• Analytical Science and Technology
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• v.15 no.4
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• pp.335-340
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• 2002

An analytical method has been developed to determine multi-elements in human hair samples by inductively coupled plasma mass spectrometry (ICP-MS). 0.05 g of hair sample was added to the Teflon digestion bomb together with 1.5 mL of nitric acid and an appropriate amount of In as an internal standard. The sample was then decomposed in the microwave digestion system. The hair certified reference material, GBW 09101, was analyzed for the validation of the analytical method. The determined values were in good agreement with the certified values within the uncertainty range.

• Textile Coloration and Finishing
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• v.27 no.4
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• pp.288-300
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• 2015

This study was executed to substitute Carbon-arc method, which is a method currently used for testing light-fastness of military textile products, with Xenon arc method. Specimens used in the study were classified according to the fabric material and color of military textile products and were composed of 11 items of 42 kinds with different colors. Light-fatness test was done by comparing the result of Carbon-arc(KS K 0700) and Xenon arc(KS K ISO 105-B02) method. In Xenon arc method, blue wool reference materials of 1~8 was used, and exposure condition preferred in American continent and light exposure method 3 were applied. After testing with both methods, grade of light-fastness, color difference, reflectance and color were examined. Even though there was a slight difference among 42 specimens used in the test, results exceeded the quality standard both in Carbon-arc-lamp and Xenon arc-lamp. Therefore, it was confirmed that applying KS K ISO 105-B02 together in the KS K 0700-regulated Ministry of National Defense standard and purchase order would also fit.

• Journal of Marine Bioscience and Biotechnology
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• v.14 no.2
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• pp.69-75
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• 2022

The micro-Kjeldahl method, a common technique for analyzing crude proteins, is time-consuming and dangerous due to the employment of reagents such as sulfuric acid and sodium hydroxide. However, a Fourier transform near-infrared (FT-NIR) spectrophotometer analysis can be completed in under a minute after simple pre-processing if data has been gathered using sufficient reference material in advance. Furthermore, the use of safe reagents in this technique ensures the safety of the experimenter and the environment. In addition, a portable FT-NIR spectrophotometer enables real-time measurement at processing or distribution sites and has recently gained popularity. The standard errors of calibration and regression (r²) for the calibration result for estimating the crude protein content of dried laver were 0.9775 and 1.2526, respectively. The standard error of prediction was 1.1814, and the r² was 0.9303 in the validation results, which was a good level. In the present study, a method for predicting the crude protein content of dried laver using an FT-NIR spectrophotometer in the range of 29%-40% crude protein content has been reported.

• The Korean Journal of Pesticide Science
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• v.20 no.3
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• pp.211-220
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• 2016

This study was to develop the analytical reference material of green-pepper for multi-residue analysis of pesticides. According to the ISO Guide 35, ISO Guide 13528 and EURL-PT protocol, the homogeneity, stability, assigned value and uncertainty were calculated to assess if it was suitable to be used as the proficiency test or quality control. The values of the within-bottle standard variation ($s_{wb}$) and the between-bottle standard variation ($s_{bb}$) were 1.7~3.7% of assigned value according to the requirement of the ISO guide 35. And, the uncertainty ($u^*{_{bb}}$) due to inhomogeneity was 0.8~1.1% for all pesticides. The storage stabilities of ten-pesticides at various conditions were assessed. For all target pesticides, the slop ($b_1$) values were smaller than the corresponding values of $[t_{0.95,n-2}{\times}s(b_1)]$ specified by the ISO guide 35, indicating that there were no statistically significant decreases in the concentration of the target pesticides when the analytical reference material was stored at room temperature ($20{\sim}30^{\circ}C$) for 7 days, freezing ($-20^{\circ}C$) for 30 days and deep freezer ($-80^{\circ}C$. except for bifenthrin, fenpropathrin) for 245 days. For proficiency test by using it developed by Korea Institute of Toxicology, inter-lab test was performed with eight organization performing the residual pesticide analysis. We found that there were some different results among them. Some were assessed as questionable or unacceptable for two pesticides and one organization didn't analyze the six pesticides. From these results, this green-pepper analytical reference material containing ten-pesticides could be used as a tool for the proficiency test to improve the reliability or consistency for pesticide residue's results.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.27 no.12
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• pp.1766-1771
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• 2003

House made differential mobility analyzer(DMA) is calibrated with NIST SRM 1691(300 nm PSL). Then the particle size and uncertainty for differential mobility analyzer(DMA) using the NIST SRM 1963(100 nm PSL). In result, calibration of prototype DMA is measured using 300 nm NIST SRM 1691, then sheath air flow was corrected 126.67 ㎤/s. Corrected sheath air flow is used in uncertainty measurement of prototype DMA. Uncertainty analysis is performed using NIST SRM 1963(100 nm PSL). The experimental result shows that NIST SRM 1963 is measured as 102.17 nm with a type A uncertainty of 0.33 nm.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2004.10a
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• pp.1335-1338
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• 2004

This paper describes the result of structure analysis of body structure. The purpose of the analysis is to evaluate an safety which body structure shall be considered fully sufficient rigidity so as to satisfy proper system function under maximum load and operating condition. Material of body structure applied an aluminum alloy. Body structure consist of side frame, under frame, roof frame, end frame. FEM analysis is based on 'Performance Test Standard for Electrical Multiple Unit, noticed by Ministry of Construction & Transportation, in 2000 ' and reference code is JIS E 7105. The analysis results have been very safety and stable for design load conditions.

• Journal of Ocean Engineering and Technology
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• v.10 no.2
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• pp.98-105
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• 1996

A method is proposed to evaluate the elastic-plastic fracture resistance curve only with load displacement records without the crack length measurement in CT specimen. This method is based on the idea that the effect of plastic deformation and the crack growth can be measured only by using a load-displacement record. If we know the reference-load curve representing the hardening of specimen, then the crack extension can be calculated by the elastic compliance determined from the load ratio. The results of this proposed method were compared to those of the elastic-plastic fracture resistance curve for the ASTM standard unloading compliance method. The experimental results for two kinds of ductile materials showed that the proposed method well simulates the material J-R curves. This method is currently applied for CT specimens. but it can be extended to the other specimen geometries.

• Proceedings of the KSR Conference
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• 2003.10c
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• pp.59-64
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• 2003

This paper describes the result of structure analysis and load test of body structure. The purpose of the analysis and test is to evaluate an safety which body structure shall be considered fully sufficient rigidity so as to satisfy proper system function under maximum load and operating condition. Material of body structure applied an aluminum alloy. This strength test is based on 'Performance Test Standard for Electrical Multiple Unit, noticed by Ministry of Construction & Transportation, in 2000' and reference code is JIS E 7105

• Proceedings of the KSR Conference
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• 2002.10a
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• pp.156-161
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• 2002

This paper describes the result of carbody load test. The purpose of the test is to evaluate an safety which carbody structure shall be considered fully sufficient rigidity so as to satisfy proper system function under maximum load and operating condition. Carbody material applied a stainless steel and an aluminum alloy, The stainless steel model is the carbody of a motor car which is delivering to KNR line 1 in 2002 and the aluminum alloy model is the carbody of a motor car which is delivering to GWANGJU line 1 in 2003. This strength test is based on "performance test standard for Electrical Multiple Unit, noticed by Ministry of Construction ＆ Transportation, in 2000" and reference code is UIC 566 and JIS E 7105.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.10a
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• pp.49-54
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• 2005

This paper describes the result of structure analysis and load test of body structure. The purpose of the analysis and test is to evaluate an safety which body structure shall be considered fully sufficient rigidity so as to satisfy proper system function under maximum load and operating condition. Material of body structure applied an aluminum alloy. Body structure consist of side frame, under frame, roof frame, end frame. Both FEM analysis and load test are based on 'Performance Test Standard for Electrical Multiple Unit, noticed by Ministry of Construction & Transportation, in 2000' and reference code is JIS E 7105. The test results have been very safety and stable fer design load conditions.