• Applied Microscopy
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• v.45 no.4
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• pp.214-217
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• 2015

This study introduces metal coating as an effective sample preparation method to remove charge-up caused by the shadow effect during field emission scanning electron microscope (FE-SEM) analysis of dynamic structured samples. During a FE-SEM analysis, charge-up occurs when the primary electrons (input electrons) that scan the specimens are not equal to the output electrons (secondary electrons, backscattered electrons, auger electrons, etc.) generated from the specimens. To remove charge-up, a metal layer of Pt, Au or Pd is applied on the surface of the sample. However, in some cases, charge-up still occurs due to the shadow effect. This study developed a coating method that effectively removes charge-up. By creating a converted sample stage capable of simultaneous tilt and rotation, the shadow effect was successfully removed, and image data without charge-up were obtained.

• Smart Structures and Systems
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• v.16 no.5
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• pp.853-872
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• 2015

Numerical analysis of large amplitude free vibration behaviour of laminated composite spherical shell panel embedded with the piezoelectric layer is presented in this article. For the investigation purpose, a general nonlinear mathematical model has been developed using higher order shear deformation mid-plane kinematics and Green-Lagrange nonlinearity. In addition, all the nonlinear higher order terms are included in the present mathematical model to achieve any general case. The nonlinear governing equation of freely vibrated shell panel is obtained using Hamilton's principle and discretised using isoparametric finite element steps. The desired nonlinear solutions are computed numerically through a direct iterative method. The validity of present nonlinear model has been checked by comparing the responses to those available published literature. In order to examine the efficacy and applicability of the present developed model, few numerical examples are solved for different geometrical parameters (fibre orientation, thickness ratio, aspect ratio, curvature ratio, support conditions and amplitude ratio) with and/or without piezo embedded layers and discussed in details.

• Transactions of the Korean Society of Mechanical Engineers
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• v.18 no.3
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• pp.701-706
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• 1994

The discharge coefficients of critical sonic nozzles were obtained in a high pressure gas flow standard system, which was a gravitational weighing system. The discharge coefficients of critical sonic nozzle farbricated according to ISO specifications are in good agreement with ISO correlation. The discharge coefficients for small inlet radius decrease significantly as the inlet length become short due3 to separation at the sharp-edged inlet. For nozzles having long inlet radius, the effects of inlet length on the discharge coefficients were relatively small, but the effects become significant at the short inlet length. The effect of separation at the sharp-edged inlet is stronger than that of the boundary layer growth. The experimental results support that the shape of critical sonic nozzles suggested by ISO specifications is excellent.

• Applied Biological Chemistry
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• v.15 no.1
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• pp.1-6
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• 1972

The naturally occurring indole derivatives in mung bean (Phaseolus vidissinus) sprouts were investigated by means of paper and thin layer chromatographic techniques. The results can be summerized as follows: 1. The mung bean sprouts are richer in free tryptophan than other plant species. 2. Indole ethanol and indole lactic acid were identified. 3. The content of indole ethanol was more than that of indole acetic acid. This result appeared to support the idea that indole ethanol is the storage product of indole acetic acid.

• Journal of the Korean Ceramic Society
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• v.32 no.3
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• pp.349-358
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• 1995

The ceramic composite membrane was synthesized by thermal oxidation after evaporation of Al on the support prepared by slip casting process. Oxidation was performed at $700^{\circ}C$ and 80$0^{\circ}C$ under dry oxygen atmosphere. It was considered as optimum oxidation condition that the membrane showed a knudsen behaviro. A further oxidation resulted in an increase of gas permeability because top layer became densified. Then, a multi-layered composite membrane was synthesized through a sol-gel method, evaporation and thermal oxidation of Al coating processes. While the membrane was thermally stable up to 80$0^{\circ}C$, gas permeability was rapidly decreased even at a slight amount of deposition of Al.

• Particle and aerosol research
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• v.9 no.4
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• pp.209-219
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• 2013

We have used the modified diffusion flame burner to synthesize silica coated iron oxide nanoparticles having enhanced superparamagnetic property. Silica-encapsulated iron oxide particles were directly observed using a high resolution transmission electron microscope. From the energy dispersive X-ray spectroscopy (EDS) and zeta potential measurements, the iron oxide particles were found to be completely covered by a silica coating layer. X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD) measurements revealed that the iron oxide core consists of ${\gamma}-Fe_2O_3$ rather than ${\alpha}-Fe_2O_3$. Our magnetization measurements support this conclusion. Biocompatibility test of the silica-coated iron oxide nanoparticles is also conducted using the protein adsorption onto the coated particle.

• ETRI Journal
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• v.30 no.3
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• pp.441-450
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• 2008

The scalable extension of H.264, known as scalable video coding (SVC) has been the main focus of the Joint Video Team's work and was finalized at the end of 2007. Synchronization between media is an important aspect in the design of a scalable video streaming system. This paper proposes an efficient media synchronization mechanism for SVC video transport over IP networks. To support synchronization between video and audio bitstreams transported over IP networks, a real-time transport protocol/RTP control protocol (RTP/RTCP) suite is usually employed. To provide an efficient mechanism for media synchronization between SVC video and audio, we suggest an efficient RTP packetization mode for inter-layer synchronization within SVC video and propose a computationally efficient RTCP packet processing method for inter-media synchronization. By adopting the computationally simple RTCP packet processing, we do not need to process every RTCP sender report packet for inter-media synchronization. We demonstrate the effectiveness of the proposed mechanism by comparing its performance with that of the conventional method.

• Journal of applied mathematics & informatics
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• v.33 no.5_6
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• pp.485-502
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• 2015

A computational method for solving singularly perturbed boundary value problem of differential equation with shift arguments of mixed type is presented. When shift arguments are sufficiently small (o(ε)), most of the existing method in the literature used Taylor's expansion to approximate the shift term. This procedure may lead to a bad approximation when the delay argument is of O(ε). The main idea for this work is to deal with constant shift arguments, which are independent of ε. In the present method, we construct the formally asymptotic solution of the problem using the method of composite expansion. The reduced problem is solved numerically by using operator compact implicit method, and the second problem is solved analytically. Error estimate is derived by using the maximum norm. Numerical examples are provided to support the theoretical results and to show the efficiency of the proposed method.

• Journal of applied mathematics & informatics
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• v.34 no.5_6
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• pp.495-508
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• 2016

A singularly perturbed reaction-diffusion fourth-order ordinary differential equation(ODE) with discontinuous source term is considered. Due to the discontinuity, interior layers also exist. The considered problem is converted into a system of weakly coupled system of two second-order ODEs, one without parameter and another with parameter ε multiplying highest derivatives and suitable boundary conditions. In this paper a computational method for solving this system is presented. A zero-order asymptotic approximation expansion is applied in the second equation. Then, the resulting equation is solved by the numerical method which is constructed. This involves non-overlapping Schwarz method using Shishkin mesh. The computation shows quick convergence and results presented numerically support the theoretical results.

• Journal of the Korean Society for Precision Engineering
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• v.17 no.10
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• pp.41-48
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• 2000

Manufacturing devices must be integrated for constructing CIM environment, but integration of heterogeneous system meets several economical and technological difficulties. In this case, MMS(Manufacturing Message Specification) can be an effective method, but it has problems which MMS products are generally very expensive and majority of the existing manufacturing devices do not support MMS. This paper describes the development of a gateway for Non-MMS-Compatible CNC machine tools to serve MMS and the implementation of OSI(Open System Interconnection) upper layer on TCP/IP. The developed system is applied to construct cell controller with heterogeneous devices under CIM environment and to evaluate interoperability and portability.