• 열처리공학회지
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• 제29권3호
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• pp.103-108
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• 2016

In recent years, TRIP steels which are composed of ferrite, bainite, and retained austenite have drawn much attention for automotive sheets due to excellent combination of strength and ductility. The effect of two-step isothermal heat treatment of bainitic transformation on microstructures, especially retained austenites and tensile properties in the conventional TRIP steel was investigated. A two-step isothermal heat treatment, in which 50% bainitic transformation occurred at high temperature, followed by bainitic transformation at low temperature, improves tensile properties, resulting from enhanced mechanical stability of retained austenite against external plastic deformation due to refinement of retained austenites, compared to single-step isothermal heat treatment.

• Progress in Superconductivity
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• 제4권1호
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• pp.90-93
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• 2002

The sintering process of BSCCO 2223 tapes is a complex process that is very sensitive to parameters, such as temperature, oxygen partial pressure, heating and cooling rate and holding time. During the first heat treatment, 2212 phase of precursor powder is partially transformed into 2223 phase and some residual secondary phases, such as $(Bi,Pb)_2$$Sr_2$CuO／sub y／(2201), $(Ca,Sr)_2$CuO／sub y／(2/1AEC), (Ca,Sr)／sub 14／Cu／sub 24／O／sub 41／(14／24 AEC) etc. The secondary phases are difficult to be removed from the BSCCO 2223 matrix on the heat treatment. These secondary phases degrade the critical current density. In order to minimize the amount and size of alkaline earth cuprate(AEC) particles step heat treatment is applied during the first heat treatment under the varying atmosphere. Experimental results showed that by adapting the step heat treatment process, the amount and particle size of the secondary phases in the final tapes are decreased. Consequently, the BSCCO 2223grain texture and Jc properties are improved.

• 열처리공학회지
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• 제37권3호
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• pp.128-137
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• 2024

In this study, the carburizing heat treatment process used in aircraft gear manufacturing was compared with the general carburizing heat treatment process using AISI 9310 steel. The process of carburizing followed by slow cooling, and then quenching after austenitizing(Process A) showed less compressive residual stress and less retained austenite in the surface layer compared to the process of quenching directly after carburizing(Process B). In prpcess B, there was a large amount of retained austenite when quenched immediately after carburization, and when treated with subzero, martensite rapidly increased and the compressive residual stress increased significantly, but at the same time, there is a risk of cracking due to severe expansion in volume. Therefore, in the case of aviation parts, it is believed that a step-by-step heat treatment cycle was adopted to ensure stability against heat treatment cracks. As a result of the final tempering after sub-zero treatment, the A process specimen showed a deeper effective case depth and HV700 depth and a higher hardness value above HV700 than the B process specimen.

• 열처리공학회지
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• 제31권3호
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• pp.97-103
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• 2018

The objective of this study is to develop the mechanical properties of AlSiCu aluminum alloy by the two-step solution heat treatment. The microstructure of gravity casting specimen represents a typical dendrite structure having a secondary dendrite arm spacing (SDAS) of 40 mm. In addition to the Al matrix, a large amount of coarsen eutectic Si phase, $Al_2Cu$ intermetallic phase, and Fe-rich phases are generated. The eutectic Si phases are fragmented and globularized with solution heat treatment. Also, the $Al_2Cu$ intermetallic phase is resolutionized into the Al matrix. The $2^{nd}$ solution temperature at $525^{\circ}C$ might be a optimum condition for enhancement of mechanical properties of AlSiCu aluminum alloy.

• 한국수소및신에너지학회논문집
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• 제27권4호
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• pp.421-430
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• 2016

To prepare mesophase pitches through low energy process, pyrolysis fuel oil with $AlCl_3$ has been modified using two-step heat treatment which is heat-treated at $330^{\circ}C$ for 3~5 h after pre-treatment at $250^{\circ}C$. The result of polarized optical microscope observation, mesophase is not observed in pitches carried out only pre-heat treatment. While mesophase content is significantly increased from 9% to 100% according to increasing secondary heat treatment time from 3 h to 5 h. Synthesizing of the mesophase pitch at low temperature of $330^{\circ}C$ is attributed to decrease of viscosity of the pitches carried out first heat treatment with $AlCl_3$. The result of Fourier-transform infrared spectroscopic analysis, it is expected that aromatization of aliphatic compounds is dominant at early secondary heat treatment, on the other hand, polycondensation reaction becomes dominant as secondary heat treatment time increases. Aromaticity and stacking height of the pitches secondary heat treated for 5 hours are more increased about 25% and 107%, respectively, than that of pitches carried out only first heat treatment.

• 한국표면공학회지
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• 제46권1호
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• pp.16-21
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• 2013

CIGS (Cu-In-Ga-Se) films were deposited on the Mo coated soda lime glass (Mo/SLG) by RF magnetron sputtering using a single sintered target with different chemical compositions. Heat treatment of the CIGS films were carried out under three different conditions, 1step ($350^{\circ}C$ for 2 hour and $550^{\circ}C$ for 2 hour) and 2step ($350^{\circ}C$ for 1 hour and $550^{\circ}C$ for 1 hour). In the case of CIGS films post-annealed on 2step method, grain size remarkably increased compared to other methods, indicating that chemical composition [Cu/(Ga+In) = 1] of CIGS films was same as CIGS target. After heat treatment by 2step method, band gap energy of the CIGS film deposited at RF 80 W showed 1.4 eV which is broadly similar to identical band gap energy (1.2 eV) of CIGS film prepared by evaporation method. Therefore, 2step heat treatment method could be expected to low temperature process.

• Transactions on Electrical and Electronic Materials
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• 제3권4호
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• pp.27-31
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• 2002

Thin film diode with reliable interfacial structure was fabricated by using multi-step anodic oxidation. The thickness of the oxide layer was preciously controlled with anodic voltage. Also, interfacial structure between oxide layer and top electrode was improved by applying post heat-treatment. The thin film diode showed symmetric and stable I-V characteristics after the post heat-treatment.

• 열처리공학회지
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• 제32권2호
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• pp.57-60
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• 2019

The impact of two-step treatment on the mechanical properties of the 6061 Al alloy was investigated by testing the hardness and electrical conductance values. After two-step aging treatment, the hardness and electrical conductivity of the alloy was increased, and if the first aging treatment temperature was lower than the secondary aging treatment temperature, both the hardness and the electrical conductivity were not increased. The higher the temperature of the first aging treatment, the higher the hardness. The temperature of the first aging treatment is $175^{\circ}C$, $150^{\circ}C$, $120^{\circ}C$, and the second is $175^{\circ}C$ and $120^{\circ}C$.

• 한국정보디스플레이학회:학술대회논문집
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• 한국정보디스플레이학회 2009년도 9th International Meeting on Information Display
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• pp.152-155
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• 2009

A novel two-step surface treatment was developed and demonstrated for the carbon nanotube (CNT) cathode with highly efficient backlight unit application. An adhesive taping method was applied firstly and then followed by a post-heat treatment for the CNT cathode. During the postheat treatment process, some residues covering the CNTs were burned out. The post-heat treatment enhanced the emission current of the CNT cathode around 20% compared with that of no heat-treated sample.

• 한국세라믹학회지
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• 제50권1호
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• pp.70-74
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• 2013

Dependence of microwave dielectric properties on the crystallization behaviors of $CaMgSi_2O_6$ (diopside) glass-ceramics was investigated with different heat treatment methods (one and/or two-step). The crystallization behaviors of the specimens, crystallite size and degree of crystallization, were evaluated by differential thermal analysis (DTA), scanning electron microscope (SEM) and X-ray diffraction (XRD) analysis by combined Rietveld and reference intensity ratio (RIR) methods. With an increase in heattreatment temperature, the dielectric constant (K) and the quality factor (Qf) increased due to the increase of the crystallite size and degree of crystallization. The specimens heat-treated by the two-step method had a higher degree of crystallization than the specimens heat-treated by the one-step method, which induced improvement in the quality factor (Qf) of the specimens.