• Title/Summary/Keyword: Stabilized method

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Preparation and Properties of Shape-Stabilized Phase Change Materials from UHMWPE and Paraffin Wax for Latent Heat Storage (파라핀과 초고분자량 폴리에틸렌으로 구성된 형태안정성 상 전이 물질의 제조 및 특성)

  • Lee, Hyun-Seok;Park, Jae-Hoon;Yim, Jong-Ha;Seo, Hye-Jin;Son, Tae-Won
    • Polymer(Korea)
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    • v.39 no.1
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    • pp.23-32
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    • 2015
  • Phase change materials based on ultra high molecular weight of polyethylene (UHMWPE) blended with paraffin wax (mp $65^{\circ}C$) were studied in this paper. In addition, this paper reviews recent studies on the preparation of shape stabilized phase change materials (SSPCM), such as SSPCM from UHMWPE and paraffin wax (mp $65^{\circ}C$), their basic properties and possible applications to latent heat storage. The preparation method was an absorption method. Also, SSPCM composites were prepared by using a hot press at $200^{\circ}C$ for 10 min. The analysis for the shape ability of SSPCM to improve heat efficiency was measured by FTIR, SEM, DSC, XRD, and ARES. UHMWPE composites with 30 wt% paraffin wax (mp $65^{\circ}C$) demonstrated less deterioration of physical property and effective thermal property compared with other conditions. As a result, these SSPCMs could be used for the heat storage and release materials for various products.

Synthesis of Yttria Stabilized Zirconia by Sol-gel Precipitation Using PEG and PVA as Stabilizing Agent

  • Bramhe, Sachin N.;Lee, Young Pil;Nguyen, Tuan Dung;Kim, Taik-Nam
    • Korean Journal of Materials Research
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    • v.23 no.8
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    • pp.441-446
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    • 2013
  • There is increasing interest in zirconia as a dental material due to its aesthetics, as well as the exceptionally high fracture toughness and high strength that are on offer when it is alloyed with certain oxides like yttria. In recent years, many solution based chemical synthesis methods have been reported for synthesis of zirconia, of which the sol-gel method is considered to be best. Here, we synthesize zirconia by a sol gel assisted precipitation method using either PEG or PVA as a stabilizing agent. Zirconia sol is first synthesized using the hydrothermal method. We used NaOH as the precipitating agent in this method because it is easy to remove from the final solution. Zirconium and yttrium salts are used as precursors and PEG or PVA are used as stabilizers to separate the metal ions. The resulting amorphous zirconia powder is calcined at $900^{\circ}C$ for 2 h to get crystallized zirconia. XRD analysis confirmed the partially stabilized zirconia synthesis in all the synthesized powders. SEM was taken to check the morphology of the powder synthesized using either PEG or PVA as a stabilizing agent and finally the transparency was calculated. The results confirmed that the powder synthesized with 10 % PVA as the stabilizing agent had highest percentage of transparency among all the synthesized powder.

Formulation of Rectal Supopositories of Omeprazole (오메푸라졸 함유 직장좌제의 제제설계)

  • 이창현;황성주;오세종;이계주
    • YAKHAK HOEJI
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    • v.37 no.4
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    • pp.370-382
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    • 1993
  • In order for formulation of rectal containing OMZ, the OMZ suppositories were prepared using water-soluble base, PEG 4000 base and oil-soluble base, Witepsol H 15. Chemical stability of OMZ in suppositories was increased when Witepsol H 15 was used as a suppository base and arginine was added as a stabilizer. The decomposition of OMZ in suppository bases followed the first-order kinetics and their rate constants were 0.11 day $^{1}(t_{1/2}$=/6.25 days) for Witepsol H 15 suppository and 0.48 day $^{1}(t_{1/2}$=/1.43 days) for PEG 4000 suppository, respectively. On the other hand, the decomposition rate constants of Witepsol suppository and PEG suppository stabilized with arginine were 3.89$\times$10$^{-3}$(t$_{1/2}$=171.1 days) and 8.76$\times$10$^{-3}$ day $^{1}(t_{1/2}=79.9 days), respectively. Shelf-lives of the Witepsol and PEG suppositories stabilized with arginine were t$_{90%}$=291.8 days and t$_{90%}$=282.1 days at $35^{\circ}C$ and 75% RH, respectively. The dissolution test of OMZ suppositories was performed by rotating dialysis cell(RDC) method and the release rate constant was calculated by the simplified Higuchi's equation, Q'=K' t$^{1/2}$. Dissolution of OMZ from suppositories was augmented as arginine was added, particle size of OMZ was reduced and a suitable surfactant such as SLS was added. RDC method was more appropriate and available than Paddle method to evaluate the dissolution rate of lipophilic-base suppositoies. Arginine was found to be a very useful exipient for the enhancement of stability and dissolution of OMZ in suppositories.

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Application of Soil Stabilization Technique for Shoulder Construction in Sri Lanka (스리랑카 길어깨 적용을 위한 안정처리 재료의 적용성 평가 연구)

  • Park, Ki Soo;Park, Hee Mun
    • International Journal of Highway Engineering
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    • v.20 no.4
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    • pp.21-26
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    • 2018
  • PURPOSES : The objective of this study is to evaluate the application of soil stabilization method for soft shoulder construction in the iRoad Project of Sri Lanka. METHODS : Firstly, the quantitative analysis of soil strength improvement due to soil stabilization was done for soil samples collected from iRoad construction sites. Two types of soils were selected from iRoad Project sites and prepared for soil stabilization testing by the Road Development Authority. Secondly, the appropriate stabilizer was selected at given soil type based on test results. Two different stabilizers, ST-1 and ST-2, produced in Korea were used for estimating soil strength improvements. Finally, the optimum stabilizer content was determined for improving shoulder performance. The uniaxial compressive strength (UCS) test was conducted to evaluate the strength of stabilized soil samples in accordance with ASTM D 1633. The use of bottom ash as a stabilizer produced from power plant in Sri Lanka was also reviewed in this task. RESULTS : It is found from the UCS testing that a 3% use of soil stabilizer can improve the strength up to 2~5 times in stabilized soft shoulder soils with respect to unstabilized soils. It is also observed from UCS testing that the ST-1 shows high strength improvement in 3% of stabilizer content but the strength improvement rate with increase of stabilizer content is relatively low compared with ST-2. The ST-2 shows a low UCS value at 3% of content but the UCS values increase significantly with increase of stabilizer content. When using the ST-2 as stabilizing agent, the 5% is recommended as minimum content based on UCS testing results. Based on the testing results for bottom ash replacement, the stabilized sample with bottom ash shows the low strength value. CONCLUSIONS : This paper is intended to check the feasibility for use the soil stabilization technique for shoulder construction in Sri Lanka. The use of soil stabilizer enables to improve the durability and strength in soft shoulder materials. When applying the bottom ash as a soil stabilizer, various testings should be conducted to satisfy the specification criteria.

Evaluation of SERS Nanoparticles to Detect Bacillus cereus and Bacillus thuringiensis

  • Hong, Jeehwa;Qin, Jianwei;Van Kessel, Jo Ann S.;Oh, Mirae;Dhakal, Sagar;Lee, Hoonsoo;Hwang, Chansong;Chan, Diane E.;Kim, Dongho;Cho, Hyunjeong;Kim, Moon S.
    • Journal of Biosystems Engineering
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    • v.43 no.4
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    • pp.394-400
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    • 2018
  • Purpose: This research evaluated five types of nanoparticles to develop a surface-enhanced Raman spectroscopy (SERS) method for the rapid detection of two Bacillus species (Bacillus cereus and Bacillus thuringiensis) that are commonly found on fresh produce, which can cause food poisoning. Methods: Bacterial concentrations were adjusted to a constant turbidity, and a total of $30{\mu}L$ of each Bacillus cell suspension was prepared for each nanoparticle. A point-scan Raman system with laser light source of wavelength 785 nm was used to obtain SERS data. Results: There was no qualitative difference in the SERS data of B. cereus and B. thuringiensis for any of the five nanoparticles. Three gold nanoparticles, stabilized in either citrate buffer or ethanol, showed subtle differences in Raman intensities of two Bacillus species at $877.7cm^{-1}$. Conclusions: Among the three types of nanoparticles, the gold nanoparticles stabilized in citrate buffer showed the lowest standard deviation, followed by gold nanoparticles stabilized in ethanol. This result supports the potential application of gold nanoparticles for SERS-based detection of B. cereus and B. thuringiensis.

Combination of Preconditioned Krylov Subspace Methods and Multi-grid Method for Convergence Acceleration of the incompressible Navier-Stokes Equations (비압축성 Navier-Stokes 방정식의 수렴 가속을 위한 예조건화 Krylov 부공간법과 다중 격자법의 결합)

  • Maeng Joo Sung;Choi IL Kon;Lim Youn Woo
    • 한국전산유체공학회:학술대회논문집
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    • 1999.05a
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    • pp.106-112
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    • 1999
  • In this article, combination of the FAS-FMG multi-grid method and the Krylov subspace method was presented in solving two dimensional driven-cavity flows. Three algorithms of the Krylov subspace method, CG, CGSTAB(Bi-CG Stabilized) and GMRES method were tested with MILU preconditioner. As a smoother of the pressure correction equation, the MILU-CG is recommended rather than MILU-GMRES(k) or MILU-CGSTAB, since the MILU-GMRES(k) preconditioner has too much computation on the coarse grid compared to the MILU-CG one. As for the momentum equation, relatively cheap smoother like SIP solver may be sufficient.

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A Study on a New Lifetime allocation Method of Genetic Algorithm with Varying Population Size (개체군 변환 유전자 알고리즘의 새로운 수명 할당 방식에 관한 연구)

  • Kwon, Key-Ho
    • Journal of the Korean Institute of Telematics and Electronics C
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    • v.36C no.1
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    • pp.66-72
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    • 1999
  • In this paper, we suggest a new lifetime allocation method of genetic algorithm with varying population size. This method can control the size of the population according to the fitness values. The population size is stabilized near the neighbourhood of the optimal value. We used the diploidy method in the coding of the chromosomes. Several simulations confirm that the new allocation method can control the size of the population.

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A Study on the Shape Finding and Patterning Procedures for Membrane Structures (막구조의 초기형상 및 재단도 결정알고리즘에 관한 연구)

  • 한상을;이경수;이상주;유용주
    • Proceedings of the Computational Structural Engineering Institute Conference
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    • 1998.10a
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    • pp.298-305
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    • 1998
  • The purpose of this study is to propose the method of determining the initial fabric membrane structures surface and membrane patterning procedures. Tension structure, such as, fabric membrane structures and cable-net, is stabilized by their initial prestress and boundary condition. The process to find initial structural overall shape of tension structures produced by initial prestress called Shape Finding or Shape Analysis. One of the most important factor for the design of membrane structures is to search initial smooth surface, because unlike steel or concrete building elements which resist loads in bending, all tension structure forces are carried within the surface by membrane stress or cable tension. To obtain initial surface of fabric membrane element in large deformation analysis, the membrane element is idealized as cable using a technique with Force-density method. and that result is compared with well-known nonlinear numerical method, such as Newton-raphson method and Dynamic relaxation method. The shape resulting from Force-density method has been dealt with as the initial membrane shape and used patterning procedures.

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ALVEOLAR BONE LOSS & BONE DENSITY CHANCES DURING THE FIRST YEAR A COMPARATIVE STUDY ON FOUR TYPES OF ROOT-FORM ENDOSSEOUS DENTAL IMPLANT SYSTEMS (치근형 골내 임플란트의 초기 1년간 치조골 소실 및 골 밀도 변화에 관한 연구)

  • Jung Young-Chul;Han Chong-Hyun;Lee Keun-Woo
    • The Journal of Korean Academy of Prosthodontics
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    • v.32 no.3
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    • pp.455-469
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    • 1994
  • Regular radiographic examination has been considered an essential diagnositic method for osseointegrated dental implantation. This study investigated marginal bone loss through the measurement on periapical radiographs and changes in bone density through digital subtraction image radiographic method around 88 endoseous root-form dental implants in 43 human subjects. Four types of endosseous dental implants were investigated : Standard series, Mini series and Hex-lock system of Steri-Oss Dental implant system, and $Br{\aa}nemark$-type implant from 3i dental implant system, in a 3 month interval for a total period of 12 months. The results were as follows : 1. Rapid bone loss occurred in the first 3 months in all 4 groups, and the bone level stabilized at the first thread of the implant fixtures. Amount of bone loss for 12 months showed correlation with the length of the polished neck portion. 2. Most of the implant systems showed resorption of alveolar bone up to the polished neck portion although a long polished neck could delay the resolution. 3. Alveolar bone loss apical to the polished neck portion stabilized at the first thread of the fixtures with no correlation to either the time of exposure of the polished neck or types of implant systems. 4. No changes in bone density around the implant threads were observed throughout the experimental period. Bone density decreased at the marginal bone, and increased at the newly-formed alveolar crest. These results indicate that most of the alveolar bone loss occur within the first 12 months after installation of endosseous root-form dental implants resulting in the exposure of polished neck portions, and the bone level stabilizes thereafter at the first thread portions of the implant fixtures. The experimental period of 12 months seems insufficient for observing changes in bone density, and a long-term observation should be needed.

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Comparisons of RCS Characteristic of Spherical Frequency Selective Surfaces with FSS Element Arrangement (FSS 단위셀 배열구조에 따른 구형 주파수 선택 구조의 RCS 특성비교)

  • Hong, Ic-Pyo;Lee, In-Gon
    • Journal of IKEEE
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    • v.16 no.4
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    • pp.328-334
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    • 2012
  • In this paper, we analyzed the electromagnetic characteristics of the spherical frequency selective surface with different arrangement of crossed dipole slot elements for reducing the RCS(radar cross section). The three dimensional MOM(method of moment) with RWG basis is used to analyze the proposed structure. To reduce the simulation time, we applied the BiCGSTab(Biconjugate Gradient Stabilized) algorithm as an iterative method and presented the comparison results with Mie's theoretical results for PEC sphere to show the validity of this paper. From the simulation results, the different arrangement of elements array showed the difference RCS that cannot be negligible. The arrangement method of element in frequency selective surface will be one of variables for the design of curved frequency selective structures.