (AFM) are the useful instruments to measure nanostructures of material surfaces. Surface pattern formation in blending homopolymer and diblock copolymer films was investigated as a function of film thickness and annealing conditions. In this study, surface structures of blending homopolymer [deuterated polystyrene (Mn 20,000), poly (methyl methacrylate) (Mn 18,000)] and diblock copolymer [Poly (deuteratedstyrene(d8)-b-methyl methacrylate) (Mn 19,500-18,100)] films were observed. The AFM result indicated that the nanostructures and film thickness depended on temperature, concentration and solvent. TOF-SIMS depth profiling was obtained for the lamellar morphology of symmetric dPS-b-PMMA which is found to orient parallel to the surface of the substrate. Elemental and molecular depth profiles measured in the negative ion mode by a Cs+ primary ion beam demonstrate variations in hydrogen, deuterium, carbon, oxygen, hydrocarbons and deuterated hydrocarbons within the diblock copolymer according to the depth.

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Roughness Measurement Performance Obtained with Optical Interferometry and Stylus Method

  • Rhee Hyug-Gyo;Lee Yun-Woo;Lee In-Won;Vorburger Theodore V.
    • Journal of the Optical Society of Korea
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    • v.10 no.1
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    • pp.48-54
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    • 2006
  • White-light scanning interferometry (WLI) and phase shifting interferometry (PSI) are increasingly used for surface topography measurements, particularly for areal measurements. In this paper, we compare surface profiling results obtained from above two optical methods with those obtained from stylus instruments. For moderately rough surfaces ($Ra{\approx}500\;nm$), roughness measurements obtained with WLI and the stylus method seem to provide close agreement on the same roughness samples. For surface roughness measurements in the 50 nm to 300 nm range of Ra, discrepancies between WLI and the stylus method are observed. In some cases the discrepancy is as large as 109% of the value obtained with the stylus method. By contrast, the PSI results are in good agreement with those of the stylus technique.

Profiling of fine displacement of spherical surface using Fourier transform method (푸리에 변환 간섭 해석법을 이용한 구면의 미세 변위 측정)

  • 손영준;주신호;권진혁;최옥식
    • Korean Journal of Optics and Photonics
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    • v.8 no.3
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    • pp.199-203
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    • 1997
  • Fine displacement of spherical suface was detected and analyzed by Twyman-Green interferometer and the interferogram analysis using Fourier transform method. The surface profile was obtained from single interferogram by introducing the carrier freguency to the interferogram. The interferogram was processed in the spatial frequency domain by fast Fourier transform, and the phase distribution was obtained by inverse Fourier transform. The 3-dimensional distribution for the surface displacement was obtained. It was compared with the calculated surface displacement and the error was less than λ/10.

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TiN coatings by HCD plasma enhanced reactive ion plating method (HCD플라즈마를 이용한 반응성 이온플레이팅법에 의한 TiN 코팅)

  • 서용운;황기웅
    • Journal of the Korean institute of surface engineering
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    • v.25 no.3
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    • pp.133-143
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    • 1992
  • Titanium nitride(TiN) films have been prepared by HCD plasma enhanced reactive ion plating. Density and temperature of the plasma generated by the HCD were investigated. It was shown that parameters such as the substrate bias voltage(0 350V) and N2 flow rate(10 180SCCM) influenced the growth, the growth, the microstructure and the color tone of the film mostly. In order to study the interface region, surface analysis by AES combined with sputter depth profiling was performed. Microhardness of the coated TiN films were measured by micro Vickers hardness tester. Also, the effect of coating parameters on composition, coating surface and fracture morphology, grain size and growth rate were examined.

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Analysis of Biocompatible TiO2 Oxide Multilayer by the XPS Depth Profiling

  • Jang, Jae-Myung;Choe, Han-Cheol
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2017.05a
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    • pp.156-156
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    • 2017
  • In this work, analysis of biocompatible TiO2 oxide multilayer by the XPS depth profiling was researched. the manufacture of the TiO2 barrier-type multilayer was accurately performed in a mixed electrolyte containing HAp, Pd, and Ag nanoparticles. The temperature of the solution was kept at approximatively $32^{\circ}C$ and was regularly rotated by a magnetic stirring rod in order to increase the ionic diffusion rate. The manufactured specimens were carefully analyzed by XPS depth profile to investigate the result of chemical bonding behaviors. From the analysis of chemical states of the TiO2 oxide multilayer using XPS, the peaks are showed with the typical signal of Ti oxide at 459.1 eV and 464.8 eV, due to Ti 2p(3/2) and Ti 2p(1/2), respectively. The Pd-3d peak was split into Pd-3d(5/2) and Pd-3d(3/2)peaks, and shows two bands at 334.7 and 339.9 eV for Pd-3d3 and Pd-3d5, respectively. Also, the peaks of Ag-3d have been investigated. The chemical states consisted of the O-1s, P-2p, and Ti-2p were identified in the forms of PO42- and PO43-. Based on the results of the chemical states, the chemical elements into the TiO2 oxide multilayer were also inferred to be penetrated from the electrolyte during anodic process.The structure characterization of the modified surface were performed by using FE-SEM, and from the result of biological evaluation in simulated body fluid(SBF), the biocompatibility of TiO2 oxide multilayer was effective for bioactive property.

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Expanded Workflow Development for OSINT(Open Source Intelligence)-based Profiling with Timeline (공개정보 기반 타임라인 프로파일링을 위한 확장된 워크플로우 개발)

  • Kwon, Heewon;Jin, Seoyoung;Sim, Minsun;Kwon, Hyemin;Lee, Insoo;Lee, Seunghoon;Kim, Myuhngjoo
    • Journal of Digital Convergence
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    • v.19 no.3
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    • pp.187-194
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    • 2021
  • OSINT(Open Source Intelligence), rapidly increasing on the surface web in various forms, can also be used for criminal investigations by using profiling. This technique has become quite common in foreign investigative agencies such as the United States. On the other hand, in Korea, it is not used a lot, and there is a large deviation in the quantity and quality of information acquired according to the experience and knowledge level of investigator. Unlike Bazzell's most well-known model, we designed a Korean-style OSINT-based profiling technique that considers the Korean web environment and provides timeline information, focusing on the improved workflow. The database schema to improve the efficiency of profiling is also presented. Using this, we can obtain search results that guarantee a certain level of quantity and quality. And it can also be used as a standard training course. To increase the effectiveness and efficiency of criminal investigations using this technique, it is necessary to strengthen the legal basis and to introduce automation technologies.