• 대한기계학회논문집A
• /
• 제25권12호
• /
• pp.1933-1943
• /
• 2001

A micromechanical model is presented for superplasticity in which heterogeneous microstructures are coupled with deformation behavior. The effects of initial distributions of grain size, and their evolutions on the mechanical properties can be predicted by the model. Alternative stress rate models such as Jaumann rate and rotation incremental rate have been employed to analyze uniaxial loading and simple shear problems and the appropriate modeling was studied on the basis of hypoelasticity and elasto-viscoplasticity. The model has been implemented into finite element software so that full process simulation can be carried out. Tests have been conducted on Ti-6Al-4V alloy and the microstructural features such as grain size, distributions of grain size, and volume fraction of each phase were examined for the materials that were tested at different strain rates. The experimentally observed stress-strain behavior on a range of initial grain size distributions has been shown to be correctly predicted. In addition, the effect of volume fraction of the phases and concurrent grain growth were analyzed. The dependence of failure strain on strain rate has been explained in terms of the change in mechanism of grain growth that occurs with changing strain rate.

• 한국주조공학회지
• /
• 제21권6호
• /
• pp.359-365
• /
• 2001

The superplastic behavior of whisker reinforced aluminum alloy matrix composites fabricated by squeeze casting as one of high pressure routes was investigated. The preforms of ${\alpha}-Si_3N_4$ and ${\beta}-SiC$ whiskers without any binder as a reinforcement were used. The matrix materials were 2024 and 7075 aluminum alloys. For the purpose of optimum superplastic condition, respectively, the whiskers volume fraction, extrusion temperature, tensile test temperature and initial strain rate were changed. Fracture surface of tested specimens were observed by SEM. By the results, it became possible to produce superplastic composites by applying only a hot extrusion process to composites obtained by the squeeze casting. The superplastic composites developed are ${\alpha}-Si_3N_4w/7075$, ${\alpha}-Si_3N_4w/2024$ and ${\beta}-SiCw/2024$ systems at high strain rate.

• 소성∙가공
• /
• 제18권4호
• /
• pp.317-322
• /
• 2009

Superplastic deformation behavior of a Zn-0.3 wt.% Al was investigated. Grain sizes of $1{\mu}m$ and $10{\mu}m$ were obtained by a thermomechanical treatment. A series of load relaxation and tensile tests were conducted at various temperatures ranging from RT ($24^{\circ}C$) to $200^{\circ}C$. A large elongation of 1400% was obtained at room temperature in the specimens with the grain size of $1{\mu}m$. In the case of specimens with the grain size of $10{\mu}m$, relatively lower elongation at room temperature was obtained and, as the temperature increases above $100^{\circ}C$, a high elongation of about 400 % has been obtained at $200^{\circ}C$ under the strain rate of $2{\times}10^{-4}/s$. Dynamic materials model (DMM) has been employed to explain the contribution from GBS of Zn-Al alloy. Power dissipation efficiency for GBS was evaluated as above 0.4 and found to be very close to the unity as strain rate decreased and temperature increased, suggesting that GBS could be regarded as Newtonian viscous flow.

• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2003년도 추계학술대회
• /
• pp.1145-1150
• /
• 2003

Zr-based bulk metallic glasses have a significant mechanical properties such as high strength and elastic strain limit, and a good processing ability due to the deformation behavior such as superplasticity under supercooled liquid region. Recently, many researches on the determination of optimum working condition in various bulk metallic glasses have been carried out. In this study, the deformation behavior and forming conditions of $Zr_{55}Cu_{30}Al_{10}Ni_{5}$ bulk metallic glass were investigated under three different strain rates and at various temperatures between 627K and 727K. The glass transition temperature, crystallization temperature and supercooled liquid region of $Zr_{55}Cu_{30}Al_{10}Ni_{5}$ bulk metallic glass are 680K, 762K and 82K, respectively.

• 소성∙가공
• /
• 제11권5호
• /
• pp.447-456
• /
• 2002

A study has been made to investigate the boundary sliding and its accommodation mode with respect to the variation of $\alpha$$_2$/$eta$ volume fraction during superplastic deformation of two-phase Ti$_3$Al-xNb intermetallics. Step strain rate and load relaxation tests have been performed at 950, 970 and 99$0^{\circ}C$ to obtain the flow stress curves and to analyze the deformation characteristics by the theory of inelastic deformation. The results show that the grain matrix deformation and boundary sliding of the three intermetallics containing 21, 50 and 77% in $eta$ volume fractions are well described by the plastic deformation and viscous flow equations. Due to the equal accommodation of both $a^2$ and $\beta$ phases, the accommodation modes for fine-grained materials are in good agreement with the iso-strain rate models. The sliding resistance analyzed for the different boundaries is the lowest in the $\alpha$$_2$/$\alpha$$_2$ boundary, and increases in the order of $\alpha$$_2$/$\alpha$$_2$<< $\alpha$$_2$/$\beta$ = $\beta$/$\beta$, which plays an important role in controlling the superplasticity of the alloys with the various $\alpha$$_2$/$\beta$ phase ratio.

• 한국주조공학회지
• /
• 제17권3호
• /
• pp.252-257
• /
• 1997

The 8 mm dia: Sn-38%Pb eutectic alloy rods were produced by use of the horizontal continuous casting process with the heated mold and chill cast process. The cast rods were rolled into 2.0${\sim}$0.5 mm thick plates and structural and mechanical properties were examined. The results revealed that the plates produced by the continuous casting process with the heated mold show much higher superplasticity at ambient temperature (1550% elongation at 0.5mm thick plate and 0.5mm/min strain rate) than the plates procuced by chill cast process (630% elongation). Such a high superplasticity of the continuous cast plates is due to the high-quality plates free from any inside and surface defects with fine and uniform distribution of eutectic phases.

• 열처리공학회지
• /
• 제35권4호
• /
• pp.211-219
• /
• 2022

It is known that superplastic materials with ultrafine grains have high elongation mainly due to grain boundary sliding. Therefore, in the present study we examined the influence of grain refinement, caused by a repetitive cold rolling and annealing process, on both superplastic elongation and superplastic deformation mechanism. The cold rolling and annealing process was repetitively applied up to 4 times using Fe-10Mn-3.5Si alloy. High-temperature tensile tests were conducted at 763 K with an initial strain rate of 1 × 10^-3 s^-1 using the specimens. The superplastic elongation increased with the number of the repetitive cold rolling and annealing process; in particular, the 4 cycled specimen exhibited the highest elongation of 372%. The primary deformation mechanism of all specimens was grain boundary sliding between recrystallized α-ferrite and reverted γ-austenite grains. The main reason for the increase in elongation with the number of the repetitive cold rolling and annealing process was the increase in fractions of fine recrystallized α-ferrite and reverted γ-austenite grains, which undergo grain boundary sliding.

• 한국재료학회지
• /
• 제30권6호
• /
• pp.301-307
• /
• 2020

In this study, factors considered to be causes of promotion of densification of sintered pellets identified during phase change are reviewed. As a result, conclusions shown below are obtained for each factor. In order for MA powder to soften, a temperature of 1,000 K or higher is required. In order to confirm the temporary increase in density throughout the sintered pellet, the temperature rise due to heat during phase change was found not to have a significant effect. While examining the thermal expansion using the compressed powder, which stopped densification at a temperature below the MA powder itself, and the phase change temperature, no shrinkage phenomenon contributing to the promotion of densification is observed. The two types of powder made of Ti-silicide through heat treatment are densified only in the high temperature region of 1,000 K or more; it can be estimated that this is the effect of fine grain superplasticity. In the densification of the amorphous powder, the dependence of sintering pressure and the rate of temperature increase are shown. It is thought that the specific densification behavior identified during the phase change of the Ti-37.5 mol.%Si composition MA powder reviewed in this study is the result of the acceleration of the powder deformation by the phase change from non-equilibrium phase to equilibrium phase.

• 한국재료학회지
• /
• 제28권8호
• /
• pp.435-439
• /
• 2018

MA Al alloys are examined to determine the effects of alloying of Mg and Cu and rolling on tensile deformation behavior at 748 K over a wide strain rate range($10^{-4}-10^3/s$). A powder metallurgy aluminum alloy produced from mechanically alloyed pure Al powder exhibits only a small elongation-to-failure(${\varepsilon}_f$ < ~50%) in high temperature(748 K) tensile deformation at high strain rates(${\acute{\varepsilon}}=1-10^2/s$). ${\varepsilon}_f$ in MA Al-0.5~4.0Mg alloys increases slightly with Mg content(${\varepsilon}_f={\sim}140%$ at 4 mass%). Combined addition of Mg and Cu(MA Al-1.5%Mg-4.0%Cu) is very effective for the occurrence of superplasticity(${\varepsilon}_f$ > 500%). Warm-rolling(at 393-492 K) tends to raise ${\varepsilon}_f$. Lowering the rolling-temperature is effective for increasing the ductility. The effect is rather weak in MA pure Al and MA Al-Mg alloys, but much larger in the MA Al-1.5%Mg-4.0%Cu alloy. Additions of Mg and Cu and warm-rolling of the alloy cause a remarkable reduction in the logarithm of the peak flow stress at low strain rates (${\acute{\varepsilon}}$< ~1/s) and sharpening of microstructure and smoothening of grain boundaries. Additions of Mg and Cu make the strain rate sensitivity(the m value) larger at high strain rates, and the warm-rolling may make the grain boundary sliding easier with less cavitation. Grain boundary facets are observed on the fracture surface when ${\varepsilon}_f$ is large, indicating the operation of grain boundary sliding to a large extent during superplastic deformation.

• 한국재료학회지
• /
• 제11권7호
• /
• pp.585-589
• /
• 2001

많은 연구결과들은 국부적 용융체의 존재가 고온인장 변형 시 발생하는 내부공극의 발달을 억제할 수 있음을 보고하고 있다. 그러나 이러한 국부적 용융체가 존재한다고 해서 반드시 고변형속도 초소성 현상이 관찰될 수 있는 것은 아니다. 금속기지와 보강재간의 계면에 국부적 용융체의 양이 너무 많이 존재하면 두상간의 결합력이 떨어져 금속기지상으로부터 보강재가 분리되는 현상이 야기될 수 있기 때문이다. 그러므로, $Si_3$$N_{4p}$ 2124 Al 복합재의 초소성 유동 특성을 이해하기 위해 변형온도에 따른 미세구조 변화와 계면특성을 조사하였다. 본 연구를 룽해 $Si_3$$N_{4p}$ 2124 Al 복합재에서 Al-기지와 $Si_3$$N_{4p}$ 강화상간의 계면상의 국부적 용융이 시작되는 온도부근에서는 큰 초소성 특성이 얻어지지만, 국부적 용융이 시작되는 온도를 지난 인장온도범위에서는 오히려 초소성 특성이 현저하게 저하되는 현상이 관찰되었다. 위의 실험결과는 $Si_3$$N_{4p}$ 2124 Al복합재의 고변형속도 초소성 거동에 기여하는 최적의 액상량이 존재한다는 것을 의미한다.