• Journal of Surface Science and Engineering
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• v.51 no.4
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• pp.249-255
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• 2018

High temperature and low temperature gaseous nitriding was performed in order to study of the surface hardening and wear properties of the nitrided AISI 410 Martensitic stainless steels. High temperature gaseous nitiridng (HTGN) was carried out using partial pressure $N_2$ gas at $1,100^{\circ}C$ for 10 hour, and Low temperature gaseous nitiridng (LTGN) was conducted in a gas mixture of NH3 and N2 at $470^{\circ}C$ for 10 hour. The nitrided samples were characterized by microhardness measurements, optical microscopy and scanning electron microscopy. The phases were identified by X-ray diffraction and nitrogen concentration was analyzed by GD-OES. The HTGN specimen had a surface hardness of about $700HV_{0.1}$, $350{\mu}m$ of case depth. A ${\sim}50{\mu}m$ thick, $1,250HV_{0.1}$ hard nitrided case formed at the surface of the AISI 410 steel by LTGN, composed nitrogen supersaturated expanded martensite and ${\varepsilon}-Fe_{24}N_{10}$ iron nitrides. Additionally, the results of the wear tests, carried out LTGN specimen was low friction coefficient and high worn mass loss of ball. The increase in wear resistance can be mainly attributed to the increase in hardness and to the lattice distortion caused by higher nitrogen concentration.

• Tribology and Lubricants
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• v.34 no.6
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• pp.217-225
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• 2018

In this study, we spray a Ni-Cr composite powder onto AISI 4340 steel using the high velocity oxygen fuel method. We subsequently subject the Ni-Cr coating (as-sprayed) to ultrasonic nanocrystal surface modification (UNSM) process to improve the tribological performance. This study aims at increasing the wear resistance and durability of the Ni-Cr coating by altering the surface integrity and microstructure via the UNSM process. The UNSM process reduces the surface roughness of the as-sprayed coating by about 64%, which is explained by observing the elimination of high peaks and valleys and filling up micro-pores. Furthermore, a change in the microstructure of the coating due to continuous high-frequency strikes to the surface by a tip can lead to an increase in hardness from about 48 to 60 HRC. Furthermore, we investigate the characterization of the friction and wear behavior of Ni-Cr coating by a ball-on-disc tribometer in the dry conditions. We determine that after the UNSM process, there is a significant reduction in the friction coefficient of the as-sprayed coating from approximately 1.1 to 0.75. This is owing to the increased hardness and smoothed surface roughness. In addition, we investigate the surface morphology and wear track of the coatings before and after the UNSM process using a scanning electron microscope, energy dispersive spectrometer, and three-dimensional laser scanning microscope. We observe that the wear track of the Ni-Cr coating after the UNSM process is lower than that of the as-sprayed one. Thus, we confirm that the UNSM process has a significant influence on the improvement of the tribological performance of the Ni-Cr composite coating.

• Tribology and Lubricants
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• v.34 no.6
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• pp.241-246
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• 2018

This research addresses the improvement of tribo-systems, specifically regarding the reduction of friction and wear through tribo-coupling between tetrahedral amorphous carbon (ta-C) with different types of counterpart materials, namely bearing steel (SUJ2), tungsten carbide (WC), stainless steel (SUS304), and alumina ($Al_2O_3$). A second variable in this project is the utilization of different values of duct bias voltage in the deposition of the ta-C coating - 0, 5, 10, 15, and 20 V. The results of this research are expected to determine the optimum duct bias and best counter materials associated with ta-C to produce the lowest friction and wear. Results obtained reveal that the tribo-couple between the ta-C coating and SUJ2 balls produces the lowest friction coefficient and wear rate. In terms of duct bias changes, deposition using 5 V produces the most optimum tribological behavior with lowest friction and wear on the tribo-system. In contrast, the tribo-couple between ta-C with a WC ball causes penetration through the coating surface layer and hence high surface delamination. This study demonstrates that the most effective ta-C coating duct bias is 5 V associated with SUJ2 counter material to produce the lowest friction and wear.

• Journal of Powder Materials
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• v.28 no.4
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• pp.336-341
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• 2021

In this study, a nanocrystalline FeNiCrMoMnSiC alloy was fabricated, and its austenite stability, microstructure, and mechanical properties were investigated. A sintered FeNiCrMoMnSiC alloy sample with nanosized crystal was obtained by high-energy ball milling and spark plasma sintering. The sintering behavior was investigated by measuring the displacement according to the temperature of the sintered body. Through microstructural analysis, it was confirmed that a compact sintered body with few pores was produced, and cementite was formed. The stability of the austenite phase in the sintered samples was evaluated by X-ray diffraction analysis and electron backscatter diffraction. Results revealed a measured value of 51.6% and that the alloy had seven times more austenite stability than AISI 4340 wrought steel. The hardness of the sintered alloy was 60.4 HRC, which was up to 2.4 times higher than that of wrought steel.

• Applied Chemistry for Engineering
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• v.26 no.1
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• pp.104-110
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• 2015

It is known that polymer concretes are 8~10 times more expensive than ordinary Portland cement concretes; therefore, in the production of polymer concrete products, it is very important to reduce the amount of polymer binders used because this occupies the most of the production cost of polymer concretes. In order to develop a technology for the reduction of polymer binders, smooth and spherical aggregates were prepared by the atomizing technology using the oxidation process steel slag (electric arc furnace slag, EAFS) and the reduction process steel slag (ladle furnace slag, LFS) generated by steel industries. A reduction in the amount of polymer binders used was expected because of an improvement in the workability of polymer concretes as a result of the ball-bearing effect and maximum filling effect in case the polymer concrete was prepared using the smooth and spherical atomized steel slag instead of the calcium carbonate (filler) and river sand (fine aggregate) that were generally used in polymer concretes. To investigate physical properties of the polymer concrete, specimens of the polymer concrete were prepared with various proportions of polymer binder and replacement ratios of the atomized reduction process steel slag. The results showed that the compressive strengths of the specimens increased gradually along with the higher replacement ratios of the atomized steel slag, but the flexural strength showed a different maximum strength depending on the addition ratio of polymer binders. In the hot water resistance test, the compressive strength, flexural strength, bulk density, and average pore diameter decreased; but the total pore volume and porosity increased. It was found that the polymer concrete developed in this study was able to have a 19% reduction in the amount of polymer binders compared with that of the conventional product because of the remarkable improvement in the workability of polymer concretes using the spherical atomized oxidation steel slag and atomized reduction steel slag instead of the calcium carbonate and river sand.

• Journal of Mechanical Science and Technology
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• v.16 no.11
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• pp.1428-1434
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• 2002

The ball-on-disk type sliding tests with boundary lubricated steels were carried out to verify the effect of initial spacing in surface profiles on wear and scuffing. Three kinds of surface spacing, which are closely related with initial surface micro-cracks on sliding surfaces, were produced on AISI 1045 steel surfaces using different grinding and polishing processes. Frictional forces and time to scuffing were measured, and the shape and amount of wear particles were analyzed to compare the with original surface profiles. From the tests, it was confirmed that the size of wear particles are related closely to the original spacing of the surface profile. The time to failure and amount of wear were sensitive to the surface spacing. The wider surface spacing shows much longer sliding life and smaller amount of wear than the others. Time to scuffing was increased with increasing surface pro(lie spacing. The size of wear particles increased while the wear and wear rate K were decreased with an increase in surface spacing. After the sliding tests, surface cracks of inner parts of the wear track formed due to scuffing were observed and compared among the specimens having the different surface spacing.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.26 no.5
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• pp.835-842
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• 2002

In this paper, static and fatigue bending strengths and failure mechanisms of CFRP (carbon fiber reinforced plastics) laminates having impact damages have been evaluated. Composite laminates used for this experiment are CF/EPOXY orthotropy laminated plates, which have two-interfaces $[0^0_ 4/90^0_4]_{ sym}$. A steel ball launched by the air gun collides against CFRP laminates to generate impact damages. The damage growth during bending fatigue test is observed by the scanning acoustic microscope (SAM) and also, the fracture surfaces were observed by using the SEM (scanning electron microscope). In the case of impacted-side compression, fracture is propagated from the transverse crack generated near impact point. On the other hand, fracture is developed toward the impact point from the edge of interface-B delamination in the case of impacted-side tension. Eventually, failure mechanisms have been confirmed based on the observed delamination areas and fracture surfaces.

• Advanced Composite Materials
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• v.18 no.4
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• pp.395-413
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• 2009

Impact tests on high-strength membrane materials under biaxial loads were experimentally conducted in order to evaluate influence of biaxial loads on impact fracture of the membrane materials for the inflated applications. Cruciform specimens of the membrane materials were fabricated for applying biaxial loadings during the impact test. A steel ball was shot using a compressed nitrogen gas gun, and struck the membrane specimen. Impact tests on uniaxial strip specimens were also conducted to obtain the effect of specimen configuration and boundary condition on the impact fracture. The results of the measured crack length and the ultra-high speed photographs indicate the impact fracture properties of the membrane fabrics under biaxial loadings. Crack length due to the impact increased with applied tensile load, and the impact damages of the cruciform membrane materials under biaxial loadings were smaller than those of under uniaxial loadings. Impact fracture of the strip specimen was more severe than that of the cruciform specimen due to the difference of boundary conditions.

• Journal of the Korean Society for Nondestructive Testing
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• v.17 no.2
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• pp.81-88
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• 1997

Impact behavior of carbon fiber reinforced plastics (CFRP) laminates were evaluated with tension test and compact tension test. A steel ball launched by an air gun collides against CFRP laminates to generate impact damage of relatively low energy. The static tensile and fracture toughness tests were performed to evaluate the residual strength and the AE behavior of impact-damaged laminates. As a results, it was found that the static strength, the fracture toughness and the AE-event count were decreased with increasing of impact velocity and delamination area, and to have a different strength ratio and fracture toughness ratio for each stacking method. And also, it was confirmed that strength and fracture toughness of impact-damaged CFRP laminates could be evaluated and analyzed quantitatively by AE techniques.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.20 no.6
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• pp.1836-1842
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• 1996

In this paper, static and fatigue bending strengths of CFRP(carbon fiber reinforced plastic laminates having impact damage(FOD) are evaluated. Composite laminates used for this experiment are CF/EPOXY and CF/PEEK orthotropy laminated plates, which have two-interfaces[${0^0}_4{90^0}_4}$]$_sym$. A steel ball launched by the air gun colides against CFRP laminates to generate impact damages. The damage growth during bending fatigue test is observed by the scanning acoustic microscope(SAM). When the impacted side is compressed, the residual fatigue bending strength of CF/PEEK specimen P is greater that that of CF/EPOXY SPECIMEN B. On the other hand, when the impacted side is in tension, the residual fatigue bending strength of CF/PEEK speicemen P is smaller than that of CF/EPOXY specimen B. In the case of impacted-side compression, fracture is proposed from the transverse crack generated near impact point. On the other hand, fracture is developed toward the impact point from the edge of interface-b delamination in the case of impacted-side tension.