• Title/Summary/Keyword: Standard reference data

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Laboratory Evaluation of the Accuracy, Precision, and Inter-instrumental Variance of a Portable Photoionization Detector (휴대용 광이온화 검출기의 정확도, 정밀도 및 기기간 차이에 대한 실험실 평가)

  • Choi, Dongmin;Choi, Youngeun;Yoon, Chungsik;Rhie, Kwangwon;Lee, Yunkeun;Lee, Ikmo;Park, Jeongim
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.22 no.3
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    • pp.200-208
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    • 2012
  • Objectives: This study investigated the performance of three separate units of a portable photoionization detector (PID, ppb-RAE 3000) for measuring volatile organic compounds (VOCs) in a laboratory. Methods: A laboratory evaluation of the accuracy, precision, and inter-instrumental variance of three separate units of a portable PID (ppb-RAE 3000) was performed. The evaluation was based on the preparation of a test air sample of known toluene or ethylacetate concentration in a Tedlar$^{(R)}$ bag. The test air sample was monitored and data were logged consecutively by the three PIDs. A certified gas of 50 ppm toluene was also monitored during the test to ensure the reliability of the generated test air sample. Four different concentrations ranging from 0.1 to 2 TLV were used and a series of five measurements for each concentration level was performed. The accuracy was evaluated using National Institute for Occupational Safety and Health (NIOSH) criteria. Results: The results from the oldest ppb-RAE3000 unit among the three test units generally fell outside the NIOSH recommended accuracy criteria of ${\pm}25%$, whereas the other two units produced results which were acceptable at, or greater than, 25 ppm of toluene, or 0.5 TLV. These units also met the NIOSH criteria for some ethylacetate measurements but the results were not consistent. Conclusions: Considering the inconsistent performance of these ppb-RAE 3000 units, this device may not be appropriate for use as an alternative to the standard measurement methods. However, it can serve good survey instruments to identify exposure sources or concentration profiles. For all applications, the ppb-RAE 3000 should be used with frequent calibration checks, additional validation using a reference material, and careful maintenance.

Markov Chain Properties of Sea Surface Temperature Anomalies at the Southeastern Coast of Korea (한국 남동연안 이상수온의 마르코프 연쇄 성질)

  • Kang, Yong-Q.;Gong, Yeong
    • 한국해양학회지
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    • v.22 no.2
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    • pp.57-62
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    • 1987
  • The Markov chain properties of the sea surface temperature (SST) anomalies, namely, the dependency of the monthly SST anomaly on that of the previous month, are studied based on the SST data for 28years(1957-1984) at 5 stations in the southeastern coast of Korea. Wi classified the monthly SST anomalies at each station into the low, the normal and the high state, and computed transition probabilities between SST anomalies of two successive months The standard deviation of SST anomalies at each station is used as a reference for the classification of SST anomalies into 3states. The transition probability of the normal state to remain in the same state is about 0.8. The transition probability of the high or the low states to remain in the same state is about one half. The SST anomalies have almost no probability to transit from the high (the low) state to the low (the high) state. Statistical tests show that the Markov chain properties of SST anomalies are stationary in tine and homogeneous in space. The multi-step Markov chain analysis shows that the 'memory' of the SST anomalies at the coastal stations remains about 3 months.

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A Study of the Nonlinear Characteristics Improvement for a Electronic Scale using Multiple Regression Analysis (다항식 회귀분석을 이용한 전자저울의 비선형 특성 개선 연구)

  • Chae, Gyoo-Soo
    • Journal of Convergence for Information Technology
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    • v.9 no.6
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    • pp.1-6
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    • 2019
  • In this study, the development of a weight estimation model of electronic scale with nonlinear characteristics is presented using polynomial regression analysis. The output voltage of the load cell was measured directly using the reference mass. And a polynomial regression model was obtained using the matrix and curve fitting function of MS Office Excel. The weight was measured in 100g units using a load cell electronic scale measuring up to 5kg and the polynomial regression model was obtained. The error was calculated for simple($1^{st}$), $2^{nd}$ and $3^{rd}$ order polynomial regression. To analyze the suitability of the regression function for each model, the coefficient of determination was presented to indicate the correlation between the estimated mass and the measured data. Using the third order polynomial model proposed here, a very accurate model was obtained with a standard deviation of 10g and the determinant coefficient of 1.0. Based on the theory of multi regression model presented here, it can be used in various statistical researches such as weather forecast, new drug development and economic indicators analysis using logistic regression analysis, which has been widely used in artificial intelligence fields.

A Study on the Performance Evaluation of Water(wash out) Resistance of 5-Type Repair Materials in Water Leakage of Underground Concrete Structures (지하 콘크리트 구조물 누수부위에 시공되는 5계열 보수재료의 유실 저항 성능 평가 연구)

  • Kim, Soo-Yeon;Yoo, Jae-Yong;Oh, Sang-Keun
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.24 no.5
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    • pp.61-68
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    • 2020
  • In this study, the international standard ISO TS 16774 Part 3 Test Method for Water (wash out) Resistance and KS F 4935 「Sealant Injection type for water leakage maintenance of adhesive flexible rubber asphalt series」, which are standardized as a quality control method of injection type repair materials used for water leakage cracks in underground concrete structures, are currently used in Korea. As a result, considering the performance criteria of "mass change rate -0.1%" stipulated in KS F 4935, the remaining 13 types repair materials, excluding RG-2 of synthetic rubber and UG-1 of urethane, need to be reviewed for stabilization of the loss resistance due to the flow of ground water. The results of this study are determined to be available as a basic indicator for the selection of repair materials used for cracks in concrete structures. In addition, it is expected that the results of this study can be utilized as reference data that can be reflected in the improvement of the quality of repair materials that will be researched and developed later.

The History and Development of the Marine Environment QA/QC (Quality Assurance/Quality Control) Management System (해양환경 정도관리제도 운영에 대한 고찰)

  • PARK, MI-OK;PARK, JUN-KUN;KIM, SEONG-GIL;KIM, SEONG-SOO
    • The Sea:JOURNAL OF THE KOREAN SOCIETY OF OCEANOGRAPHY
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    • v.26 no.3
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    • pp.185-200
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    • 2021
  • The Marine Environment QA/QC management system has been operated since 2010 to secure the reliability of data and improve the analysis capabilities of measurement and analysis institutions. From 2010 to 2020, the cumulative number of measurement and analysis institutions participated in the QA/QC management system was 266. And the number of certificates issued by the ministry of oceans and fisheries is 182. A total of 32 reference materials for proficiency testing and interlaboratory comparisons have been developed. They were first developed focusing on items (Nutrients, COD) commonly analyzed in marine environmental measuring network, marine pollution impact surveys, sea area utilization impact assessment, deepsea water surveys, and information network on fishing ground environments. In addition, it is time to expand the filed of the QA/QC management system, such as seawater temperature, salinity, PCBs and PAHs in sediments, which are mainly analyzed in most monitoring programs. On-site assessment has been conducted for 162 laboratories according to ISO/IEC 17025 to evaluate their conformity of the quality management system and deficiency. In terms of management and technology requirements, about 4.2% of organizations showed insufficient division of duties among employees 8.7% of them revealed the lack of employee training. By test item, about 6.3% of organizations showed the lack of standard substance management and the state of the cleaning glassware was pointed out in about 5.4% of them. The QA/QC management system should be continuously supplemented by identifying the causes of nonconformities and area for improvement.

A research on cyber target importance ranking using PageRank algorithm (PageRank 알고리즘을 활용한 사이버표적 중요성 순위 선정 방안 연구)

  • Kim, Kook-jin;Oh, Seung-hwan;Lee, Dong-hwan;Oh, Haeng-rok;Lee, Jung-sik;Shin, Dong-kyoo
    • Journal of Internet Computing and Services
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    • v.22 no.6
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    • pp.115-127
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    • 2021
  • With the development of science and technology around the world, the realm of cyberspace, following land, sea, air, and space, is also recognized as a battlefield area. Accordingly, it is necessary to design and establish various elements such as definitions, systems, procedures, and plans for not only physical operations in land, sea, air, and space but also cyber operations in cyberspace. In this research, the importance of cyber targets that can be considered when prioritizing the list of cyber targets selected through intermediate target development in the target development and prioritization stage of targeting processing of cyber operations was selected as a factor to be considered. We propose a method to calculate the score for the cyber target and use it as a part of the cyber target prioritization score. Accordingly, in the cyber target prioritization process, the cyber target importance category is set, and the cyber target importance concept and reference item are derived. We propose a TIR (Target Importance Rank) algorithm that synthesizes parameters such as Event Prioritization Framework based on PageRank algorithm for score calculation and synthesis for each derived standard item. And, by constructing the Stuxnet case-based network topology and scenario data, a cyber target importance score is derived with the proposed algorithm, and the cyber target is prioritized to verify the proposed algorithm.

Estimating soils properties using NIRS to assess amendments in intensive horticultural production

  • Pena, Francisco;Gallardo, Natalia;Campillo, Carmen Del;Garrido, Ana;Cabanas, Victor Fernandez;Delgado, Antonio
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.1615-1615
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    • 2001
  • During the past ten years, Near Infrared Spectroscopy has been successfully applied to the analysis of a great variety of agriculture products. Previous works (Morra et al., 1991; Salgo et al., 1998) have shown the potential of this technology for soil analysis, estimating different parameters just with one single scan. The main advantages of NIR applications in soils are the speed of response, allowing the increase of the number of samples analysed to define a particular soil, and the instantaneous elaboration of recommendations for fertilization and soil amendment. Another advantage is to avoid the use of chemical reagents at all, being an environmentally safe technique. In this paper, we have studied a set of 129 soil samples selected from representative glasshouse soils from Southern Spain. The samples were dried, milled, and sieved to pass a 2 mm sieve and then analysed for organic carbon, total nitrogen, inorganic nitrogen (nitrate ammonium), hygroscopic humidity, pH and electrical conductivity in the 1:1 extract. NIR spectra of all samples were obtained in reflectance mode using a Foss NIR Systems 6500 spectrophotometer equipped with a spinning module. Calibration equations were developed for seven analytical parameters (ph, Total nitrogen, organic nitrogen, organic carbon, C/N ratio and Electric Conductivity). Preliminary results show good correlation coefficients and standard errors of cross validation in equations obtained for Organic Carbon, Organic Nitrogen, Total Nitrogen and C/N ratio. Calibrations for nitrates and nitrites, ammonia and electric conductivity were not acceptable. Calibration obtained for pH had an acceptable SECV, but the determination coefficient was found very poor probably due to the reduced range in reference values. Since the estimation of Organic Carbon and C/N ratio are acceptable NIIRS could be used as a fast method to assess the necessity of organic amendments in soils from Mediterranean regions where the low level of organic matter in soils constitutes an important agronomic problem. Furthermore, the possibility of a single and fast estimation of Total Nitrogen (tedious determination by modifications of the Kjeldahl procedure) could provide and interesting data to use in the estimation of nitrogen fertilizer rates by means of nitrogen balances.

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Comparison of physical characteristics of eggs of Trachemys scripta elegans, Pseudemys concinna, and Mauremys reevesii (붉은귀거북(Trachemys scripta elegans)과 리버쿠터(Pseudemys concinna), 국내종 남생이(Mauremys reevesii) 간 알의 외형적 특징 비교)

  • Seung-Ju Cheon;Choong-Ho Ham;Seung-Min Park;Ju-Hee Bae;Ju-Hee Lee;Seong-Ik Jo;Suk-Jin Cheon;Ha-Cheol Sung
    • Korean Journal of Environmental Biology
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    • v.41 no.2
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    • pp.138-144
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    • 2023
  • The main factor of biodiversity decline in major biological populations around the world is invasion of alien species. To protect native species, it is necessary to manage alien species. Recently, to eradicate ecosystem disturbance caused by alien species in Korea, many efforts have been made to capture individuals using nets and purchase captured individuals. However, there is no standard for classifying species due to the form of nest site or external characteristics of eggs of freshwater turtles. Thus, Mauremys reevesii eggs might be discarded due to mistaking as eggs of alien turtles. Based on more data, this study aims to compare and analyze external differences among eggs of Trachemys scripta elegans, Pseudemys concinna, and M. reevesii and use them as reference materials in the process of eradicating alien turtles. This study measured characteristics of eggs of the three turtle species. As a result of comparison, all variables of external characteristics of alien turtles and M. reevesii eggs showed significant differences. The shape of egg was also different, with eggs of T. scripta elegans and P. concinna showing a bicone shape and those of M. reevesii showing an ellipsoid shape. In conclusion, based on results of previous studies and the present study, eggs of M. reevesii, T. scripta elegans, and P. concinna are different in shape and structure. Thus, it is possible to distinguish between M. reevesii and invasive alien turtle using their eggs.

A Temperature Predicting Method for Thermal Behaviour Analysis of Curved Steel Box Girder Bridges (곡선 강박스거더교의 온도거동 분석을 위한 온도분포 예측기법에 관한 연구)

  • Cho, Kwang-Il;Won, Jeong-Hun;Kim, Sang-Hyo;Lu, Yung-Chien
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.28 no.1A
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    • pp.105-113
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    • 2008
  • Solar radiation induces non-uniform temperature distribution in the bridge structure depending on the shape of the structure and shadows cast on it. Especially in the case of curved steel box girder bridges, non-uniform temperature distribution caused by solar radiation may lead to unusual load effects enough to damage the support or even topple the whole curved bridge structure if not designed properly. At present, it is very difficult to design bridges in relation to solar radiation because it is not known exactly how varying temperature distribution affects bridges; at least not specific enough for adoption in design. Standard regulations related to this matter are likewise not complete. In this study, the thermal behavior of curved steel box girder bridges is analyzed while taking the solar radiation effect into consideration. For the analysis, a method of predicting the 3-dimensional temperature distribution of curved bridges was developed. It uses a theoretical solar radiation energy equation together with a commercial FEM program. The behavior of the curved steel box girder bridges was examined using the developed method, while taking into consideration the diverse range of bridge azimuth angles and radii. This study also provides reference data for the thermal design of curved steel box girder bridges under solar radiation, which can be used to develop design guidelines.

A Study on the Comparison of One Step Method and Two Step Method to Improve Reporting of CA 19-9 Results (CA 19-9 결과보고 개선을 위한 One step 방식과 Two step 방식의 비교에 관한 연구)

  • Jae-Seok An;Ji-Na Kim;Kwang-Seo Park;Eun-Bit Joo;Sang-Hyuk Yoon;Yoon-Cheol Kim
    • The Korean Journal of Nuclear Medicine Technology
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    • v.28 no.1
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    • pp.81-87
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    • 2024
  • Purpose: CA 19-9 is the most widely used tumor marker for the diagnosis of digestive system tumor, especially pancreatic and biliary tract cancer. This study was conducted to improve the result value near reference range by comparing the reagents of CA 19-9 one step method and two step method. In addition, it was intended to establish a standard for selecting reagents. Material and Methods: 120 patients who visited the National Cancer Center in 2023 were selected as subjects for this study. The reagents used in the study were CA 19-9 IRMA kits (Shinjin, Korea) and three types of reagents were compared. Two step method reagent that is currently being used (A), one step method reagent (B) and two step method reagent improved by request (C) were compared and regression analysis was performed on their data. And we also performed recovery test, linearity test and hook effect test for each reagent. Result: There were 46 cases of reagent B in which the concentration value was lower than the result measured in reagent A that was previously used, and 77 cases of reagent C. As a result of regression analysis of reagents A, B, and C, the coefficients of determination of reagents A and B, reagents A and C, and reagents B and C were 0.653, 0.577, and 0.875. In the recovery rate test and the linearity test, the results of all reagents were good, and in the hook effect test, reagent B showed a hook effect at a low value. Conclusion: The improved reagent C appears to have been improved based on the concentration value of reagent B, which the manufacturer judged to be more stable at low concentrations. The hook effect in reagent B can be a fatal reason for disqualification when selecting reagents in general patient samples which high-concentration samples appear frequently. The first improved reagent C will be able to be used once it is confirmed that it has more stability for various concentration values.