• Bulletin of the Korean Chemical Society
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• v.32 no.1
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• pp.77-82
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• 2011

A new high performance liquid chromatograpgy (HPLC) stationary phase that possesses an internal carbonyl functional group is synthesized by heterogeneous "graft from" method. This new stationary phase, poly (vinyl octadecanoate) grafted silica (Sil-2) is then characterized by different physico-chemical methods such as diffuse reflectance infrared fourier transform, suspension state $^1H$ NMR, solid state $^{13}C$ CP/MAS NMR, $^{29}Si$ CP/MAS NMR, elemental analysis and thermogravimetric analysis. Chromatographic properties of Sil-2 were evaluated under reversed phase condition by separating polycyclic aromatic hydrocarbons (PAHs) and comparing the chromatographic results with those on polymeric as well as monomeric octadecylated silica stationary phases.

• Analytical Science and Technology
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• v.33 no.4
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• pp.169-176
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• 2020

Separation of basic compounds using reverse phase chromatography on a silica-based stationary phase represents a major challenge, because of the interaction between the cationic sites of the basic compounds with the anionic silanols of the stationary phase. This study presents a simple, reliable, and organic solvent - free liquid chromatographic method for the determination of terbutaline and salbutamol, in which a room temperature ionic liquid (RTIL) is used as mobile phase additive. We investigated various mobile phase parameters affecting the retention of the two compounds, such as types and concentration of RTILs and, pH of the mobile phase were investigated. The developed method was validated according to International Conference on Harmonization (ICH) guidelines and successfully applied effectively to determine salbutamol sulfate in pharmaceutical preparations.

• The Journal of the Acoustical Society of Korea
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• v.19 no.7
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• pp.28-33
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• 2000

For efficient quantization of speech representation, it is common to incorporate Perceptual characteristics of human hearing. However, the focus has been confined only to the magnitude information of speech, and little attention has been paid to phase information. This paper presents a novel approach, termed perceptually irrelevant phase elimination (PIPE), to find out irrelevant phase information of acoustic signals in terms of perception. The proposed method, which is based on the observation that the relative phase relationship within a critical band is perceptually important, is derived not only for stationary Fourier signal but also for harmonic signal. The proposed method is incorporated into the analysis/synthesis system based on harmonic representation of speech, and subjective test results demonstrate the effectiveness of proposed method.

• Journal of Magnetics
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• v.16 no.4
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• pp.391-397
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• 2011

An inductance measurement method for interior permanent magnet synchronous machine (IPMSM) is proposed in this paper. In this method, the motor is measured at standstill condition, and only a 3-phase voltage source, an oscilloscope and a DC voltage source are required. Depending on the deductive dq-axis voltage equations in the stationary frame of reference, the dq-axis inductances at different current magnitude and vector angle can be calculated by the measured 3-phase voltages and currents. And hence, the saturation and cross-magnetizing effect of the inductances are measurable. This paper introduces the principle equations, experiment setup, data processing, and results comparison on the concentrated-winding and distributed-winding IPMSMs.

• Journal of Mechanical Science and Technology
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• v.20 no.6
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• pp.849-863
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• 2006

IBM (Immersed Boundary Method) with feedback momentum forcing was applied to stationary and moving bodies. The capability of IBM to treat the obstacle surfaces, especially with moving effect has been tested for two dimensional problems. Stationary and oscillating cylinders were simulated by using IBM based on finite volume method with Cartesian coordinates. For oscillating cylinder, lateral and vertical motions are considered, respectively. Present results such as time histories of drag and lift coefficients for both stationary and oscillating cases are in good agreement with previous numerical and experimental results. Also, the instantaneous wake patterns of oscillating cylinder with different oscillating frequency ratios well represented those of previous researches. More feasibility study for IBM has been carried out to two oscillating cylinders. Drag and lift coefficients are presented for two cylinders oscillating sinusoidally with phase difference of $180^{\circ}$.

• Journal of Mechanical Science and Technology
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• v.18 no.11
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• pp.1941-1948
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• 2004

This paper presents a novel design of indoor airship having a passive wheeled mechanism and its stationary position control. This wheeled blimp can work both on the ground using wheeled vehicle part and in the air using the floating capability of the blimp part. The wheeled blimp stands on the floor keeping its balance using a caster-like passive wheel mechanism. In tele-guidance application, stationary position control is required to make the wheeled blimp naturally communicate with people in standing phase since the stationary blimp system responds sensitively to air flow even in indoor environments. To control the desired stationary position, a computed torque control method is adopted. By performing a controller design through dynamic analysis, the control characteristics of the wheeled blimp system have been found and finally the stable control system has been successfully developed. The effectiveness of the controller is verified by experiment for the real wheeled blimp system.

• The Journal of Korea Institute of Information, Electronics, and Communication Technology
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• v.2 no.2
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• pp.29-36
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• 2009

The analysis of Radar signal, telecommunication, bioengineering, seismic, and acoustic signal is consist of the Non-stationary signal which has non-linear phase variation. Non-stationary signal means that the physical properties of signal depend on time variation and the instantaneous frequency represents physical property of these type of signal. Thus estimation of the instantaneous frequency of non-stationary signal is important subject in signal processing. In this work, the instantaneous frequency analysis method utilizing continuous wavelets transform is represented and compared with Hilbert Transform method.

• Bulletin of the Society of Naval Architects of Korea
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• v.27 no.3
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• pp.11-18
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• 1990

The Kelvin's method of stationary phase breaks down at the cusp point and yields a nonuniform expansion near it. By making use of the nonuniform expansion, we derive a uniform expansion near the cusp point.

• Bulletin of the Korean Chemical Society
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• v.33 no.12
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• pp.4141-4144
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• 2012

This paper introduces a technique for resolving amino acids that combines the advantages of the conventional CSP (chiral stationary phase) method with the CMPA (chiral mobile phase additive) method. A commercially available chiral crown ether column, CROWNPAK CR(+), was used as the CSP and three cyclodextrins (${\beta}$-CD, ${\gamma}$-CD, HP-${\beta}$-CD) were used as the mobile phase additives. Chromatographic resolution was performed at $25^{\circ}C$ and $50^{\circ}C$ with or without sonication. A comparison of the chromatographic results under ultrasonic conditions with those under non-ultrasonic conditions showed that ultrasound decreased the elution time and enantioselectivity at all temperatures. In the case of the ${\beta}$-CD mobile phase additive, the elution time and enantioselectivity under ultrasonic condition were significantly higher than under non-sonic condition at all temperatures. Commercially available Chiralpak AD, Whelk-O2 and Pirkle 1-J columns were used as CSPs to examine more meticulously the effects of ultrasonication and temperature on the optical resolution. The optical resolution of some chiral samples analyzed at $25^{\circ}C$ and $50^{\circ}C$ with or without sonication was compared. As in the previous case, the enantioselectivity was lower at $25^{\circ}C$ but similar enantioselectivity was observed at $50^{\circ}C$.

• The Transactions of the Korean Institute of Power Electronics
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• v.25 no.1
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• pp.13-20
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• 2020

Accurate parameters based on equivalent circuit are required for high-performance field-oriented control in a three-phase induction motor. In a normal case, stator resistance can be accurately measured using a measuring equipment. Except for stator resistance, all machine parameters on the equivalent circuit should be estimated with particular algorithms. In the viewpoint of traditional regions, the parameters of an induction motor can be identified through the no-load and standstill test. This study proposes an identification method that uses the d-axis model of the induction motor in a stationary frame with the predefined information on stator resistance. Mutual inductance is estimated on the rotational dq coordination similar to that in the traditional no-load experiment test. The leakage inductance and rotor resistance can be estimated simply by applying different voltages and frequencies in the d-axis model of the induction motor. The proposed method is verified through simulation and experimental results.