• 분석과학
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• 제15권4호
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• pp.335-340
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• 2002

유도결합 플라스마 질량분석법 (ICP-MS)을 이용하여 모발 중 다원소 동시 정량법을 확립하였다. 0.05 g의 모발 시료에 내부표준물질인 In을 가하고 질산 1.5 mL와 함께 테플론 가압분해 용기에 넣어 마이크로파를 이용하여 분해하는 시료전처리법을 사용하였다. 측정값의 정확도 및 신뢰도를 확인하기 위하여 모발 인증표준물질인 GBW 09101을 반복 분석하였는데 측정값은 인증값과 불확도 범위 내에서 잘 일치하는 결과를 얻었다.

• 한국염색가공학회지
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• 제27권4호
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• pp.288-300
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• 2015

This study was executed to substitute Carbon-arc method, which is a method currently used for testing light-fastness of military textile products, with Xenon arc method. Specimens used in the study were classified according to the fabric material and color of military textile products and were composed of 11 items of 42 kinds with different colors. Light-fatness test was done by comparing the result of Carbon-arc(KS K 0700) and Xenon arc(KS K ISO 105-B02) method. In Xenon arc method, blue wool reference materials of 1~8 was used, and exposure condition preferred in American continent and light exposure method 3 were applied. After testing with both methods, grade of light-fastness, color difference, reflectance and color were examined. Even though there was a slight difference among 42 specimens used in the test, results exceeded the quality standard both in Carbon-arc-lamp and Xenon arc-lamp. Therefore, it was confirmed that applying KS K ISO 105-B02 together in the KS K 0700-regulated Ministry of National Defense standard and purchase order would also fit.

• 한국해양바이오학회지
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• 제14권2호
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• pp.69-75
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• 2022

The micro-Kjeldahl method, a common technique for analyzing crude proteins, is time-consuming and dangerous due to the employment of reagents such as sulfuric acid and sodium hydroxide. However, a Fourier transform near-infrared (FT-NIR) spectrophotometer analysis can be completed in under a minute after simple pre-processing if data has been gathered using sufficient reference material in advance. Furthermore, the use of safe reagents in this technique ensures the safety of the experimenter and the environment. In addition, a portable FT-NIR spectrophotometer enables real-time measurement at processing or distribution sites and has recently gained popularity. The standard errors of calibration and regression (r²) for the calibration result for estimating the crude protein content of dried laver were 0.9775 and 1.2526, respectively. The standard error of prediction was 1.1814, and the r² was 0.9303 in the validation results, which was a good level. In the present study, a method for predicting the crude protein content of dried laver using an FT-NIR spectrophotometer in the range of 29%-40% crude protein content has been reported.

• 농약과학회지
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• 제20권3호
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• pp.211-220
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• 2016

본 연구는 풋고추 시료를 이용하여 농약다성분 분석표준물질을 개발하기 위해 수행하였다. 10종의 농약성분을 풋고추 시료에 처리하여 균질하게 분포될 수 있도록 조제하였으며, 국제적인 지침서인 'ISO Guide 35', 'ISO Guide 13528' 그리고 'EURL-PT'에서 요구하는 균질성, 안정성, 인증값 및 표준불확도가 확립된 농약다성분 풋고추 분석표준물질을 개발하였다. 개발된 분석표준물질의 병간 표준편차와 병내 표준편차는 인증값의 1.7~3.7%로 매우 우수한 균질성을 나타냈으며, 불균질성에 의한 표준불확도는 인증값의 0.8~1.15% 매우 낮아 분석표준물질로 사용하기에 매우 적합하였다. 다양한 조건에서의 안정성을 확인한 결과, 실온 $20{\sim}30^{\circ}C$)에서는 7일, 냉동($-20^{\circ}C$)에서는 30일 동안 안정하였으며, 초저온 상태($-80^{\circ}C$)에서는 bifenthrin, Fenpropathrin을 제외한 8종이 245일 동안 안정하였다. 개발된 농약다성분 풋고추 분석표준물질을 사용하여 잔류농약을 분석하는 8기관의 시험소를 평가한 결과, 일부기관에서는 6성분을 검출하지 못하였으며 일부 농약성분에 대해서는 의심스러운(questionable) 또는 부적합(unacceptable)의 평가를 받았다. 동일한 분석표준물질에 대해서 각 기관마다 분석결과의 차이가 나타나는 것을 확인하였으며, 이런 결과를 통해서 잔류농약의 분석결과 신뢰성과 일관성을 향상시키기 위해 풋고추 분석표물질을 활용한 정도관리 또는 숙련도 평가시험이 필요할 것으로 보인다.

• 대한기계학회논문집B
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• 제27권12호
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• pp.1766-1771
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• 2003

House made differential mobility analyzer(DMA) is calibrated with NIST SRM 1691(300 nm PSL). Then the particle size and uncertainty for differential mobility analyzer(DMA) using the NIST SRM 1963(100 nm PSL). In result, calibration of prototype DMA is measured using 300 nm NIST SRM 1691, then sheath air flow was corrected 126.67 ㎤/s. Corrected sheath air flow is used in uncertainty measurement of prototype DMA. Uncertainty analysis is performed using NIST SRM 1963(100 nm PSL). The experimental result shows that NIST SRM 1963 is measured as 102.17 nm with a type A uncertainty of 0.33 nm.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2004년도 추계학술대회 논문집
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• pp.1335-1338
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• 2004

This paper describes the result of structure analysis of body structure. The purpose of the analysis is to evaluate an safety which body structure shall be considered fully sufficient rigidity so as to satisfy proper system function under maximum load and operating condition. Material of body structure applied an aluminum alloy. Body structure consist of side frame, under frame, roof frame, end frame. FEM analysis is based on 'Performance Test Standard for Electrical Multiple Unit, noticed by Ministry of Construction & Transportation, in 2000 ' and reference code is JIS E 7105. The analysis results have been very safety and stable for design load conditions.

• 한국해양공학회지
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• 제10권2호
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• pp.98-105
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• 1996

A method is proposed to evaluate the elastic-plastic fracture resistance curve only with load displacement records without the crack length measurement in CT specimen. This method is based on the idea that the effect of plastic deformation and the crack growth can be measured only by using a load-displacement record. If we know the reference-load curve representing the hardening of specimen, then the crack extension can be calculated by the elastic compliance determined from the load ratio. The results of this proposed method were compared to those of the elastic-plastic fracture resistance curve for the ASTM standard unloading compliance method. The experimental results for two kinds of ductile materials showed that the proposed method well simulates the material J-R curves. This method is currently applied for CT specimens. but it can be extended to the other specimen geometries.

• 한국철도학회:학술대회논문집
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• 한국철도학회 2003년도 추계학술대회 논문집(III)
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• pp.59-64
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• 2003

This paper describes the result of structure analysis and load test of body structure. The purpose of the analysis and test is to evaluate an safety which body structure shall be considered fully sufficient rigidity so as to satisfy proper system function under maximum load and operating condition. Material of body structure applied an aluminum alloy. This strength test is based on 'Performance Test Standard for Electrical Multiple Unit, noticed by Ministry of Construction & Transportation, in 2000' and reference code is JIS E 7105

• 한국철도학회:학술대회논문집
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• 한국철도학회 2002년도 추계학술대회 논문집(I)
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• pp.156-161
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• 2002

This paper describes the result of carbody load test. The purpose of the test is to evaluate an safety which carbody structure shall be considered fully sufficient rigidity so as to satisfy proper system function under maximum load and operating condition. Carbody material applied a stainless steel and an aluminum alloy, The stainless steel model is the carbody of a motor car which is delivering to KNR line 1 in 2002 and the aluminum alloy model is the carbody of a motor car which is delivering to GWANGJU line 1 in 2003. This strength test is based on "performance test standard for Electrical Multiple Unit, noticed by Ministry of Construction ＆ Transportation, in 2000" and reference code is UIC 566 and JIS E 7105.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2005년도 추계학술대회 논문집
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• pp.49-54
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• 2005

This paper describes the result of structure analysis and load test of body structure. The purpose of the analysis and test is to evaluate an safety which body structure shall be considered fully sufficient rigidity so as to satisfy proper system function under maximum load and operating condition. Material of body structure applied an aluminum alloy. Body structure consist of side frame, under frame, roof frame, end frame. Both FEM analysis and load test are based on 'Performance Test Standard for Electrical Multiple Unit, noticed by Ministry of Construction & Transportation, in 2000' and reference code is JIS E 7105. The test results have been very safety and stable fer design load conditions.