• 제목/요약/키워드: Stainless needle

검색결과 45건 처리시간 0.043초

Dynamic SPME를 이용한 공기 중 지방산 분석 (Analysis of Volatile Fatty Acids in Air by Dynamic SPME)

  • 유미선;양성봉;하남기
    • 한국환경과학회지
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    • 제19권12호
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    • pp.1447-1454
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    • 2010
  • In this study, the detection limits of lower fatty acids in air were investigated by using Dynamic SPME(Solid Phase Micro-Extraction), i.e. improved Head Space - SPME method(HS-SPME). This Dynamic SPME, called SPDE(Solid Phase Dynamic Extraction), is the analytical method for volatile compounds in air with the extraction by using a stainless steel needle of which inner surface is coated with adsorption material and following the gas chromatographic analysis by inserting the needle into a injection port of GC and subsequently, desorption of the volatile compounds into a gas-chromatographic column. Extraction was carried out by passing the sample air through the needle with a suction pump which has been used for a detection tube. The result of measurement for the 6 lower fatty acids showed that the detection limits ranged from 0.10 ppm to 0.44 ppm and the linear correlation coefficients were over 0.99. Relative standard deviations obtained from 5 analytical repetition of a ca. 1.6 ppm standard mixture were in the range of 1.87%~2.47%. This method has been shown to be a adequate for the measuring C2~C5 fatty acids in air in the concentrations of over several hundreds ppb.

불평등 전계 시 에폭시와 N2, dry-air 혼합절연체의 절연파괴특성 (Electrical Breakdown Characteristics of Composite Insulation Composed of Epoxy Resins with N2, Dry-air in Non-uniform Field)

  • 정해은;박성희;강성화;임기조
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.462-463
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    • 2007
  • SF6 widely used as insulating gas is rising as the environment problem. For decreasing this greenhouse gas, electrical breakdown characteristics of composite insulation composed of epoxy resins with N2, air are studied in non-uniform field. The gap of needle to plane was 3mm, 5mm. The pressure of air, nitrogen was varied within the range of 0.1~0.6MPa. The thickness of a needle is 1mm and the curvature radius of the end of needle is 100um. The diameter of a plane made of the stainless steel is 50mm. As a result of the experiment, the breakdown voltage is increased about 3 times when epoxy resins is composited. The thickness of epoxy resins filled opposite to electrode concentrated electric field weakly influences on breakdown voltage.

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에폭시와 dry-air 혼합절연물의 절연파괴특성 (Electrical Breakdown Characteristics of Epoxy and dry-air Composite Insulation)

  • 정해은;오진헌;임종남;강성화;임기조
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2007년도 제38회 하계학술대회
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    • pp.1389-1390
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    • 2007
  • SF6 gas used widely as insulating component is rising as the environment problem. Electrical breakdown characteristics of epoxy and dry-air composite insulation was investigated on thickness of epoxy and pressure of dry-air under non-uniform field. The gap of needle to plane was from 2mm to 5mm. The pressure of dry-air was varied within the range of $0.1{\sim}0.6$ MPa. The thickness of a needle was 1mm and the curvature radius of a needle end was 100um. The diameter of a plane made of the stainless steel was 50mm. As a result of the experiment, breakdown voltage was increased about 3 times when epoxy was used. The impact that the thickness of epoxy influences on breakdown voltage was poor. It needs suitable thickness computation because the insulating gap of the gas is short as epoxy thickness increases.

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Dental needle foreign body in the neck: a case report

  • Mohammed, Hassen;Shallik, Nabil;Barsoum, Mina;Abdulla, Majid Al;Dogan, Zynel;Ahmed, Hassan Haidar;Moustafa, Abbas
    • Journal of Dental Anesthesia and Pain Medicine
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    • 제20권2호
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    • pp.83-87
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    • 2020
  • Foreign body (FB) ingestion is commonly seen in the ear nose and throat (ENT) field, with different presentations and sequelae. FBs can arrest in the upper aerodigestive tract or continue further down into either the airway tract to the bronchus or the digestive tract to the intestines. The pathway of an FB depends on the size and shape of the FB and how sharp its edges are. Since the 20th century, the use of disposable stainless-steel needles in the oral cavity has proven to be an effective and safe method for performing various intraoral procedures like dental infiltration or a root canal wash. Complications from their use are rare. Generally, dental needle breakages are caused by patients biting the needle, incorrect injection techniques, or inadequate preventative measures. The sudden movement of a patient during a procedure is one of the most common causes of breakage. Occasionally, needles are swallowed during dental procedures such as a root canal. Here, we report a case of a patient that swallowed a broken needle during a dental procedure. A few days later, the patient presented with neck pain, swelling, and a FB sensation. When the patient presented, she claimed that her symptoms had onset after consuming a meal containing duck meat. Initially, the patient was diagnosed as having ingested a duck bone. However, intraoperatively, the FB was discovered to be an injection needle that had migrated from the throat to the neck.

온침 시술 시 생체 조직 내 열분포 분석에 관한 연구 (Thermal Distribution in Living Tissue during Warm Needling Therapy)

  • 김종연;이종수
    • 한방재활의학과학회지
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    • 제24권3호
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    • pp.111-119
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    • 2014
  • Objectives This study aims to analyze a thermal distribution in biological living tissue during warm needling therapy by using a finite element method. The analysis provides an understanding of warm needling's efficacy and safety. Methods A model which consisted of four-layered tissue and stainless steel needle was adopted to analyze the thermal distribution in living tissue with a bioheat transfer analysis. The governing equation for the analysis was a Pennes' bioheat equation. A heat source characteristic of warm needling therapy was obtained by previous experimental measurements. The first analysis of the time-dependent temperature distribution was conducted through points on a boundary between the needle and the tissue. The second analysis was conducted to visualize the horizontal temperature distribution. Results When heat source's peak temperatures was above $500^{\circ}C$ and temperature rising rates were relatively slow, the peak temperature at skin surface exceeded a threshold of pain and tissue damage ($45^{\circ}C$), whereas when the peak temperature was around $400^{\circ}C$, the peak temperature at the skin surface was within a safe limit. In addition, the conduction of combustion energy from the moxa was limited to the skin layer around the needle. Conclusions The results suggest that the skin layer around the needle can be heated effectively by warm needling therapy, but it appears to have little effect at the deeper tissue. These findings enhance our understanding of the efficacy and the safety of the warm needling therapy.

22Cr-15Ni-5W 슈퍼 오스테나이트계(系) 스테인리스강(鋼)의 고온산화(高溫酸化) 및 내식성(耐蝕性)에 미치는 결정립(結晶粒) 크기의 영향(影響) (Effect of Grain Size on Corrosion Resistance and High Temperature Oxidation Behavior of 22Cr-15Ni-5W Super Austenitic Stainless Steels)

  • 김효종;이해우;이종문;강창룡
    • 동력기계공학회지
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    • 제10권3호
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    • pp.51-57
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    • 2006
  • The effect of grain size on corrosion resistance and high temperature oxidation behavior was studied in 22Cr-15Ni-5W super austenitic stainless steels for desulfurization equipment as a heat power station. In the high temperature oxidation test, oxidation rate was increased as the temperature increased from $600^{\circ}C\;to\;800^{\circ}C$. In vapor, oxidation rate was faster than that in air. Because the vapor was inhibited nucleation of $Cr_2O_3$ film. And the high temperature oxidation resistance at $600^{\circ}C{\sim}800^{\circ}C$ was excellent from all specimens and specimen of the smallest grain size was the most excellent. Because increasing of diffusion course through the grain-boundary was promoted nucleation and growth of $Cr_2O_3$ film. In the test temperature at $600^{\circ}C{\sim}800^{\circ}C$, Cr rich round particle oxide was formed in air, whereas Fe rich needle type oxide was developed in vapor.

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13%Cr 스테인리스강의 표면 질소침투처리에 미치는 Al첨가의 영향 (Effect of Al Addition on the Surface Nitrogen Permeation Treatment of 13%Cr Stainless Steels)

  • 윤삼석;김기돈;이해우;강창룡;성장현
    • 열처리공학회지
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    • 제12권3호
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    • pp.221-230
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    • 1999
  • The surface nitrogen permeation of Al alloyed 0.14%C-13%Cr stainless steels was investigated after heat treating at $1050^{\circ}C{\sim}1150^{\circ}C$ in the nitrogen gas atmosphere. The strong affinity between Al and nitrogen permeates the nitrogen through the interior of the steels. Two precipitates of round type and needle type are observed at the surface layer. These precipitates mainly consist of AlN containing plenty of aluminum. The surface layer of 0.53%Al alloyed specimen shows ferrite phase, while the surface layers of 1.65%Al and 2.27%Al alloyed specimens appear ${\gamma}$ plus ${\alpha}$ phases. The depth of nitrogen permeation depends upon the Al content and microstructure of the matrix. The 1.65%Al alloyed specimen representing ${\alpha}+{\gamma}$ matrix phases at the nitrogen permeation temperature shows the maximum case depth in this experiment. Although the surface hardness increases by raising the Al content of the specimen owing to the increase of nitride precipitation density, the nitride precipitation deteriorates the corrosion resistance in the solution of HCl, $H_2SO_4$, and $FeCl_3$.

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식중독 미생물의 biofilm 형성에 대한 계피, 정향 및 레몬그래스 정유의 억제 효과 (Inhibitory Effects of Cinnamon, Clove and Lemongrass Essential Oils against Biofilm Formation by Food Poisoning Bacteria)

  • 김형은;김용석
    • 한국식품위생안전성학회지
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    • 제36권5호
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    • pp.430-439
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    • 2021
  • 항균활성이 뛰어난 식물 정유를 이용하여 식품가공 기구 및 용기에 다양하게 사용되는 polyethylene과 stainless steel 표면에 형성된 식중독 6종의 biofilm 형성에 대한 억제 효과를 연구하였다. 식물 정유 20종의 식중독 미생물에 대한 항균활성을 disk diffusion 방법으로 평가한 결과 cinnamon > clove > lemongrass > peppermint > pine needle 순으로 항균활성을 나타냈다. Cinnamon과 clove 정유의 최소억제농도(MIC)와 최소살균농도(MBC)는 각각 0.63-1.25 mg/mL과 1.25-2. mg/mL의 범위를 나타냈으며, lemongrass 정유의 MIC와 MBC는 각각 1.25-2.50 mg/mL과 2.50-5.00 mg/mL로 약간 낮은 항균활성을 나타냈다. 정유 3종의 biofilm 형성 예방효과는 식중독 미생물과 polyethylene 및 stainless steel에 따라 다소 차이가 있었지만, 0.5% 농도의 cinnamon, clove와 lemongrass 정유를 식품접촉 표면에 미리 코팅하였을 때 biofilm 형성에 영향을 주는 것을 확인하였다. 정유의 농도가 증가할수록 모든 식중독 미생물에 대해서 biofilm 형성을 유의적으로 억제하였으며(P<0.05), 0.5% cinnamon과 clove 정유 처리에 의해 L. monocytogenes ATCC 19112와 S. aureus KCCM 11812의 biofilm이 형성되지 않았다. Polyethylene과 stainless steel coupon 표면에 형성된 식중독 미생물의 biofilm의 제거 효과를 측정한 결과, 식중독 미생물의 종류에 따라 차이가 있었지만 정유의 농도가 증가할수록 biofilm 제거 효과는 높아졌으며, 대체로 clove 정유의 biofilm 제거율이 높은 것으로 나타났다. 본 연구를 통하여 0.5%의 cinnamon과 clove 정유는 polyethylene과 stainless steel 표면에 식중독 미생물이 형성하는 biofilm을 예방, 성장 억제 및 제거할 수 있는 천연 소재로 적용이 가능한 것으로 나타났다.

전기수력학적 분무에서 노즐재질이 입경분포에 미치는 영향 (Effect of Nozzle Material on Drop Size Distribution in Electrohydrodynamic Spraying)

  • 김명찬;이상용
    • 대한기계학회논문집B
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    • 제26권10호
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    • pp.1451-1457
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    • 2002
  • When an aqueous liquid such as water having high electric conductivity and high surface tension is discharged from a nozzle under a strong DC electric field, fine drops ranging from 30 to 450 microns can be obtained only through the spindle mode. In the present study, effects of the electric conductivity and the surface wettability of nozzle materials on formation of drops with this mode were investigated. For that, three nozzles with the same size but with different materials were prepared and tested; a stainless steel needle, and a plain and a metal (gold)-coated (except for the tip portion) silica needles. Uniform drops were obtained with the gold-coated silica nozzle over the wider range of the DC voltage input. That is, formation of the liquid cone and detachment of the liquid spindle (ligament) can be more stabilized and frequent with the needles having high electric conductivity but with low surface wettability at their tips.

진공에서 전극 재질에 따른 절연파괴 전압 특성 파악 (characteristic of breakdown voltage of electrode material in vacuum)

  • 이승수;허준;윤재훈;임기조;강성화
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2008년도 Techno-Fair 및 추계학술대회 논문집 전기물성,응용부문
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    • pp.101-102
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    • 2008
  • SF6 widely used as insulating gas is rising as the environment problem. For decreasing this greenhouse gas, electrical breakdown characteristics of vacuum with air are studied in non-uniform field. The gap of needle to plane was 0.5mm. The pressure of vacuum the range of 10^-4${\sim}$10^-5torr. The diameter of a plane made of the stainless steel is 150mm. As a result of the experiment, the breakdown voltage is increased about degree of vacuum increased. The electrode material influenced breakdown voltage in vacuum.

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