• Title/Summary/Keyword: Surface Adhesion

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EFFECT OF ION BEAM ASSISTED CLEANING ON ADHESION OF ALUMINIUM TO POLYMER SUBSTRATE OF PC AND PMMA

  • Kwon, Sik-Chol;Lee, Gun-Hwan;Lee, Chuel-Yong;Gob, Han-Bum;Lim, Jun-Seop;Goh, Sung-Jin
    • Journal of the Korean institute of surface engineering
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    • v.32 no.3
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    • pp.428-432
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    • 1999
  • As metallic surface has its unique lustrous appearance and optical reflectance in visible range of light, the metallization of plastic surface has been an essential drive toward weight reduction for fuel economy and decorations in transportation industry and has been put into practiced from wet chemical-electrochemial to dry vacuum process in view of an environmental effect. Electron-beam metallization was used in this work with an aim at improving the scratchproof surface hardness of plastic substrate with metallic finish character. Thin film of Al ($1000\AA$) and $SiO_2$($7000\AA$) were metallized on substrate of PC and PMMA and the films were evaluated by pencil test for surface hardness and by cross-cut tape test for adhesion. The ion beam treatment improved around twice as hard as non-treat surface. The ion beam is effect on its hardness and adhesion to surface hardened PC substrate.

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Adhesion Strength Measurement of Rabbit Knee Chondrocyte (연골세포 부착력 평가)

  • Lee Kwon-Yong;Park Sang-Guk;Shin Daehwan;Park Jong-Chul
    • Tribology and Lubricants
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    • v.21 no.5
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    • pp.236-240
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    • 2005
  • In order to prepare for the suitable surfaces of implants or medical devices, quantitative evaluation of adhesion between cells and biomaterials is essential. To better understand adhesion formation between cells and biomaterials, we used the cytodetachment technique which measures the adhesive force of a single cell through changing the, culture time and detachment speed. The results showed that the adhesive force could be affected by the culture time of cells on the surface of materials and the detachment speed. Moreover, there was a large discrepancy among the adhesion strength measured by similar techniques conducted on the different cells and substrates. It can be 'concluded that the variation of the force measurement technique can seriously alter the level of the force required to detach a cell on the surface of materials.

Study on Properties of Self-Assembled Monolayer as Anti-adhesion Layer on Metallic Nano Stamper (금속 나노 스탬퍼 점착방지막으로서의 자기조립 단분자막 특성 연구)

  • 최성우;강신일
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.10a
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    • pp.367-370
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    • 2003
  • In this study, application of SAM (self-assembled monolayer) to nano replication process as an anti-adhesion layer was presented to reduce the surface energy between the nano mold and the replicated polymeric nano patterns. The electron beam lithography was used for master nano patterns and the electorforming process was used to fabricate the nickel nano stamper. Alkanethiol SAM as an anti-adhesion layer was deposited on metallic nano stamper using solution deposition method. To analyze wettability and adhesion force of SAM, contact angle and LFM (Lateral Force Microscopy) were measured at the actual processing temperature and pressure for the case of nano compression molding and at the actual UV dose for the case of nano UV molding. It was found that the surface energy due to SAM deposition on the nickel nano stamper markedly decreased and the quality of SAM on the nickel stamper maintained under the actual molding environments.

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The effect of deposition conditions on the adhesion strength of TiN multilayer by D. C. magnetron sputtering (D. C. 마그네트론 스퍼터링에 의한 증착조건이 TiN다층박막의 밀착력에 미치는 영향)

  • 김선규;유정광;이건환;권식철
    • Journal of the Korean institute of surface engineering
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    • v.29 no.4
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    • pp.261-267
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    • 1996
  • The characteristics and adhesion strength of TiN layer deposited by D. C. magnetron sputtering were investigated. Three types of TiN layers were deposited on STS304 stainless steel. Scratch tests were performed to determine the effect of deposition temperature, the thickness of coated TiN layer and the titanium inter-layer on the adhesion strength. TiN multilayer with titanium inter-layer showed the highest critical load in the deposition temperature range of $25^{\circ}C$ to $300^{\circ}C$. Adhesion strength of TiN multilayer with titanium inter-layer was raised from 15N to 20N by raising deposition temperature from $25^{\circ}C$ to $400^{\circ}C$. Adhesion strength was raised from 18N to 38N by increasing the thickness of outer layer of TiN multilayer from 2.1 $\mu\textrm{m}$ to 9.5 $\mu\textrm{m}$.

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Effect on the Adhesion of Ice Slurry by the Characteristic of Cooling Surface (냉각면 성상이 빙부착에 미치는 영향)

  • Seung Hyun;Hong Hi Ki;Kang Chae Dong
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.17 no.2
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    • pp.183-190
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    • 2005
  • In the process of ice-slurry making, ice adhesion on cooling wall or in narrow flow Path disturbs continuous ice formation. In this study, the effect on the ice adhesion to cooling surface by some freezing experiments was investigated, quantitatively. Three types of solutions were frozen in various coating vessels with stirring. In the experiment, the ice adhesion between cooling wall and Ice-slurry was evaluated by measuring stirring power. From the result, the stirring power of slurry mixture in PTFE-coating vessel was smaller than those in PE-coating, PFA-coating and bare SUS vessel. Especially, in EG H PG 1.S/ HD 1.5 mass$\%$ solution, the stirring power in the PE-coating vessel was smaller than that in the PFA-coating or SUS vessel.

Adhesion improvement of electroless plated Ni layer by modifying zincating process (징케이트 공정 변화에 따른 무전해 니켈 도금 막의 접착력향상)

  • 이성기;진정기;김영호
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2002.05a
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    • pp.109-114
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    • 2002
  • The adhesion of electroless plated Ni layer on Al/Si substrates has been investigated. The zincating treatment was conducted with a conventional method and a modified method. In a modified method, ultrasonic agitation was applied during zincating. Adhesion strength was evaluated by a pull-off test. The ultrasonic agitation during zincating increased the nucleation density of Zn particles and refined Zn particle size. the adhesion strength of electroless Ni layer deposited on the modified zincated surface was higher than that on the conventionally zincated surface. the improvement of adhesion was attributed to the fine and dense Zn particles.

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The Effects of Stabilizers on Adhesion of Electroless Copper Deposits on Alumina (Alumina 소지상의 무전해 동도금층의 밀착력에 미치는 안정제의 영향)

  • 최순돈;이희록
    • Journal of the Korean institute of surface engineering
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    • v.29 no.2
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    • pp.109-119
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    • 1996
  • In order to improve adhesion of electroless copper deposits on alumina substrates, some stabilizers such as 2-Mercapto Benzothiazole, thiourea and NaCN were added over a wide range of concentrations. The adhesion tests of the deposits were performed by using the cellophane tape and the push-pull scale. With the minor addition of the stabilizers, 2-MBT having a large molecular size gives poor adhesion, together with a finer grain structure, whereas Thiourea and NaCN show a high mechanical strength of the deposits. The high mechanical strength is supposed to be due to the easy desorption of hydrogen gas generated from the electroless reactions. A large amount of the three stabilizers decreases the adhesion for all the cases, resulting from strong adsorption of the stabilizers to the substrates.

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Effect of Substrate Roughness on the Adhesion of TiN Deposition by PACVD (플라즈마 화학증착법에 있어 모재의 표면조도가 TiN 박막층의 밀착력에 미치는 영향에 관하여)

  • Kang, H.Y.;Kim, M.I.
    • Journal of the Korean Society for Heat Treatment
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    • v.4 no.2
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    • pp.27-37
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    • 1991
  • The adhesion strength of TiN films to substrate(STC 3) steel has been studied using the scratch adhesion test. Before deposition, the substrates were mechanically polished and TiN films were deposited at different substrate temperature($480^{\circ}C-540^{\circ}C$). The chemical properties of TiN films were investigated by RBS, and EDS, and the physical properties were investigated by micro-hardness tester, SEM, and X-ray diffractometer. According to results of this study, the adhesion strength of TiN films increase with increasing the deposition temperature. The roughness of the polished substrates surface were measured with a profilometer. It was observed that, as a general rule, the adhesion strength of deposited TiN films increase with decreasing the substrates surface roughness.

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Evaluating the Tensile Adhesion Strength of Methyl Methacrylate (MMA) Based Road Repair Materials (Methyl Methacrylate(MMA)계 도로보수재의 인장 접착 강도 평가)

  • Ji, Sung-jun;Kim, Gyu-yong;Pyeon, Su-jeong;Choi, Byung-cheol;Park, Jun-young;Nam, Jeong-soo
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2023.11a
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    • pp.107-108
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    • 2023
  • In this study, the tensile adhesion strength was evaluated according to KS F 4932 to assess the suitability of MMA-based repair materials for concrete roads. Two types of MMA were used. Mortar mock-ups were made and tested for adhesion strength in three different surface conditions: air, water, and salt water. Both showed strengths above the standardized strength of 0.6 MPa. Type B, which has a relatively low adhesion strength, is considered more suitable.

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Evaluation of C. Albicans and S. Mutans adherence on different provisional crown materials

  • Ozel, Gulsum Sayin;Guneser, Mehmet Burak;Inan, Ozgur;Eldeniz, Ayce Unverdi
    • The Journal of Advanced Prosthodontics
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    • v.9 no.5
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    • pp.335-340
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    • 2017
  • PURPOSE. Bacterial adhesion on provisional crown materials retained for a long time can influence the duration for which permanent prosthetic restorations can be healthily worn in the oral cavity. The aim of this study was to compare seven different commonly used provisional crown materials with regard to Streptococcus mutans and Candida albicans surface adhesion. MATERIALS AND METHODS. For each group, twenty specimens of the provisional fixed prosthodontic materials TemDent ($Sch{\ddot{u}}tz$), Imident (Imicryl), Tab 2000 (Kerr), Structur Premium (Voco), Systemp (Ivoclar Vivadent), Acrytemp (Zhermack), and Takilon-BBF (Takilon) were prepared (diameter, 10.0 mm; height, 2.0 mm). Surface roughness was assessed by atomic force microscopy. Each group was then divided into 2 subgroups (n=10) according to the microbial suspensions used: S. mutans and C. albicans. The specimens were incubated at $37^{\circ}C$ with S. mutans or C. albicans for seven days. Bacterial adherence on surfaces was assessed using the 2,3-bis[2-methyloxy-4-nitro-5-sulfophenyl]-2H-tetrazolium-5-carboxanilide (XTT) assay. RESULTS. S. mutans showed maximum adhesion to Structur, followed by Systemp, Acrytemp, Takilon, Tab 2000, Imident, and TemDent (P<.05). The highest vital C. albicans adhesion was noted on Takilon, followed by Imident and Tab 2000; the lowest adhesion was noted on Systemp (P<.05). CONCLUSION. The materials showed significant differences in the degree of bacterial adhesion. C. albicans showed higher surface adhesion than S. mutans on provisional crown and fixed partial denture denture materials.