• Korean Journal of Materials Research
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• v.26 no.5
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• pp.271-280
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• 2016

When a single inorganic precursor is used for the synthesis of a sol-gel coating, there is a problem of cracking on the surface of coating layer. In order to solve this problem of surface cracking, we synthesized inorganic-organic coatings that have hybrid properties of inorganic and organic materials. Sols of various ratios (1:0.07, 0.2, 0.41, 0.82, 1.64, 3.26, 6.54, 13.2) of an inorganic precursor of Tetrabutylorthotitanate ($Ti(OBu)_4$, TBOT) and an organic precursor of ${\gamma}$-Methacryloxy propyltrimethoxysilane (MAPTS) were prepared and coated on stainless steels (SUS316L) by dip coating method. The binding structure and the physical properties of the synthesized coatings were analyzed by FT-IR, FE-SEM, FIB (Focused Ion Beam), and a nano-indenter. Dynamic polarization testing and EIS (electrical impedance spectroscopy) were carried out to evaluate the micro-defects and the corrosion properties of the coatings. The prepared coatings show hybrid properties of inorganic oxides and organic materials. Crack free coatings were prepared when the MAPTS ratio was above a critical value. As the MAPTS ratio increased, the thickness and the corrosion resistance increased, and the hardness decreased.

• Journal of Ocean Engineering and Technology
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• v.1 no.1
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• pp.104-110
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• 1987

Fatigue tests by axial loading (R = 0.05) were carried out to investigate fatigue crack growth characteristics of small surface cracks in 2 1/4 Cr-1 Mo steel at room temperature by using flat specimens with a small artificial pit. All the data of the fatigue crack growth rate obtained in the present test are determined as a function of the stress intensity factor range about a semi-elliptical crack, so that the application of linear fracture mechanics to the surface fatigue crack growth and to the fatigue crack growth into depth, and all the data obtained from tests were discussed in comparison with the data of Type 304 stainless steel and two type of mild steel under the same test conditions. The obtained results are as follows: 1)When the cycle ratios are same, surface fatigue crack length and its depth are almost same and fall within a narrow scatter band in spite of different stress levels. 2)Relations of the surface fatigue crack growth rate (da/dN) and fatigue crack growth rate into depth (db/dN) to its stress intensity factor range ($\Delta K_{Ia}, \Delta K_{Ib}$) can be plotted as a straight line at log-log diagram without dependence of stress level and coincide with the data of part-through crack in various steels.

• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.14 no.1
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• pp.8-14
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• 2018

Printed circuit heat exchangers (PCHEs) are widely used with an increasing demand for industrial applications. PCHEs are capable of operating at high temperatures and pressure. We consider a PCHE as a candidate intermediate heat exchanger type for a high temperature gas-cooled reactor (HTGR). For conventional application using stainless steels, design and manufacturing of PCHEs are well established. For applications to HTGR, knowledge of longitudinal conduction and deformation of channel is required to estimate design margin. This paper analyzes the effects of longitudinal conduction and deformation of channel on thermal performance using a code internally developed for design and analysis of PCHEs. The code has a capability of two dimensional simulations. Longitudinal conduction is estimated using the code. In HTGR operating condition, about ten percent of design margin is required to compensate thermal performance. The cross-sectional images of PCHE channels are obtained using an optical microscope. The images are processed with computer image process technique. We quantify the deformation of channel with dimensional parameters. It is found that the deformation has negative effect on structural integrity. The deformation enhances thermal performance when the shape of channel is straight in laminar flow regime. It reduces thermal performance in cases of a zigzag channel and turbulent flow regime.

• Proceedings of the KWS Conference
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• 2002.10a
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• pp.89-93
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• 2002

A study of noticeable improvement in welding speed in thin-plate Type 304 stainless steels gas tungsten arc (GTA) welding was investigated. The welding speeds were increased to more than 3m/min, up to 8m/min. During the welding, Direct Current Straight Polarity (DCSP) and pulsed current GTA welding processes were carried out, respectively. The appropriate high speed welding parameters were established while achieving a high quality weld. After this, Erichsen test and tensile test were performed. The results obtained wert summarized as following: ultra high speed welding for thin-plate Type 304 could be satisfactorily welded with high speed from 3m/min to 8m/min in both DCSP and pulsed GTA welding; Increasing welding speed was found to decrease the ductility, tensile strength md elongation of welded joint; The optimal frequency would be 200Hz-500Hz for high speed welding in pulsed current welding; DCSP welding could obtain the better results of Erichsen test and tensile test than those of pulsed current welding obtained.

• Journal of Welding and Joining
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• v.18 no.3
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• pp.51-59
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• 2000

Sink roll has been used in molten 55%Al-Zn alloy bath of continuous galvanizing line for sinking and stabilizing working steel strip in molten metal bath. In the process, the sink roll body inevitably build up dross compounds and pitting on the sink roll surface during 55%Al-Zn alloy coated strip production, and the life time of the sink roll is shorten by build up dross compounds and pitting. The present study examined the application of thermally sprayed ceramic coatings method on sink roll body for improving erosion resistance at molten 55% Al-Zn pool. In this experiment, the stainless steels such as STS 316L and STS 430F were used as the substrate materials. The CoNiCr and WE-Co powder were selected as bond coating materials. Moreover $Al_2O_3-ZrO_2-SiO_2 and ZrO_2-SiO_2$ powders selected as the top coating materials. Appearances of the specimens before and after dipping to molten 55%Al-Zn pool were compared and analyzed. As a result of this study, STS430F of substrate, WC-Co of bond spray coatings, $ZrO_2-SiO_2$ power of top spray coatings is the best quality in erosion resistance test at molten 55%Al-Zn pool

• Journal of Ocean Engineering and Technology
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• v.24 no.6
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• pp.97-102
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• 2010

This paper deals with the variability of short term creep rupture time based on previous creep rupture tests and the statistical methodology of the creep life prediction. The results of creep tests performed using constant uniaxial stresses at 600, 650, and $700^{\circ}C$ elevated temperatures were used for a statistical analysis of the inter-specimen variability of the short term creep rupture time. Even under carefully controlled identical testing conditions, the observed short-term creep rupture time showed obvious inter-specimen variability. The statistical aspect of the short term creep rupture time was analyzed using a Weibull statistical analysis. The effect of creep stress on the variability of the creep rupture time was decreased with an increase in the stress level. The effect of the temperature on the variability also decreased with increasing temperature. A long term creep life prediction method that considers this statistical variability is presented. The presented method is in good agreement with the Lason-Miller Parameter (LMP) life prediction method.

• Proceedings of the KSME Conference
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• 2001.11a
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• pp.266-271
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• 2001

Spherical indentation technique was developed to evaluate the flow properties of metallic materials in carbon steel, stainless steel and alloys, etc. Through the spherical indentation test, differently degraded 1Cr-1Mo-0.25V steel's mechanical properties were observed and compared with conventional standard test data. The flow properties of 1Cr-1Mo-0.25V steels were estimated by analyzing the indentation load-depth curve. To characterize the flow property, we used material yield slope and constraint factor index rather than strain-hardening exponent because the variation of strain-hardening exponent was very little and the data showed irregularly. And the constraint factor's effect was small when the material yield slope was taken into account.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.23 no.7 s.166
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• pp.1094-1103
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• 1999

Ice-plugging of tube in nuclear power plant has been widely used for the purpose of preventing flow of the tube temporarily like a valve. Most common plugging method employs Liquid Nitrogen Gas of $-196^{\circ}C$. According to the change of tube materials and its dimension, the thermal stress caused from the application of the frozen gas can be varied. In this research, a series of experiments have been carried out to inspect the effect of tube geometry on thermal stresses induced due to ice-plugging. Two typical dimension of stainless and mild steels of 3 and 6 inch diameters were used for the experiments. Each critical spots were checked using strain rosette gages. Another inspection was made on the pressure and temperature of the fluid. It is shown that significant thermal stress level which can cause plastic deformation of failure has not been noticed in this series of experiments.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.25 no.4
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• pp.741-747
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• 2001

Three-dimensional, elastic-plastic finite element analyses for circumferential through-wall cracked pipes are performed using actual tensile data of stainless steels, for two purposes. The first one is to validate the recently-proposed enhanced reference stress (ERS) method to estimate the J-integral and COD for circumferential through-wall cracked pipes. The second one is to compare those results with the GE/EPRI estimations. It is found that the J-integral and COD estimations according to the GE/EPRI method can be very sensitive to how the stress-strain data are fitted using the Ramberg-Osgood relation. Moreover, no tendency can be found regarding the most appropriate fitting range for the Ramberg-Osgood fit. On the contrary, the J-integral and COD estimations based on the ERS method give more accurate results than the GE/EPRI estimation. The present results provide confidence in applying the proposed method to the Leak-Before-Break(LBB) analysis.

• Proceedings of the Korean Nuclear Society Conference
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• 1998.05b
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• pp.336-343
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• 1998

An iteration method has been developed for determining crack growth and fracture resistance cure (J-R curve) from the load versus load-line displacement record only. In this method, the hardening curve, the load versus displacement curve at a given crack length, is assumed to be a power-law function, where the exponent varies with the crack length. The exponent is determined by an iterative calculation method with the assumption that the exponent varies linearly with the load-line displacement. The proposed method was applied to the static J-R tests using compact tension(CT) specimens, a three-point bend (TPB) specimen, and a cracked round bar (CRB) specimen as well as it was applied to the quasi-dynamic J-R tests using CT specimens. The J-R curves determined by the proposed method were compared with those obtained by the conventional testing methodologies. The results showed that the J-R curves could be determined directly by the proposed iteration method with sufficient accuracy in the specimens from SA508, SA533, and SA516 pressure vessel steels and SA312 Type 347 stainless steel.