• 대한화학회지
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• 제23권4호
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• pp.217-236
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• 1979

소성변형에 대한 著者들의 이론을 초소성합금(Zn-Al eutectoid, A1-Cu, Pb-Sn, Sn-Bi, Mg-Al eutectics)에 적용하였다. 그 결과 초소성합금의 소성변형은 두 개의 grain boundary流動單位의 平行連結로 나타낼 수 있었다. 이 두 개의 流動單位는 流動式에 나타나는 parameter $X_{gj}/{\alpha}_{gj}$와 ${\beta}_{gj}$(j=1 혹온 2)로 表現할 수 있으며 이들을 實驗的으로 求할 수 있었다. 著者들의 流動式은 實驗과 잘 一致하였다. Strain rate sensitivity 對 -In(strain rate) 곡선을 이론으로 구한 결과 유동단위수만큼의 peak가 ${\beta}_{gj}$(j=1 or 2) 값에 따라 분리되어 나타났고 초소성의 조건도 ${beta}_{gj}$값에 의하여 결정됨을 알았다. ${\beta}_{gj}값의 粒子크기 依存性을 구하였고 온도변화에 따른 ${\beta}_{gj}$값 변화로부터 각 流動單位의 활성화엔탈피, ${\Delta}H_{gj}^{\neq}$도 구하였다. 그 결과 ${\Delta}H_{gj}^{\neq}$는 재료성분원소들의 grain boundary 자체확산에 의한 활성화엔탈피와 같이 나타났고 또 이들은 粒子 크기 증가에 마라 증가함을 보였다

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2009년도 추계학술대회 논문집
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• pp.387-390
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• 2009

This study was designed to fabricate the micro-electro-mechanical systems (MEMS) parts such as micro spur gears using hot extrusion of gas atomized Al-78Zn powders. For this purpose, it is important to develop new methods to fabricate micro-dies and choose suitable extrusion conditions for a micro-forming. Micro-dies with Ni were fabricated by LIGA technology. LIGA technology was capable to produce micro-extrusion dies with close tolerances, thick bearing length and adequate surface quality. Superplastic Al-78Zn powders have the great advantage in achieving deformation under low stresses and exhibiting good micro formability with average strain rates ranging from $10^{-3}$ to $10^{-2}\;s^{-1}$ and constant temperatures ranging from 503 to 563K. Al-78Zn powders were compacted into a cylindrical shape (${\Phi}3{\times}h10$) under compressive force of 10kN and, subsequently, the compacted powders were extruded at 563k in a hot furnace. Micro-extrusion has succeeded in forming micro-gear shafts.

• 항공우주기술
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• 제2권2호
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• pp.133-141
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• 2003

초소성 공정을 이용하여 구형 압력용기를 제작하는 경우 두께와 구형의 형상은 일정하지 않고 성형공정이 진행함에 따라 변하게 된다. 본 연구에서는 공정과정 동안 발생하는 초기 블랭크의 두께변화 예측을 이론적으로 해석하였다. 두께변화 예측을 위한 이론적인 모델은 Kuglov 등이 적용한 박막이론을 사용하였으며 요구되는 최종 두께를 얻기 위한 초기 블랭크의 두께, 블랭크의 균일한 변형을 얻기 위한 시간에 따른 압력 프로파일, 각 성형단계에서 위치에 따른 두께분포 및 시간에 따른 두께분포를 결정하였다. 공정 단계 전반에 걸쳐서 적용 모델 및 해석 프로그램의 적합성을 문헌의 시험 결과와 비교하여 검증하였다.

• 한국재료학회지
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• 제30권2호
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• pp.57-60
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• 2020

Titanium aluminides have attracted special interest as light-weight/high-temperature materials for structural applications. The major problem limiting practical use of these compounds is their poor ductility and formability. The powder metallurgy processing route has been an attractive alternative for such materials. A mixture of Ti and Al elemental powders was fabricated to a mechanical alloying process. The processed powder was hot pressed in a vacuum, and a fully densified compact with ultra-fine grain structure consisting of Ti₃Al intermetallic compound was obtained. During the compressive deformation of the compact at 1173 K, typical dynamic recrystallization (DR), which introduces a certain extent of grain refinement, was observed. The compact had high density and consisted of an ultra-fine equiaxial grain structure. Average grain diameter was 1.5 ㎛. Typical TEM micrographs depicting the internal structure of the specimen deformed to 0.09 true strain are provided, in which it can be seen that many small recrystallized grains having no apparent dislocation structure are generated at grain boundaries where well-developed dislocations with high density are observed in the neighboring grains. The compact showed a large m-value such as 0.44 at 1173 K. Moreover, the grain structure remained equiaxed during deformation at this temperature. Therefore, the compressive deformation of the compact was presumed to progress by superplastic flow, primarily controlled by DR.

• 대한기계학회논문집A
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• 제25권12호
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• pp.1933-1943
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• 2001

A micromechanical model is presented for superplasticity in which heterogeneous microstructures are coupled with deformation behavior. The effects of initial distributions of grain size, and their evolutions on the mechanical properties can be predicted by the model. Alternative stress rate models such as Jaumann rate and rotation incremental rate have been employed to analyze uniaxial loading and simple shear problems and the appropriate modeling was studied on the basis of hypoelasticity and elasto-viscoplasticity. The model has been implemented into finite element software so that full process simulation can be carried out. Tests have been conducted on Ti-6Al-4V alloy and the microstructural features such as grain size, distributions of grain size, and volume fraction of each phase were examined for the materials that were tested at different strain rates. The experimentally observed stress-strain behavior on a range of initial grain size distributions has been shown to be correctly predicted. In addition, the effect of volume fraction of the phases and concurrent grain growth were analyzed. The dependence of failure strain on strain rate has been explained in terms of the change in mechanism of grain growth that occurs with changing strain rate.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2006년도 제5회 박판성형 SYMPOSIUM
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• pp.99-102
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• 2006

In the present study, the blow forming characteristics of AZ31 sheet was investigated to test the feasibility of the practical application of wrought Mg alloys. Mg alloys have drawn a huge attention in the field of transportation and consumer electronics industries since it is the lightest alloy which could be industrially applicable. Most Mg alloy components have been fabricated by casting method. However, there have been a lot of research activities on the wrought alloys and their plastic forming process recently. Shallow cups for the small electronics cases have been stamped with warm die system. However, some technical issues will challenge Mg forming when large parts are considered with warm die system over $200^{\circ}C$. Most of all, thermal expansion of die system will deteriorate a die accuracy. On the other hand, blow forming does not have a problem with inaccuracy with die system. In this study, tensile tests were followed by blow forming at various temperature and pressure. AZ31 sheet showed a superplastic deformation behavior with extensive grain boundary sliding at the temperature above $300^{\circ}C$. However, the deformation behavior was likely to differ depending on stress condition.

• 한국재료학회:학술대회논문집
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• 한국재료학회 2009년도 춘계학술발표대회
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• pp.6.2-6.2
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• 2009

Ultra-fine grained (UFG) Al alloys, which have submicron grain structures, are expected to show outstanding high strength at ambient temperature and excellent superplastic deformation at elevated temperatures and high strain rate. In order to get the UFG microstructure, various kind of severe plastic deformation (SPD) processes have been developed. Among these processes, accumulative roll bonding (ARB) process is a promising process to make bulky Al sheets with ultrafine grained structure continuously. The purpose of the present study is to clarify the grain refinement mechanism during the ARB process and to investigate on the effects of ultra-fine grained structure on the mechanical properties. In addition, UFG AA8011 alloy (Al-0.72wt%Fe-0.63wt%Si) manufactured by the ARB had fairly large tensile elongation, keeping on the strength. In order to clarify the reason for the increase of elongation in the UFG AA8011 alloy, detailed microstructural and crystallographic analysis was performed by TEM/Kikuchi-line and SEM/EBSP method. The unique tensile properties of the UFG AA8011 alloy could be explained by enhanced dynamic recovery at ambient temperature, owing to the large number of high angle boundaries and the Al matrix with high purity.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2005년도 춘계학술대회 논문집
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• pp.279-282
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• 2005

Composites comprising various volume fractions of crystalline nickel and bulk amorphous (BA) were produced by means of electroless coating of nickel on BA powder of $Cu_{54}Ni_6Zr_{22}Ti_{18}$ and subsequent spark plasma sintering (SPS) of coated BA powder. The flow curves of composites at various temperatures in the supercooled liquid region were determined by the uniaxial compression test with various strain rates. During compression at $450^{\circ}C$ with $\dot{\varepsilon}=2\times10^{-3}$, the monolithic BA sample and crystalline-BA composites displayed the superplastic deformation with $\varepsilon>1.4$. At temperatures above $460^{\circ}C$, the stress-strain curve of the monolithic BA sample depicted a sharp peak stress and a fellowing stress drop due to cracking, while those of the crystalline-BA composites displayed work-hardening up to the imposed strain. FEM analysis indicated that a fairly homogeneous strain state prevailed throughout the composite, while a higher level of stress was obtained in a harder BA.

• 한국재료학회지
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• 제5권1호
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• pp.132-139
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• 1995

Al-Mg-Cu-Mn계 합금을 가공열처리하고 초소성 특성을 조사한 후 광학 및 전자 현미경을 이용하여 초소성에 영향을 미치는 주요한 인자들을 조사하였다. 균질화 과정에서 제거되지 않은 조대한 2차상들은 그 후의 가공열처리 과정에서도 계속 잔류하여 초소성 변형 중 기공을 유발함으로써ㅓ 초소성 신율을 저하시켰다. 반면에 가공열처리 과정에서 생성된 미세한 석출물은 결정립 성장을 억제하여 조직을 안정화함으로써 초소성 특성을 향상시켰다. 균질화처리 조건은 2차상의 크기과 분포에 큰 영향을 주어 2단계 균질화-공냉처리는 1단계 균질화-노냉처리보다 조대한 2차상의 제거와 미세석출물의 생성에 효과적이었다.

• 한국재료학회지
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• 제12권9호
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• pp.701-705
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• 2002

High temperature tensile test has been performed at $450^{\circ}C$ at different strain rate with various grain size due to different reduction rate of Al-4wt%Mg-0.4wt%Sc alloy which is known to be one of useful superplastic alloys. The grain size of Al-4wt%Mg-0.4wt%Sc alloy is $67~100\mu\textrm{m}$ which is courser than that of the alloy which is commonly used as the superplastic material. The total elongation of the Al-4wt%Mg-0.4wt%Sc alloy is strongly dependent on the average grain size, and is a linear function of the inverse average grain size for the present alloy.