• 한국표면공학회지
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• 제28권6호
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• pp.361-367
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• 1995

When steels are heated at $1000^{\circ}C$ in a fused borax bath containing $V_2O_5$ and $B_4C$powders, vanadium carbide layers are formed on the steel surfaces. Since a decrease in carbon concentration and in microhardness in the substrate just below the carbide layer has been observed, gas nitrocarburizing and vanadium carbide forming processes were combined to form a V(C,N) type layer which prevented the decrease in carbon concentration in the substrate. EPMA analysis was done for this V(C,N) type layer. Hardness just below the layer and wear resistance properties of such treated specimens were investigated.

• 한국표면공학회지
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• 제43권1호
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• pp.31-35
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• 2010

Coatings of Ni-17 at.%W were electroplated on a steel substrate, and their corrosion behavior was investigated between 600 and $800^{\circ}C$ in an Ar-0.2%$SO_2$ atmosphere. They delayed the corrosion of the steel substrate. They were corroded into an outer NiO-rich layer, and an inner ($WO_3+NiO+NiWO_4$)-mixed oxide layer. Below these oxide layers, a sulfide layer gradually formed.

• Transactions on Electrical and Electronic Materials
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• 제7권4호
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• pp.184-188
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• 2006

This work describes efforts in the fabrication and testing of robust microelectromechanical systems (MEMS). Robustness is typically achieved by investigating non-silicon substrates and materials for MEMS fabrication. Some of the traditional MEMS fabrication techniques are applicable to robust MEMS, while other techniques are drawn from other technology areas, such as electronic packaging. The fabrication technologies appropriate for robust MEMS are illustrated through laminated polymer membrane based pressure sensor arrays. Each array uses a stainless steel substrate, a laminated polymer film as a suspended movable plate, and a fixed, surface micromachined back electrode of electroplated nickel. Over an applied pressure range from 0 to 34 kPa, the net capacitance change was approximately 0.14 pF. An important attribute of this design is that only the steel substrate and the pressure sensor inlet is exposed to the flow; i.e., the sensor is self-packaged.

• 한국표면공학회지
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• 제8권1호
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• pp.15-23
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• 1975

Electrodeposition of metals form aqueous solutions (eg, electroplating ) is frequently accompanied, by the discharge of hydrogen ions(in acidic solutions) or water molecules ( in alkaline electrolytes). The atomic hydrogen produced thus may partly diffuse into the interior of the substrate and when this is absorbed by iron/steel substrate, it has detrimental effects on the mechanical properties of the steel, leading to ahydrogen embrittlement. Steels, particularly the high strength steels, are prone to hydrogen embrittlement. In view of the increasing applications of high strength steels in variousindustries, particularly in the aircraft manufacture, there has been renewed interest in the studiesonhydrogen embrittlement during electroplating of metals. In this review, the author summarizes the reports on hydrogen embrittlement during preplating of metals. In this review , the author sumamrizes the hydrogen embrittlement during electroplating of metals. In this review , the author summarizes the reports on hydrogen embrittlement during preplating operations and electroplating of metals like copper, nickel, tin, zinc ,cadimum and chromium. Finally, the effect of degassing by baking to deembrittle the plated high tensile steels and mechanism of hydrogen embrittlement are briefly indicated.

• 한국표면공학회지
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• 제53권6호
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• pp.306-311
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• 2020

In this work, diamond-like carbon (DLC) films are coated onto plasma nitrided AISI 4140 steel by DC-pulsed PECVD. One problem of DLC films is their very poor adhesion on steel substrates. The purpose of the nitriding was to enhance adhesion between the substrate and the DLC films. The white layer formation is avoided. Plasma nitriding increased adhesion from 8 N for DLC coating to 25 N for duplex coating. Duplex plasma nitriding/DLC coating was proven to be more effective in improving the adhesion. The purpose of the bond layer was to enhance adhesion between the substrate and the DLC films.

• 수산해양교육연구
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• 제11권2호
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• pp.139-149
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• 1999

Thermal sprayed Ni-Cr alloy coating on the carbon steel was carried out erosion-corrosion test and electrochemical corrosion test in the marine environment. The erosion-corrosion behavior and electrochemical corrosion characteristics of substrate(SS400) and thermal sprayed Ni-Cr coating was investigated. The erosion-corrosion control efficiency of Ni-Cr coating to substrate was also estimated quantitatively. The main results obtained are as follows : 1) The weight loss rate of Ni-Cr coating layer by the erosion-corrosion compared with substrate was smaller. With the lapse of time, the weight loss rate of substrate was linearly increased in $25{\Omega}{\cdot}cm$ solution, but that of Ni-Cr coating became stable. 2) The corrosion potential of substrate became less noble than that of Ni-Cr coating layer, and the corrosion current density of Ni-Cr coating became lower than that of substrate. 3) The control efficiency of erosion-corrosion of Ni-Cr coating compared to substrate became more dull than that of corrosion in $25{\Omega}{\cdot}cm$ and $5000{\Omega}{\cdot}cm$ solution.

• 한국결정성장학회지
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• 제14권1호
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• pp.6-11
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• 2004

Bias 인가된 hot filament CVD 방법을 이용해 티타늄을 RF sputtering 법으로 고속도강에 피복하여 중간 층으로 한 후 다이아몬드 박막을 피복할 때 bias 전압의 영향과 계면 층의 특성을 조사하였다. 다이아몬드 증착 시 bias가 인가될 경우 필라멘트에서 전자 방출이 촉진되어 다이아몬드 핵생성과 성장을 촉진시켰으며 본 실험에서의 최적 증착 조건은 증착 압력 20 torr, bias 인가전압 200V, 기판온도 $700^{\circ}C$로 나타났다. 강에의 다이아몬드 박막 형성 시 중간 층으로서의 티타늄은 Fe 및 C에 대한 확산도가 높고 탄화물 형성 원소이므로 다이아몬드 핵생성 및 성장에 적합한 원소로 나타났다.

• 한국재료학회지
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• 제11권4호
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• pp.324-328
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• 2001

아크이온 플레이팅 장치를 이용하여 STD61강 기판 위에 이온질화 전처리를 행하거나 하지 않은 후, CrN 박막을 증착하고, 대기중 $700~900^{\circ}C$의 온도에서 40시간동안 이들에 대한 산화거동을 연구하였다. 산화거동은 열중량분석기, X선회절기, EDS, SEM을 이용하여 조사하였다. 증착된 CrN박막은 CrN과 $Cr_2$N의 두 상으로 구성되어 있었다. CrN박막은 보호적 $Cr_2$O$_3$층을 형성하여 기판을 산화로부터 보호하였다. 이온질화처리는 CrN박막의 내산화성에 영향을 주지 않았다.

• 한국화재소방학회논문지
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• 제19권1호
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• pp.51-58
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• 2005

본 연구는 새로 개발된 난연도료를 바탕재(FRP PVC, AL, 스테인레스 스틸)에 도장한 실험체에 대하여 난연성. 화염전파. 산소지수. 가연성, 연기밀도, 독성지수를 평가하였다 연구결과 실험체(AL, 스테인레스 스틸)의 난연1급실험은 적합하였으며, 실험체(FRP, AL, 스테인레스 스틸)의 화염전파실험에서 착화되지 않았고, 실험체 모두의 산소지수는 약 $50\%$, 가연성실험은 V-0급으로 나타났다. 또한 연기밀도 챔버를 이용한 Flaming mode에서 최대연기밀도는 43-338 및 덕성지수는 0.57-1.12인 것으로 나타났다.

• 한국세라믹학회지
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• 제31권9호
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• pp.1060-1068
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• 1994

Stable zirconia sol was prepared from zirconium butoxide Zr(OC4O9)4 as a precursor and ethylacetoacetate(EAcAc) or diethylene glycol(DEG) as a chelating agent under ambient agent under ambient atmosphere by Sol-Gel process. The sythesized sol was coated on 304 stainless steel substrate by dip coating, thereafter zirconia film could be obtained by heat-treatment at $600^{\circ}C$. The characteristics of coating film were determined by FT-IR, XRD, and ellipsometion peak represented Zr-O-Zr bonding of tetragonal phase was shown at 470cm-1. Crystallization of zirconia gel and film from amorphous state to tetragonal phase started at 40$0^{\circ}C$, and then transformed into monoclinic phase around $700^{\circ}C$. Zirconia film coated on 304 stainless steel substrate showed relatively low porosity of 16% when it was coated with 0.4M zirconia sol and thereafter heat-treated at 80$0^{\circ}C$ and the film was densified continuously up to 90$0^{\circ}C$. The zirconia film of 10 nm thick acted as a protective layer against oxidation up to $700^{\circ}C$.